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Tytuł:
Thermodynamics of solids with a state equation
Autorzy:
Wojnar, R.
Powiązania:
https://bibliotekanauki.pl/articles/279690.pdf
Data publikacji:
1999
Wydawca:
Polskie Towarzystwo Mechaniki Teoretycznej i Stosowanej
Tematy:
thermodynamics
thermoelasticity
phase transitions
Opis:
The thermodynamic relations describing equilibrium of a multi--phase thermoelastic solid are obtained in a way similar to that used in the multiphase fluid theory. The phase transitions of the first order are defined and equilibrium equations of the Capeyron--Clausius type are derived. Also, the phase transistions of the second order are introduced and equilibrium equations of the Ehrenfest type are obtained. A general theory is illustrated by examples.
Analizujemy związki termodynamiczne opisujące równowagę ciała termosprężystego złożonego z wielu faz. Czynimy to w sposób podobny do stosowanego w teorii płynów wielofazowych. Po określeniu przejść fazowych drugiegi i trzeciego rodzaju wyprowadzamy związki typu Clapeyrona--Clausiusza i Ehrenfesta. Ogólną teorię uzupełniamy przykładami.
Źródło:
Journal of Theoretical and Applied Mechanics; 1999, 4; 809-827
1429-2955
Pojawia się w:
Journal of Theoretical and Applied Mechanics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positron annihilation in liquid crystals
Autorzy:
Dryzek, E.
Juszyńska-Gałązka, E.
Powiązania:
https://bibliotekanauki.pl/articles/148118.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
liquid crystals
positron annihilation
phase transitions
Opis:
Positron annihilation studies of liquid crystals are reviewed with particular reference to thermotropic liquid crystals with rod-like molecules. The studies of compounds exhibiting smectic A or smectic E phases indicate that local arrangement of dipole molecules play an important role because high electron density at the end group of molecules can influence substantially formation and annihilation of positronium. The obtained ortho-positronium lifetimes in these phases can be explained by antiparallel pairing of molecules in case of the smectic A phase or a structure with a nanosegregation of alkyl chains and others parts of molecules into sublayers and liquid-like state of alkyl chains in case of the smectic E phase.
Źródło:
Nukleonika; 2015, 60, No. 4, part 1; 703-708
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Exotic phase transitions in RERhSn compounds
Autorzy:
Łątka, K.
Kmieć, R.
Kruk, R.
Pacyna, A.
Rams, M.
Schmidt, T.
Pöttgen, R.
Powiązania:
https://bibliotekanauki.pl/articles/148856.pdf
Data publikacji:
2003
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
magnetic properties
phase transitions
Mössbauer spectroscopy
Opis:
Crystal and magnetic properties of three equiatomic ternary RERhSn compounds (where RE = Ce, Nd, Gd) have been studied by means of X-ray diffraction, ac, and dc magnetic susceptibility measurements, as well as using Mössbauer spectroscopy with 119Sn and 155Gd resonances. CeRhSn does not order magnetically down to 2 K while NdRhSn undergoes ferromagnetic transition at TC = 10.3 K and GdRhSn orders antiferromagnetically below TN = 16 K. Our CeRhSn and NdRhSn samples become superconductive below 6.5 K and 6.9 K, respectively.
Źródło:
Nukleonika; 2003, 48,suppl.1; 35-40
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Critical Phenomena : Towards Modeling with Cellular Automata
Autorzy:
Wiśniewski, A.
Powiązania:
https://bibliotekanauki.pl/articles/92942.pdf
Data publikacji:
2007
Wydawca:
Uniwersytet Przyrodniczo-Humanistyczny w Siedlcach
Tematy:
phase transitions
cellular automata
self-organized criticality
Opis:
The paper presents basic description methods of critical phenomena, i.e. first-order, continuous phase transitions, and an overview of the self-organized criticality concept. In this approach an attempt is made to identify the determinant factors of modeling critical events using cellular automata.
Źródło:
Studia Informatica : systems and information technology; 2007, 2(9); 69-76
1731-2264
Pojawia się w:
Studia Informatica : systems and information technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ammonium nitrate phase state stabilization with small amounts of some organic compounds
Autorzy:
Golovina, N.
Nechiporenko, G.
Nemtsev, G.
Zyuzin, I.
Manelis, G. B.
Lempert, D.
