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    Wyświetlanie 1-8 z 8
    Tytuł:
    Investigation of structural-geometric parameters and elemental composition of spherical VT20 alloy powders
    Autorzy:
    Duriagina, Z. A.
    Filimonov, O. S.
    Kulyk, V. V.
    Lemishka, I. A.
    Kuziola, R.
    Powiązania:
    https://bibliotekanauki.pl/articles/368582.pdf
    Data publikacji:
    2019
    Wydawca:
    Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
    Tematy:
    spherical VT20 alloy powders
    structural-geometric parameters
    additive technologies
    fluidity
    bulk density
    hydrodynamic radius
    proszek sferyczny
    technologie przyrostowe
    płynność
    gęstość objętościowa
    promień hydrodynamiczny
    Opis:
    Purpose: Identification of structural-geometrical parameters, technological properties and elemental composition of spherical powders in a wide fraction range with respect to the VT20 alloy has been carried out. This is important for evaluating the optimum filling of a given volume by mixture of powders of different fractions during 3D printing. Design/methodology/approach: During the investigation of spherical Ti-alloy powders, a comprehensive approach was performed using Scanning Electron Microscopy (SEM), Energy-Dispersive X-ray Spectroscopy (EDS), Dynamic Light Scattering (DLS) and Inductively Coupled Plasma Mass Spectrometry (ICP-MS). The surface morphology of the powders was studied on a Tuescan Vega 3 Scanning Electron Microscope. Using the Quantax energy dispersive spectrometer, element distribution maps were obtained and histograms of element distribution in the investigated powders were constructed. ICP-MS analysis was performed to clarify the elemental composition. DLS analysis using Malvern's Zetasizer Nano-ZS equipment allowed us to determine the functional parameters (hydrodynamic radius – Rh, zeta potential – z and specific conductivity) of particles of titanium alloy powder that indirectly indicate a tendency to form conglomerates. Findings: According to the microscopic examinations, the VT20 alloy powder consists of globular-shaped particles with the lamellar traces on their surfaces. The uniformity of the chemical element distribution within each fraction of the investigated powders was confirmed by EDS, and the full conformity of the powder fractions with the elemental composition of the VT20 alloy was confirmed by ICP-MS. The DLS method allowed to establish that the formation of conglomerates would not occur within the studied fractions of the VT20 alloy powder. Research limitations/implications: The use of high sensitive investigation methods gives understanding of the mechanisms of fine structure formation and possibility to control the processes of powder coagulation in the stage of electrostatic interactions. Practical implications: The obtained results can be used for the formation of fine spherical particles of the powder, but at the same time, these technologies can be extended for the particles of non-spherical shape. Originality/value: The DLS method allowed to establish that the formation of conglomerates would not occur within the studied fractions of the VT20 alloy powder. This, in turn, will improve powder melting during 3D printing. The measured zeta potential values allowed us to reveal mechanisms of fine structure formation and to control the processes of powder coagulation in the stage of electrostatic interactions.
    Źródło:
    Journal of Achievements in Materials and Manufacturing Engineering; 2019, 95, 2; 49-56
    1734-8412
    Pojawia się w:
    Journal of Achievements in Materials and Manufacturing Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Mechanical behavior of wheel steels with solid solution and precipitation hardening
    Autorzy:
    Kulyk, V. V.
    Shipitsyn, S. Ya.
    Ostash, O. P.
    Duriagina, Z. A.
    Vira, V. V.
