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Wyświetlanie 1-3 z 3
Tytuł:
Impact of Impulse Shot Peening Parameters on Properties of Stainless Steel Surface
Autorzy:
Wiertel, M.
Zaleski, K.
Gorgol, M.
Skoczylas, A.
Zaleski, R.
Powiązania:
https://bibliotekanauki.pl/articles/1033967.pdf
Data publikacji:
2017-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.-b
81.20.Wk
62.20.Qp
61.72.-y
78.70.Bj
Opis:
Shot peening was applied to austenitic stainless steel 1.4541 (EN). The surface treatment was performed at various impact energies E, impact densities j and ball diameters D. This resulted in improved microhardness, which increases monotonically with the increase of E, j and 1/D. However, its changes with E and j achieve saturation at about 400 HV0.1. On the contrary, no saturation is observed in the investigated range for 1/D. In the un-shot peened 1.4541 (EN) steel, the lifetime component of low intensity was found with use of positron annihilation lifetime spectroscopy (PALS). It corresponds to positron annihilation from delocalized state of positrons in bulk. In the shot peened samples the bulk component is no longer observed. Instead, two types of defects can be identified: vacancy-like defects coupled with edge dislocations and vacancies or their small clusters (consisting 3÷5 vacancies). The results of PALS and hardness testing do not correspond very well, especially in the case of the samples shot peened with balls of varying diameters. The most probable reason for this are different depth profiles of both methods. It seems that the defects, which are responsible for the increase of static microhardness above 400 HV0.1 are located mostly below the surface layer penetrated by positrons.
Źródło:
Acta Physica Polonica A; 2017, 132, 5; 1611-1615
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Gas filling of SBA - 15 silica micropores probed by positron annihilation lifetime spectroscopy (PALS)
Autorzy:
Gorgol, M.
Zaleski, R.
Kierys, A.
Powiązania:
https://bibliotekanauki.pl/articles/147961.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
SBA-15 porous silica
positron annihilation
Opis:
Positron annihilation lifetime measurements were conducted in situ while two gasses (nitrogen and oxygen, respectively) were introduced into the SBA-15 porous silica sample. Slow changes in lifetime spectra were observed during a long lasting gas interaction with the sample. Introduced gases slowly filled the free volumes, starting from the smallest ones, especially small micropores. In the presence of a gas, the rate of change of ortho-positronium (o-Ps) and unbound positron intensity was larger than the rate of change of lifetime. This suggests the existence of an additional process, which reduces the number of ortho-positronium atoms due to the interaction with the gas. Moreover, the process of filling pores with gas was slower than the process of emptying them while the gas was pumped out.
Źródło:
Nukleonika; 2013, 58, 1; 229-233
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Porosity of Silica Monoliths with Tailored Mesopores of Ink-Bottle Shape Determined by Nitrogen Adsorption and Positron Annihilation Lifetime Spectroscopy
Autorzy:
Sienkiewicz, A.
Kierys, A.
Gorgol, M.
Zaleski, R.
Powiązania:
https://bibliotekanauki.pl/articles/1033934.pdf
Data publikacji:
2017-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Rm
68.43.-h
81.70.-q
78.70.Bj
36.10.Dr
Opis:
The comparison of pore size distributions obtained with the use of two porosimetric methods: low temperature nitrogen sorption (LN2) and positron annihilation lifetime spectroscopy (PALS), was performed for porous silica monoliths. Four investigated samples were prepared under various synthesis conditions. Nitrogen sorption showed the presence of bottle-shaped pores in all investigated samples. In addition, it seems that the presence of methanol during synthesis influences porosity to a greater extent than organic additives. Quite good agreement between the LN2 and PALS results was observed only for the silica monolith synthesized with β-cyclodextrins as pore directing agent. The biggest discrepancy in the results obtained from these two techniques was observed for the silica gel synthesized with no additives. The origin of such discrepancies, taking into account the shape of pore size distribution and deficiencies of data analysis techniques, is discussed.
Źródło:
Acta Physica Polonica A; 2017, 132, 5; 1568-1571
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-3 z 3

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