Powiązania:
https://bibliotekanauki.pl/articles/358906.pdf
Data publikacji:
2009
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
ammonium nitrate
phase transitions
phase stabilization
intermolecular interactions
Opis:
The investigation considers phase stabilization of ammonium nitrate for considerable extension of its application area including new generation of gas-generating compositions for airbag inflators. It was shown that alloys of ammonium nitrate with small amounts (2-10%) of some organic compounds can have no phase transitions or at least have only one instead of three ones in initial ammonium nitrate. The mostly effective as stabilizers are the compounds that have rather close crystallographic parameters. A strong donor-acceptor interaction between nitrate-anion and organic molecules are found. Using quantum-chemical calculations, X-ray analysis, X-ray phase analysis, UV- and IR-spectroscopy it was found a new ammonium nitrate phase state in its alloy with some organic additives. This state is stable in temperature range between -50 and +100 C.
Źródło:
Central European Journal of Energetic Materials; 2009, 6, 1; 45-56
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Alternative, Direct Synthesis Method of the Ceramic Solid Solutions Based on BaTiO3 Through a High Energy Ball Milling
Autorzy:
Bąk, W.
Dulian, P.
Garbarz-Glos, B.
Czekaj, D.
Lisińska-Czekaj, A.
Powiązania:
https://bibliotekanauki.pl/articles/351595.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ceramics
mechanochemical synthesis
dielectric properties
phase transitions
ferroelectrics
Opis:
Polycrystalline samples BaTiO3 and the solid solutions Ba0.9 Sr0.1 TiO3, 0.9 Sr0.1 Ti0.9 Sn0.1 O3, Ba0.9 Sr0.1 Ti0.8 Sn0.2 O3 were obtained by means of a mechanochemical treatment based on the high-energy ball milling technique and next a high temperature solid state reaction method. The influence of synthesis condition on microstructural, dielectric and ferroelectric properties of obtained solid solutions were investigated. The structure and morphology of the investigated samples were characterized by an X-ray diffraction (XRD) and scanning electron microscopy (SEM). The characterization of electrical properties of the ceramics within the temperature range from –130°C to 250°C were performed by means of a dielectric spectroscopy method at the frequency ranging from 0.1 Hz to10 MHz. The diffusion of the paraelectric – ferroelectric phase transition and dielectric relaxation for ceramic samples are described.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 805-810
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Temperature-dependent Shock Initiation of CL-20-based High Explosives
Autorzy:
Pi, Z.
Chen, L.
Wu, J.
Powiązania:
https://bibliotekanauki.pl/articles/358764.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
CL-20
shock initiation
heated explosive
phase transitions
numerical simulation
Opis:
To investigate the effects of temperature on the shock initiation characteristics of hexanitrohexaazaisowurtzitane (CL-20), shock initiation experiments on heated C-1 explosive (94% epsilon phase CL-20, and 6% binder, by weight) were performed at temperatures of 20 °C, 48 °C, 75 °C, 95 °C, 125 °C, 142 °C, and 175 °C. An explosive driven flyer device was used to initiate the C-1 charges and manganin pressure gauges were embedded in the C-1 specimen to record the pressure changes with time. Our results show that C-1 becomes more sensitive as the temperature is increased from 20 °C to 95 °C. The ε to γ phase transition in CL-20 occurs at 125 °C; C-1 with CL-20 in the γ phase at 142 °C is less shock sensitive than C-1 with CL-20 in the ε phase at 95 °C or 75 °C. Compared with C-1 at 142 °C, C-1 at 175 °C shows a dramatic increase in shock sensitivity. An ignition and growth reactive flow model was used to simulate the shock initiation of C-1 at various temperatures, and the parameters were obtained by fitting the experimental data. With this parameter set, the shock initiation characteristics of C-1 for temperatures between 20 °C and 175 °C can be derived.
Źródło:
Central European Journal of Energetic Materials; 2017, 14, 2; 361-374
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Properties of Pb1-xBax(Zr1-yTiy)1-zSnzO3 (x = 0.03, y = 0.02, z = 0÷0.08) Ceramics
Autorzy:
Brzezińska, D.
Powiązania:
https://bibliotekanauki.pl/articles/354740.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
PBZT and PBZTS ceramics
phase transitions
dielectric properties
electrical conductivity
Opis:
This paper presents the results of obtaining and investigations of Pb1-xBax(Zr1-yTiy)1-zSnzO33(PBZTS) ceramics with constant x = 0.03 and y = 0.02, and variable z = 0, 0.04, 0.06 and 0.08 (abbreviations of the samples were following PBZTS0, PBZTS4, PBZTS6, PBZTS8, respectively). The investigated compositions are close to rhombohedral-orthorhombic morphotropic phase boundary. The ceramic samples have been obtained by conventional ceramic technology from simple oxides PbO, ZrO2, TiO2, SnO2 and barium carbonate BaCO3. The ceramic powders, after calcination, have been pressed into discs and sintered using free sintering (FS) method. For samples obtained in such a way, the dielectric properties at various frequencies and electrical conductivity have been investigated. The increase of Sn content orders the microstructure of ceramics, and as a result the improvement of the dielectric properties of ceramic samples can be obtained.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 975-982
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Semiconductor Element Substitution on the Electric Properties of Barium Titanate Ceramics
Autorzy:
Garbarz-Glos, B.