    Powiązania:
    https://bibliotekanauki.pl/articles/378578.pdf
    Data publikacji:
    2019
    Wydawca:
    Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
    Tematy:
    railway wheel steel
    alloying
    resistance to flat formation
    wear
    damaging
    stalowe koło kolejowe
    stopowanie
    odporność na formowanie płaskie
    zużycie
    uszkodzenia
    Opis:
    Purpose: The aim of the proposed research is to investigate operational properties of a wheel steel treated with simultaneous solid solution and precipitation hardening at various carbon content, in comparison with the standard wheel grade T steel. Design/methodology/approach: The mechanical behaviour of wheel steels with increased content of silicon, manganese, vanadium, and nitrogen at various carbon content has been investigated and compared to that of the standard high-strength wheel grade T steel. The steels were undergo thermal treatment due to austenitic heating up to a temperature of 950.C with cooling down in water to 550.C followed by intense blowing of blanks in the air. After that, a tempering was performed at a temperature in the range of 450-650.C. Static strength (UTS), relative elongation (TEL), impact toughness tests (KCV) were determined on standard specimens. The characteristics of Mode I fatigue crack growth resistance of steel were determined on the basis of fatigue macrocrack growth rate diagrams da/dN–ΔKI, obtained by the standard method on compact specimens with the thickness of 10 mm at a frequency of 10-15 Hz and the stress ratio R = 0.1 and R = 0.5 of the loading cycle. The characteristics of Mode II fatigue crack growth resistance were determined on the basis of da/dN–ΔKII diagrams, obtained earlier method on edge notched specimens with the thickness 3.2 mm at a frequency of 10-15 Hz and R = -1 taking account of the crack face friction. Rolling contact fatigue testing was carried out on the model specimens. Findings: The regularities of the change of mechanical characteristics of the high-strength wheel steel with simultaneous solid solution and precipitation hardening at lowered carbon content under static, impact and cyclic loading are studied. Research limitations/implications: The results obtained using laboratory samples should be checked during a real railway wheels investigation. Practical implications: The investigated steel with simultaneous solid solution and precipitation hardening provides high wear resistance of the tread surface and damage resistance determined on the model wheels. Originality/value: A steel with solid solution hardening due to increased content of silicon (up to 0.7%) and manganese (up to 0.8%) and also with precipitation hardening (at optimal content of vanadium and nitrogen [V‧N]‧104 = 28.9%) at lowered carbon content (0.52) possesses high strength and fatigue fracture toughness in cases of Mode I and Mode II loading, causing better combination of wear and damage resistances of the tread surface of the model wheels, as compared to corresponding parameters for grade T steel.
    Źródło:
    Archives of Materials Science and Engineering; 2019, 95, 2; 49-54
    1897-2764
    Pojawia się w:
    Archives of Materials Science and Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and electrochemical properties of the vanadium alloys after low-temperature nitrogen plasma treatment
    Autorzy:
    Duriagina, Z. A.
    Ryzhak, D. D.
    Kulyk, V. V.
    Tepla, T. L.
    Lemishka, I. A.
    Bohun, L. I .
    Powiązania:
    https://bibliotekanauki.pl/articles/1818517.pdf
    Data publikacji:
    2020
    Wydawca:
    Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
    Tematy:
    vanadium alloy
    surface layers
    microhardness
    corrosion
    stop wanadu
    warstwy powierzchniowe
    mikrotwardość
    korozja
    Opis:
    Purpose: The proposed research aims to determine the expediency of surface treatment of vanadium alloys of V-Cr and V-Ti systems due to irradiation of their surfaces with low- temperature nitrogen plasma using plasma torch NO-01. Design/methodology/approach: The investigation of microstructure and X-ray fluorescence analysis (XRF) of the samples were performed using an electron microscope TESCAN Vega3. The microhardness (Vickers hardness) of the samples was measured before and after surface treatment. The study of corrosive properties of the surface layers was performed by an electrochemical impedance spectroscopy (EIS) method. Corrosion damages were identified using impedance dependences. Findings: The microstructure of the surface layers of the V-8Ti, V-15Cr, and V-35Cr alloys in the initial state and after plasma treatment have been investigated. The chemical composition of the surface layers is determined and comparative measurements of the microhardness of these alloys are carried out. Corrosion-electrochemical properties (corrosion potentials, electrochemical impedance spectroscopy and constructed potential-dynamic polarization curves) of investigated alloys after treatment with nitrogen plasma are evaluated. Research limitations/implications: The results obtained using laboratory samples should be checked at the conditions of power equipment operation. Practical implications: This treatment has advantages over other methods of surface engineering since it provides strong surface plastic deformation and the possibility of formation of secondary phases resulting in increases in surface hardness and corrosion resistance. Originality/value: Vanadium alloys have significant advantages over other structural materials due to their high thermal conductivity and swelling resistance, high strength and plasticity up to temperatures of 700-800°C, and good weldability.
    Źródło:
    Archives of Materials Science and Engineering; 2020, 102, 1; 5--12
    1897-2764
    Pojawia się w:
    Archives of Materials Science and Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The character of the structure formation of model alloys of the Fe-Cr-(Zr, Zr-B) system synthesized by powder metallurgy
    Autorzy:
    Duriagina, Z. A.
    Romanyshyn, M. R.
    Kulyk, V. V.
    Kovbasiuk, T. M.
    Trostianchyn, A. M.
