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    Wyświetlanie 1-4 z 4
    Tytuł:
    Study On The Electro-Refining Of Tin In Acid Solution From Electronic Waste
    Badanie elektrorafinacji cyny w roztworze kwasu z e-odpadów
    Autorzy:
    Son, S. H.
    Park, S. C.
    Kim, J. H.
    Kim, Y. H.
    Lee, M. S.
    Ahn, J.-W.
    Powiązania:
    https://bibliotekanauki.pl/articles/352665.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    electrorefining
    tin
    electronic waste
    recycling
    high purity
    elektrorafinacja
    cyna
    odpady elektroniczne
    recykling
    Opis:
    The tin metal could be retractable from wasted tin scrap, sludge, and wasted electroplated solution hydrometallurgical treatment, and purification process. In order to be used as resource of electronic devices, the retracted crude metal should be purified to the extent of higher than 99.9%. In this study, tin electro-refining process was performed to purify the casted tin crude metal at various experimental conditions: at the current density of 3, 5A/dm2, and in various electrolytes such as hydrochloric acid, sulfuric acid and methansulfonic acid. Additional experiment was conducted using Rotating Disk Electrode (RDE) in order to investigate the rate determining step of tin electro-refining process. The current efficiency, 65.6%, was achievable at the condition of current density, 5A/dm2, and in the electrolyte of Hydrochloric acid. During tin electro-refining process, impurity dissolved from tin crude metal into the electrolyte was analyzed using Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES), and the result showed the concentration of impurity metal gradually increased. Quantitative analysis on casted tin crude metal showed that it consists of tin with 93.9 wt.% and several impurity metals of Ag, Bi, Pb, Cu, and etc. After tin electro-refining process, the purity of tin increased up to 99.985 wt.%.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1217-1220
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Extraction Factor Of Pure Ammonium Paratungstate From Tungsten Scraps
    Współczynnik ekstrakcji czystego parawolframianu amonu z odpadów wolframowych
    Autorzy:
    Pee, J-H.
    Kim, G. H.
    Lee, H. Y.
    Kim, Y. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/356567.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    raw material
    recycling
    ammonium paratungstate
    tungsten scraps
    extraction
    surowce
    recykling
    parawolfrawian amonu
    odpady wolframowe
    ekstrakcja
    Opis:
    Typical oxidation process of tungsten scraps was modified by the rotary kiln with oxygen burner to increase the oxidation rate of tungsten scraps. Also to accelerate the solubility of solid oxidized products, the hydrothermal reflux method was adapted. By heating tungsten scraps in rotary kiln with oxygen burner at around 900° for 2hrs, the scraps was oxidized completely. Then oxidized products (WO3 and CoWO4) was fully dissolved in the solution of NaOH by hydrothermal reflux method at 150° for 2hrs. The dissolution rate of oxidized products was increased with increasing the reaction temperature and concentration of NaOH. And then CaWO4 and H2WO4 could be generated from the aqueous sodium tungstate solution. Ammonium paratungstate (APT) also could be produced from tungstic acid using by aqueous ammonium solution. The morphologies (cubic and plate types) of APT was controlled by the stirring process of purified solution of ammonium paratungstate.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1403-1405
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Extraction Factor Of Tungsten Sources From Tungsten Scraps By Zinc Decomposition Process
    Współczynnik ekstrakcji związków wolframu z odpadów wolframowych w procesie rozkładu cynku
    Autorzy:
    Pee, J-H.
    Kim, G. H.
    Lee, H. Y.
    Kim, Y. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/354774.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    raw material
    recycling
    zinc decomposition process
    tungsten carbide
    tungstic acid
    surowce
    recykling
    proces rozkładu cynku
    węglik wolframu
    kwas wolframowy
    Opis:
    Decomposition promoting factors and extraction process of tungsten carbide and tungstic acid powders in the zinc decomposition process of tungsten scraps which are composed mostly of tungsten carbide and cobalt were evaluated. Zinc volatility was suppressed by the enclosed graphite crucible and zinc volatilization pressure was produced in the reaction graphite crucible inside an electric furnace for ZDP (Zinc Decomposition Process). Decomposition reaction was done for 2hours at 650°, which 100% decomposed the tungsten scraps that were over 30 mm thick. Decomposed scraps were pulverized under 75μm and were composed of tungsten carbide and cobalt identified by the XRD (X-ray Diffraction). To produce the WC(Tungsten Carbide) powder directly from decomposed scraps, pulverized powders were reacted with hydrochloric acid to remove the cobalt binder. Also to produce the tungstic acid, pulverized powders were reacted with aqua regia to remove the cobalt binder and oxidize the tungsten carbide. Tungsten carbide and tungstic acid powders were identified by XRD and chemical composition analysis.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1311-1314
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Novel Extraction Process Of Rare Earth Elements From NdFeB Powders Via Alkaline Treatment
    Nowy sposób ekstrakcji pierwiastków ziem rzadkich z proszków NdFeB w roztworach alkalicznych
    Autorzy:
    Chung, K. W.
    Kim, C.-J.
    Yoon, H.-S.
    Powiązania:
    https://bibliotekanauki.pl/articles/355324.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    recycling
    NdFeB magnet
    alkaline treatment
    leaching
    selective leaching efficiency
    recykling
    magnes neodymowy
    obróbka alkaliczna
    ługowanie
    wydajność
    Opis:
    The alkaline treatment of NdFeB powders in NaOH solution at various equivalent amounts of NaOH at 100°C was performed. The resultant powders were then leached in 0.5M H2SO4 solution at 25°C for 2 minutes. At 5 equivalents of NaOH, neodymium in NdFeB powders was partially transformed to neodymium hydroxide. The transformation of neodymium to neodymium hydroxide actually occurred at 10 equivalents of NaOH and was facilitated by increasing the equivalent of NaOH from 10 to 30. In addition, iron was partially transformed to magnetite during the alkaline treatment, which was also promoted at a higher equivalent of NaOH. The leaching yield of neodymium from alkaline-treated powders was increased with an increasing equivalent of NaOH up to 10; however, it slightly decreased with the equivalent NaOH of over 10. The leaching yield of iron was inversely proportional to that of rare earth elements. NdFeB powders treated at 10 equivalents of NaOH showed a maximum leaching yield of neodymium and dysprosium of 91.6% and 94.6%, respectively, and the lowest leaching yield of iron of 24.2%, resulting in the highest selective leaching efficiency of 69.4%.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1301-1305
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-4 z 4

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