Lisińska-Czekaj, A.
Czekaj, D.
Bąk, W.
Powiązania:
https://bibliotekanauki.pl/articles/354672.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
barium titanate
ceramics
dielectric permittivity
electric conductivity
phase transitions
PTCR effect
Opis:
The investigated ceramics were prepared by a solid-state reaction from simple oxides and carbonates with the use of a mixed oxide method (MOM). The morphology of BaTi0.96Si0.04O3 (BTSi04) ceramics was characterised by means of a scanning electron microscopy (SEM). It was found that Si+4 ion substitution supported the grain growth process in BT-based ceramics. The EDS results confirmed the high purity and expected quantitative composition of the synthesized material. The dielectric properties of the ceramics were also determined within the temperature range (ΔT=130-500K). It was found that the substitution of Si+4 ions had a significant influence on temperature behavior of the real (ε’) and imaginary (ε”) parts of electric permittivity as well as the temperature dependence of a.c. conductivity. Temperature regions of PTCR effect (positive temperature coefficient of resistivity) were determined for BTSi04 ceramics in the vicinity of structural phase transitions typical for barium titanate. No distinct maximum indicating a low-temperature structural transition to a rhombohedral phase in BTSi04 was found. The activation energy of conductivity was determined from the Arrhenius plots. It was found that substitution of Si ions in amount of 4wt.% caused almost 50% decrease in an activation energy value.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 887-890
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Diffusive and Displacive Phase Transformations in Nanocomposites under High Pressure Torsion
Autorzy:
Straumal, B.
Kilmametov, A.
Gornakova, A.
Mazilkin, A.
Baretzky, B.
Korneva, A.
Zięba, P.
Powiązania:
https://bibliotekanauki.pl/articles/356575.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high-pressure torsion
Ti-Fe alloys
phase transitions
high-pressure phases
Opis:
The high-pressure torsion (HPT) of Ti-Fe alloys with different iron content has been studied at 7 GPa, 5 anvil rotations and rotation speed of 1 rpm. The alloys have been annealed before HPT in such a way that they contained different amounts of α/α' and β phases. In turn, the β phase contained different concentration of iron. The 5 anvil rotations correspond to the HPT steady-state and to the dynamic equilibrium between formation and annihilation of microstructure defects. HPT leads to the transformation of initial α/α' and β-phases into mixture of α and high-pressure ω-phase. The α → ω and β → ω phase transformations are martensitic, and certain orientation relationships exist between α and ω as well as β and ω phases. However, the composition of ω-phase is the same in all samples after HPT and does not depend on the composition of β-phase (which is different in different initial samples). Therefore, the martensitic (diffusionless) transformations are combined with a certain HPT-driven mass-transfer. We observed also that the structure and properties of phases (namely, α-Ti and ω-Ti) in the Ti – 2.2 wt. % Fe and Ti – 4 wt. % Fe alloys after HPT are equifinal and do not depend on the structure and properties of initial α'-Ti and β-Ti before HPT.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 2; 457-465
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Condensed Geometry II: New Constraints, Temporal Confinement Phase and Structure and Interpretation of Space and Time
Autorzy:
Kabe, Koustubh
Powiązania:
https://bibliotekanauki.pl/articles/1190218.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Ashtekar variables
Loop Quantum Gravity
surface states
phase transitions
string theory
Opis:
In this paper we basically intend to deductively study aspects and physical behavior of time in the Quantum Mechanical and Loop Quantum Gravity regime and the physical interpretations therein. The implicit gauge invariance of the vortical time is deduced. A new form of the Hamiltonian constraint is produced and the corresponding Vector or Diffeomorphism constraint is also introduced, the Gauss constraint being found to be the same as that in the original. The new consequences are discussed. The paper presents fresh new ideas and interpretations as well as perspectives on the spatial as well as the now introduced temporal aspects of Loop Quantum Gravity. In this we basically intend to deductively study aspects and physical behavior of Time in the Quantum Mechanical and Loop quantum gravity regime and the physical interpretations therein. In what follows, we provide a systematic mathematico-physical treatment of the vortical aspect of quantum gravity or a test quantum system, relative to space, as the time for that system. The implicit gauge invariance of the vortical time is deduced. A general theory of implicit and explicit gauge invariance is proposed. The gauging out of the acausality gauge degree of freedom is deduced and the causal direction of time is shown to nucleate out as a self ordered criticality due to a “tweaking” field which is shown to be a form of magnetic phase transition. This magnetic phase arising in the Kodama holomorphic wave functional universe, arises naturally due to the Ashtekar “magnetic” field in general. Also the wave-particle duality of gravity/ geometry as a quantum system is interpreted in terms of the physical role played by time. The long standing problem of the interpretation of the quantum mechanical time-inverse temperature has apriori been resolved with a heuristic interpretation. As an epilogue, the Pauli theorem on time as an operator has been discussed along with the standard proof.