    Lemishka, I. A.
    Powiązania:
    https://bibliotekanauki.pl/articles/366907.pdf
    Data publikacji:
    2020
    Wydawca:
    Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
    Tematy:
    model alloys
    phase diagram
    microstructure
    microhardness
    XRD analysis
    stop modelowy
    diagram fazowy
    mikrostruktura
    mikrotwardość
    analiza XRD
    Opis:
    Purpose: The purpose of the work is to synthesize and investigate the character of structure formation, phase composition and properties of model alloys Fe75Cr25, Fe70Cr25Zr5, and Fe69Cr25Zr5B1. Design/methodology/approach: Model alloys are created using traditional powder metallurgy approaches. The sintering process was carried out in an electric arc furnace with a tungsten cathode in a purified argon atmosphere under a pressure of 6·104 Pa on a water cooled copper anode. Annealing of sintered alloys was carried out at a temperature of 800°C for 3 h in an electrocorundum tube. The XRD analysis was performed on diffractometers DRON-3.0M and DRON-4.0M. Microstructure study and phase identification were performed on a REMMA-102-02 scanning electron microscope. The microhardness was measured on a PMT-3M microhardness meter. Findings: When alloying a model alloy of the Fe-Cr system with zirconium in an amount of up to 5%, it is possible to obtain a microstructure of a composite type consisting of a mechanical mixture of a basic Fe2(Cr) solid solution, solid solutions based on Laves phases and dispersive precipitates of these phases of Fe2Zr and FeCrZr compositions. In alloys of such systems or in coatings formed based on such systems, an increase in hardness and wear resistance and creep resistance at a temperature about 800°C will be reached. Research limitations/implications: The obtained results were verified during laser doping with powder mixtures of appropriate composition on stainless steels of ferrite and ferrite-martensitic classes. Practical implications: The character of the structure formation of model alloys and the determined phase transformations in the Fe-Cr, Fe-Cr-Zr, and Fe-Cr-B-Zr systems can be used to improve the chemical composition of alloying plasters during the formation of ferrite and ferrite-martensitic stainless steel coatings. Originality/value: The model alloys were synthesized and their phase composition and microstructure were studied; also, their microhardness was measured. The influence of the chemical composition of the studied materials on the character of structure formation and their properties was analysed.
    Źródło:
    Journal of Achievements in Materials and Manufacturing Engineering; 2020, 100, 2; 49-57
    1734-8412
    Pojawia się w:
    Journal of Achievements in Materials and Manufacturing Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study of structure and morphology of surface layers formed on TRIP steel by the femtosecond laser treatment
    Autorzy:
    Duriagina, Z. A.
    Tepla, T. L.
    Kulyk, V. V.
    Kosarevych, R. Ya.
    Vira, V. V.
    Semeniuk, O. A.
    Powiązania:
    https://bibliotekanauki.pl/articles/367952.pdf
    Data publikacji:
    2019
    Wydawca:
    Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
    Tematy:
    femtosecond laser
    TRIP steel (03X13AG19)
    image processing algorithms
    digital image analysis
    metallographic complex
    laser femtosekundowy
    stal TRIP
    algorytmy przetwarzania obrazu
    cyfrowa analiza obrazu
    Opis:
    Purpose: The purpose of the work is to demonstrate the possibility of using a femtosecond laser for forming surface layers with an adjustable microstructure on the surface of TRIP steel 03X13AG19, and processing the obtained images using digital complexes. Design/methodology/approach: A laser treatment of TRIP steel (03X13AG19) with pulses of femtosecond duration was carried out in a melting mode. The source of the radiation is a femtosecond titanium-sapphire Ti:Al2O3 complex consisting of a predefining femtosecond generator “Mira Optima 900-F” and regenerative amplifier Legend F-1K-HE. Peculiarities of the surface structure of irradiated samples were studied using a Solver P47-PRO atomic force microscope. The structural-geometric parameters of the surface of the investigated steel treated with the femtosecond laser were determined using the software package Nova 1.0.26.1443 and the functions of the Image Analysis. Microstructural analysis was performed using a raster electron microscope JSM 6700F and a METAM-1P microscope. In this work, the digitization of images of microstructures obtained as a result of surface irradiation by highly concentrated energy streams of femtosecond duration has been carried out. The analysis of the surface structure of laser-structured materials was carried out using a metallographic complex with the software ImProcQCV. Findings: It has been revealed that the predetermined change of the laser treatment mode changes the microrelief and the shape and size of the fragments of the surface structure of the investigated steel. The use of digital image processing allowed to generalize the morphological features of the surface structure, to assess in detail the character of the microrelief, and to monitor under in-situ mode the structure and properties of the surface of the material being studied. Research limitations/implications: The obtained research results can be applied to stainless steels of various structural classes. Practical implications: Surface digitization significantly reduces the time for research, improves the quality and accuracy of the data obtained, makes it possible to conduct in-situ researches with the further implementation of the results using the Internet of Things technologies. Originality/value: A comprehensive approach is proposed for the estimation of parameters of laser-induced periodic surface structures (LIPSS) using a metallographic complex with the software ImProcQCV.
