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Wyszukujesz frazę "degree of deacetylation" wg kryterium: Temat


Wyświetlanie 1-2 z 2
Tytuł:
Influence of chitosan molecular weight and degree of deacetylation on membrane physicochemical and separation properties in ethanol dehydration by the vapour permeation process
Autorzy:
Gnus, Małgorzata
Powiązania:
https://bibliotekanauki.pl/articles/1034007.pdf
Data publikacji:
2020
Wydawca:
Sieć Badawcza Łukasiewicz - Polskie Towarzystwo Chitynowe
Tematy:
chitosan
degree of deacetylation
molecular weight
separation properties
vapour permeation
Opis:
Membranes were prepared using three chitosans with different molecular weights and degrees of deacetylation. The influence of chitosan features on membrane physicochemical properties, i.e. degree of swelling, contact angle and tensile strength, as well as membrane separation properties in ethanol dehydration by the vapour permeation process are discussed. The conducted experiments showed that an increase in the chitosan molecular weight led to an increase in the membrane surface contact angle concomitant with a decrease in the material selectivity coefficient. On the other hand, an increase in the chitosan degree of deacetylation caused a reduction in ethanol and improved the water permeate flux. There was greater selectivity in the test process for membranes prepared from chitosan with the lowest molecular weight.
Źródło:
Progress on Chemistry and Application of Chitin and its Derivatives; 2020, 25; 79-93
1896-5644
Pojawia się w:
Progress on Chemistry and Application of Chitin and its Derivatives
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Express analysis of chitosan and its derivatives by gel electrophoresis
Autorzy:
Konovalova, Mariya
Shagdarova, Balzhima Ts.
Zubov, Vitaliy
Svirshchevskaya, Elena
Powiązania:
https://bibliotekanauki.pl/articles/1034210.pdf
Data publikacji:
2019
Wydawca:
Sieć Badawcza Łukasiewicz - Polskie Towarzystwo Chitynowe
Tematy:
agarose gel electrophoresis
chitosan
chitosan derivatives
degree of deacetylation
molecular weight
Opis:
Chitosan is one of the most promising polymers for biomedical applications due to its unique properties, such as its biocompatibility, low toxicity, biodegradation, and the presence of reactive amino and hydroxyl groups. Analysis of physicochemical properties of chitosan and its derivatives is a time-consuming process and requires expensive equipment and large amounts of the sample. This paper proposes a method for express analysis of the molecular weight (MW), the degree of deacetylation (DD), the substitution degree (SD), and the charge of chitosan and its derivatives using agarose gel electrophoresis under acidic and neutral conditions with Coomassie staining. Positively charged chitosan samples required acidic Tris Acetate-EDTA (TAE) buffer to move in the gel. The electrophoretic mobility of chitosan depended on MW, DD, SD, and the chitosan charge. Based on the dependences obtained by the proposed method, the MW and DD of commercial chitosan samples were determined. Express analysis of chitosan and its derivatives in agarose gel can be used to monitor the reactions of chitosan modification and to analyse samples with unknown characteristics.
Źródło:
Progress on Chemistry and Application of Chitin and its Derivatives; 2019, 24; 84-95
1896-5644
Pojawia się w:
Progress on Chemistry and Application of Chitin and its Derivatives
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-2 z 2

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