Źródło:
World Scientific News; 2016, 44; 236-256
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Phase transitions in the borate minerals from the Kłodawa Salt Dome (Central Poland) as the indicators of the temperature processes in salt diapirs
Autorzy:
Wachowiak, J.
Toboła, T.
Powiązania:
https://bibliotekanauki.pl/articles/2060065.pdf
Data publikacji:
2014
Wydawca:
Państwowy Instytut Geologiczny – Państwowy Instytut Badawczy
Tematy:
boracite
congolite
phase transitions
temperature study
Zechstein
salt dome
Kłodawa
Polska
Opis:
The diapiric structures of the Polish Lowlands are tectonically deeply seated down to the autochthonous Zechstein strata at a depth of ca. 6 km. In the process of deep burial and halokinetic diapirism, the salt rocks were subjected to diagenetic and metamorphic transformations, with the temperature being an essential factor. Considering the thermal gradient, a temperature of up to ca. 200°C can be achieved in the salt dome within a depth range from several hundred metres to 6 km, which may lead to transformations of the majority of salt minerals. Phase transitions of two borate minerals – boracite and congolite from the Kłodawa salt dome – provide evidence for higher temperatures in the salt dome rocks. The authigenic euhedral crystals of those borate minerals display their external habitus in ambient temperature in the form of regular symmetry (F43c – pseudo-regular polyhedrons), whereas their internal structure is lower: orthorhombic (Pca21) for boracite and rhombohedral (R3C) for congolite. The heating and cooling of boracite and congolite crystals show reversible phase transition. At a temperature of ca. 270°C, boracite crystals change their symmetry: orthorhombic ↔ cubic. In the case of congolite three reversible phase transitions within a temperature range of 50–339°C can be observed: rhombohedral ↔ monoclinic ↔ orthorhombic ↔ cubic symmetry. Those phase transitions, confirmed experimentally in our study, clearly document at least local occurrences of temperatures exceeding 339°C in the Kłodawa salt dome.
Źródło:
Geological Quarterly; 2014, 58, 3; 543--554
1641-7291
Pojawia się w:
Geological Quarterly
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Separate Kinetics of the Polar and Antiferrodistortive Order Parameters in the Antiferroelectric Transition of PbZr1-xTixO3 and the Influence of Defects
Oddzielne kinetyki polarnych i antyferroelektrycznych dystorsji parametrów uporządkowania w przemianie antyferroelektrycznej PBZR1-XTIXO3 oraz wpływ defektów
Autorzy:
Cordero, F.
Craciun, F.
Trequattrini, F.
Galassi, C.
Powiązania:
https://bibliotekanauki.pl/articles/355151.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
antiferroelectric PZT
phase transitions
defect
elasticity
przemiana antyferroelektryczna
przejścia fazowe
defekt
elastyczność
Opis:
The transition from the rhombohedral-ferroelectric to the lower temperature orthorhombic-antiferroelectric phase in Zr-rich PZT involves two order parameters (OPs): 1) the polar OP for the displacements of the cations with respect to the O octahedra; 2) an antiferrodistortive OP responsible for tilting of the octahedra. It is shown that at Ti compositions near the morphotropic boundary with the FE phase (0.046 ≤ x ≤ 0.054), the two OPs may be almost independent of each other at cooling rates of 0.5 K/min or faster, depending on the sample history. This fact gives rise to a great variety of shapes of the curves of the elastic compliance s(T), but all of them can be fitted very well as superpositions of variously broadened steps for each of the modes involved in the transitions, including the tilt transition occurring in the untransformed FE fraction. The evolution of the s(T) curves includes enhancements up to a factor of four during aging for weeks in the region of the AFE/FE coexistence. Restiffening and reduction of the thermal hysteresis of the AFE/FE transition are recovered by heating up to 800-900 K. It is proposed that ageing is due to the clustering of relatively mobile defects, most likely O vacancies, at the domain walls in the coexisting AFE/FE phases. Such defect structures are probably at the origin of intense thermally activated relaxation processes observed above TC in the dielectric and anelastic spectra, and can be annealed out above 800 K, allowing the AFE transition to recover a fast kinetics.