    Źródło:
    Journal of Achievements in Materials and Manufacturing Engineering; 2019, 93, 1-2; 5-19
    1734-8412
    Pojawia się w:
    Journal of Achievements in Materials and Manufacturing Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Assessing surface fatigue crack growth in railway wheelset axle
    Autorzy:
    Rudavskyi, D. V.
    Kaniuk, Yu. I.
    Duriagina, Z. A.
    Kulyk, V. V.
    Shefer, M. S.
    Dolinska, I. Ya.
    Powiązania:
    https://bibliotekanauki.pl/articles/1818483.pdf
    Data publikacji:
    2020
    Wydawca:
    Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
    Tematy:
    fatigue crack growth
    mixed mode
    railway axles
    stress intensity factor
    estimation model
    wzrost pęknięć zmęczeniowych
    tryb mieszany
    osie kolejowe
    współczynnik intensywności naprężeń
    model szacowania
    Opis:
    Purpose: The aim of the proposed research is to create a calculation model of surface fatigue crack growth at the axle of railway wheelset working under operational loads. Design/methodology/approach: The energy approach of the fracture mechanics was used to formulate the calculation model of fatigue crack propagation at the wheelset axle surface. The method of least squares was used to determine the investigated material mechanical constants that the kinetic equations of the calculation model contain. The system of differential equations of crack growth kinetics was solved numerically using the Runge-Kutta method. Findings: On the basis of the energy approach of the fracture mechanics the calculation model of fatigue macrocrack growth in three-dimensional elastic-plastic body in case of a mixed-mode I+II+III macromechanism of fracture has been built. On the basis of the created calculation model, the kinetics of the growth of fatigue cracks was investigated both in the middle part of the wheelset axle and in the axle journal. Research limitations/implications: The results obtained on laboratory specimens should be tested during a real railway wheelset axle investigation. Practical implications: The created calculation model can be used in practice to formulate method of residual lifetime estimation of railway wheelset axle. Originality/value: It was shown, that surface crack kinetics depends not only on the crack initial area but also significantly depends on the crack edge geometry and comparatively small crack-like defects at the wheelset axle surface can reach critical sizes in comparatively short run. It has been found that mechanical shear stresses caused by the weight of the loaded railway wagon in the cross section of the wheelset axle journal can significantly accelerate the growth of the transverse fatigue crack at the axle surface, reducing the period of crack subcritical growth by about 20%.
    Źródło:
    Archives of Materials Science and Engineering; 2020, 106, 2; 59--67
    1897-2764
    Pojawia się w:
    Archives of Materials Science and Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The effect of electrolyte composition on the plasma electrolyte oxidation and phase composition of oxide ceramic coatings formed on 2024 aluminium alloy
    Autorzy:
    Posuvailo, V. M.
    Kulyk, V. V.
    Duriagina, Z. A.
    Koval’chuck, I. V.
    Student, M. M.
    Vasyliv, B. D.
