- Tytuł:
- Size and Morphology of Yttria Nanopowders Obtained by Solution Combustion Synthesis
- Autorzy:
-
Gizowska, M.
Kobus, I.
Perkowski, K.
Piątek, M.
Konopka, G.
Witosławska, I.
Osuchowski, M. - Powiązania:
- https://bibliotekanauki.pl/articles/354879.pdf
- Data publikacji:
- 2018
- Wydawca:
- Polska Akademia Nauk. Czytelnia Czasopism PAN
- Tematy:
-
particle size distribution
solution combustion synthesis
thermal analysis
Y2O3 nanopowder - Opis:
- The work presents results of solution combustion method utilization for yttria (Y2O3) nanopowder fabrication. Experiments were carried out with four different reducing agents: urea, glycine, citric acid and malonic acid added in stoichiometric ratio. The reactions were investigated using simultaneous DSC/DTA thermal analysis. After synthesis the reaction products were calcined at temperature range of 800-1100°C and analyzed in terms of particle size, specific surface area and morphology. Best results were obtained for nanoyttria powder produced from glycine. After calcination at temperature of 1100°C the powder exhibits in a form of nanometric, globular particles of diameter <100 nm, according to SEM analysis. The dBET for thus obtained powder is 104 nm, however the powder is agglomerated as the particle size measured by dynamic light scattering analysis is 1190 nm (dV50).
- Źródło:
-
Archives of Metallurgy and Materials; 2018, 63, 2; 743-748
1733-3490 - Pojawia się w:
- Archives of Metallurgy and Materials
- Dostawca treści:
- Biblioteka Nauki
Artykuł