Przemiana fazy romboedrycznej-ferroelektrycznej do niskotemperaturowej fazy rombowej-antyferroelektrycznej bogatej w Zr ceramiki piezoelektrycznej PZT obejmuje dwa parametry uporządkowania (OP): 1) polarny OP z przemieszczeń kationów Zr/Ti w odniesieniu do oktaedrów tlenowych; 2) antyferroelektryczna dystorsja OP odpowiedzialna za przechylenie oktaedrów. Pokazano, że dla zawartości Ti w pobliżu morfotropowej granicy z fazą ferroelektryczną (0,046≤x≤0,054), obydwa OP mogą być prawie niezależne od siebie podczas chłodzenia z szybkością 0,5 K/min lub mniejszą, w zależności od historii próbki. Ten fakt powoduje wielką różnorodność kształtów krzywych podatności sprężystej s(T), ale wszystkie z nich mogą być bardzo dobrze przybliżone jako superpozycje różnie poszerzonych etapów dla każdego z trybów zaangażowanych w przemianę, w tym przemianę nachylenia występującą w nietransformowanej fazie ferroelektrycznej. Zmiana krzywych s(T) obejmuje czterokrotne poszerzenia krzywych po okresie starzenia przez kilka tygodni w regionie współistnienia faz antyferroelektrycznej (AFE) i ferroelektrycznej (FE). Zesztywnienie i zwężenie pętli histerezy termicznej przemiany AFE / FE są odzyskiwane przez podgrzanie do temperatury 800-900 K. Proponuje się, że starzenie się jest spowodowane grupowaniem się stosunkowo mobilnych defektów, najprawdopodobniej wakansów tlenowych, na ścianach domen w współistniejących fazach AFE / FE. Defekty te są zapewne przyczyną silnych, aktywowanych termicznie procesów relaksacyjnych obserwowanych powyżej temperatury krytycznej TC w widmie strat dielektrycznych i mechanicznych, i mogą być wyżarzane powyżej 800 K, umożliwiając przejściu AFE odzyskanie szybkiej kinetyki przemiany.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 1; 381-384
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A review of phase transitions in RbIn-molybdate
Autorzy:
Zapart, M. B.
Zapart, W.
Powiązania:
https://bibliotekanauki.pl/articles/146342.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
electron magnetic resonance (EMR)
trigonal double molybdates
incommensurate phase
ferroelastics
phase transitions
Opis:
The paper gives a brief review of the results of EPR temperature studies of RbIn(MoO4)2 crystal. A sequence of several structural phase transitions has been found in this crystal in the temperature region 84–163 K. The transition at T1 = 163 K leads to an incommensurate triply modulated state, whereas ferroelastic phases start below T2 = 143 K. All the low temperature phases in the temperature region 84–143 K are examples of simultaneously ferroelastic and incommensurate ones. The transition observed at T5 = 84 K seems to suppress the ferroelastic properties of the crystal.
Źródło:
Nukleonika; 2013, 58, 3; 365-370
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Crystalline structures of Rb2UBr6 ionic conductor determined by neutron diffraction
Autorzy:
Małetka, Krzysztof
Ressouche, Eric
Rundlof, Hakan
Tellgren, Rolland
Szczepaniak, Włodzimierz
Zabłocka-Malicka, Monika
Powiązania:
https://bibliotekanauki.pl/articles/146364.pdf
Data publikacji:
2020
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
neutron diffraction
Ionic conductivity
solid electrolyte
phase transitions
crystalline structure
uranium bromide
Opis:
The neutron powder diffraction technique has been used for structural studies of Rb2UBr6 solid electrolyte as a function of temperature. The low-, room-, and high-temperature structures have been determined. At the temperature range of 4.2–80 K, the compound crystallizes in a monoclinic unit cell in the P21/c space group. At 80 K and 853 K, the compound crystallizes in a tetragonal unit cell in the P4/mnc space group. At 300 K, the lattice constants are a = b = 7.745(1) and c = 11.064(1) Å. At the temperature range of 853–960 K, a trigonal phase is observed in the P–3ml space group.
Źródło:
Nukleonika; 2020, 65, 1; 3-11
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
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