    Powiązania:
    https://bibliotekanauki.pl/articles/1818491.pdf
    Data publikacji:
    2020
    Wydawca:
    Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
    Tematy:
    microstructure
    hydrogen peroxide
    porosity
    plasma electrolyte synthesis
    plasma electrolyte oxidation
    mikrostruktura
    nadtlenek wodoru
    porowatość
    Opis:
    Purpose: Purpose of this work is to analyse the process of synthesis of oxide ceramic coatings in plasma electrolytes on 2024 aluminium alloy and to form an electrolyte which allows to reduce energy consumption for the coating formation. Design/methodology/approach: The oxide ceramic coatings were synthesized on 2024 aluminium alloy. The coatings were formed by the alternate application of anode and cathode pulses to the sample. X-ray diffraction analysis of coatings was performed on a DRON-3.0 X-ray diffractometer using CuKa radiation. The thickness of the coatings was determined using a CHY TG-05 thickness gauge. The porosity of the coatings was investigated by analysing the micrographs of the plasma electrolyte oxidation (PEO) coatings obtained on a scanning electron microscope at x500 magnification using the image processing technique. Findings: The electrolyte with 5 g/l H2O2 additive have been elaborated as an optimal composition for synthesis of a coating with an increased content of corundum (a-Al2O3) as compared to a coating synthesized in the same mode in the 3KOH+2Na2SiO3 electrolyte without H2O2. This synthesis mode allows obtaining a coating with a high corundum content at low energy consumption. Research limitations/implications: For further optimization of the synthesis modes, it is necessary to analyse the influence of the phase composition and porosity of the obtained oxide ceramic coatings on their microhardness, wear resistance, and corrosion resistance. Practical implications: Based on the developed modes of synthesis of the coatings, it will be possible to obtain wear and corrosion resistant oxide ceramic coatings with predetermined functional properties and to reduce energy consumption for their formation. Originality/value: Methods for accelerating the formation of coatings have been proposed and tested, in particular, by adding various amounts of hydrogen peroxide to the electrolyte. The content of oxides in the obtained coatings, in particular, their ratios at various concentrations of hydrogen peroxide in the electrolyte, were determined by X-ray phase analysis. The modes of synthesis of the coatings were developed which allow obtaining a continuous coating without cracks with simultaneous decreasing porosity from 4.32% to 3.55-3.53%.
    Źródło:
    Archives of Materials Science and Engineering; 2020, 105, 2; 49--55
    1897-2764
    Pojawia się w:
    Archives of Materials Science and Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The effect of the modification by ultrafine silicon carbide powder on the structure and properties of the Al-Si alloy
    Autorzy:
    Kovbasiuk, T. M.
    Selivorstov, V. Yu.
    Dotsenko, Yu. V.
    Duriagina, Z. A.
    Kulyk, V. V.
    Kasai, O. M.
    Voitovych, V. V.
    Powiązania:
    https://bibliotekanauki.pl/articles/1818500.pdf
    Data publikacji:
    2020
    Wydawca:
    Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
    Tematy:
    Al-Si alloy
    silicon carbide
    modification
    mechanical properties
    microstructure
    microhardness
    Stop Al-Si
    węglik krzemu
    modyfikacja
    właściwości mechaniczne
    mikrostruktura
    mikrotwardość
    Opis:
    Purpose: Determine the possibility of modifying aluminium alloys of the Al-Si system with an ultrafine SiC modifier with a particie size of 3-5 pm. Design/methodology/approach: Processing of the Al-Si alloy was carried out by introducing an ultrafine modifier in the amount of 0.1, 0.2, or 0.3 wt.%. Silicon carbide (SiC) with a particle size in the range of 3-5 pm was used as a modifier. To study the microstructure of the formed surface layers, a metallographic analysis was performed according to the standard method on a microscope MIKPOTEX® MMT-14C using TopView software. Microhardness studies of the samples were carried out on a Vickers microhardness tester NOVOTEST TC-MKV1. The microstructure of castings of the AlSi12 grade was studied at magnification from 100 to 400 times on the horizontal and vertical surfaces of the samples after etching with a 2% NaOH aqueous solution. Findings: Aluminium cast alloy of Al-Si system has been synthesized with the addition of 0.1, 0.2, and 0.3 wt.% ultrafine SiC modifier. It was found that the modification of the AlSi12 alloy by SiC particles of 3-5 pm in size led to an improvement of its microstructure due to the reduction of the volume fraction of micropores and primary Si crystals. It was shown that the AlSi12 aluminium alloy due to the modification by 0.2 wt.% SiC has the best micromechanical properties and macrostructure density. Research limitations/implications: The obtained research results are relevant for cast specimens of the indicated sizes and shapes. The studies did not take into account the influence of the scale factor of the castings. Practical implications: The developed modification technology was recommended for use in the conditions of the foundry "Dnipropetrovsk Aggregate Plant" (Dnipro, Ukraine). Originality/value: The technology of AlSi12 alloy modification of ultrafine SIC modifier with a particle size of 3-5 pm was used for the first time.
    Źródło:
    Archives of Materials Science and Engineering; 2020, 101, 2; 57--62
    1897-2764
    Pojawia się w:
    Archives of Materials Science and Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-8 z 8

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