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Wyświetlanie 1-2 z 2
Tytuł:
Study of Zeolite Phase Made from Rice Husk Ash and Sidrap Clay
Autorzy:
Armayani, M.
Mansur, Musdalifa
Asra, Reza
Irwan, Muh
Ramadhanty, Dhian
Subaer, Subaer
Abdullah, Mohd Mustafa Al Bakri
Aziz, Ikmal Hakem A.
Jeż, Bartłomiej
Nabiałek, Marcin
Powiązania:
https://bibliotekanauki.pl/articles/2203746.pdf
Data publikacji:
2023
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
autoclave
clay
rice husk ash
zeolite
Opis:
Zeolite has been successfully synthesized from clay and rice husk ash in the form of powder by using the hydrothermal method with variations in chemical compositions of alkaline solution and the amount of rice husk ash. The clay raw material was obtained from the Sidrap area of South Sulawesi and rice husk ash is obtained from the burning pile of rice husks. Sidrap clay and rice husk ash were activated using an alkaline solution of NaOH and varied rice husk ash and the addition of AlCl3. The addition of AlCl3, an alkaline solution of NaOH and H2O was used in the amount of 25.5 grams and variations of rice husk ash were 2.5 grams and 6.5 grams. Meanwhile, without the addition of AlCl3, an alkaline solution of NaOH and H2O was used for 20.5 grams and variations of rice husk ash from 2.5 grams and 6.5 grams. Then the mixture was then put into an autoclave with a temperature of 100°C for 3 hours. The basic material used in the manufacture of zeolite is carried out by X-ray Fluorescence (XRF) characterization to determine the constituent elements of basic material, which showed the content of SiO2 was 45.80 wt% in the clay and 93.40% in the rice husk ash. The crystalline structure of the zeolite formed was characterized by X-Ray Diffraction (XRD). It was found the resulting zeolite were identified as Zeolite-Y, Hydrosodalite, and ZSM-5. The microstructure properties of the resulting zeolite were determined by using Scanning Electron Microscopy (SEM).
Źródło:
Archives of Metallurgy and Materials; 2023, 68, 1; 269--274
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of SnO2/TiO2 with the Addition of Polyethylene Glycol via Sol-Gel Method for Self-Cleaning Application
Autorzy:
Halin, Dewi Suriyani Che
Azliza, Azani
Razak, Kamrosni Abdul
Abdullah, Mohd Mustafa Al Bakri
Salleh, Mohd Arif Anuar Mohd
Wahab, Juyana A
Chobpattana, Varistha
Kaczmarek, Łukasz
Nabiałek, Marcin
Jeż, Bartłomiej
Powiązania:
https://bibliotekanauki.pl/articles/2203743.pdf
Data publikacji:
2023
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TiO2
SnO2
thin film
polyethylene glycol
self-cleaning
Opis:
TiO2 is one of the most widely used metal oxide semiconductors in the field of photocatalysis for the self-cleaning purpose to withdraw pollutants. Polyethylene glycol (PEG) is recommended as a stabilizer and booster during preparation of water-soluble TiO2. Preparation of SnO2/TiO2 thin film deposition on the surface of ceramic tile was carried out by the sol-gel spin coating method by adding different amount of PEG (0g, 0.2g, 0.4g, 0.6g, 0.8g) during the preparation of the sol precursor. The effects of PEG content and the annealing temperature on the phase composition, crystallite size and the hydrophilic properties of SnO2/TiO2 films were studied. The X-ray diffraction (XRD) spectra revealed different phases existed when the films were annealed at different annealing temperatures of 350°C, 550°C and 750°C with 0.4 g of PEG addition. The crystallite sizes of the films were measured using Scherrer equation. It shows crystallite size was dependent on crystal structure existed in the films. The films with mixed phases of brookite and rutile shows the smallest crystallite size. In order to measure the hydrophilicity properties of films, the water contact angles for each film with different content of PEG were measured. It can be observed that the water contact angle decreased with the increasing of the content of PEG. It shows the superhydrophilicity properties for the films with the 0.8 g of PEG annealed at 750°C. This demonstrates that the annealed temperature and the addition of PEG affect the phase composition and the hydrophilicity properties of the films.
Źródło:
Archives of Metallurgy and Materials; 2023, 68, 1; 243--248
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-2 z 2

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