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    Wyświetlanie 1-8 z 8
    Tytuł:
    Microstructural Changes in a High-Manganese Austenitic Fe-Mn-Al-C Steel
    Zmiany mikrostrukturalne w wysokomanganowej stali austenitycznej Fe-Mn-Al-C
    Autorzy:
    Witkowska, M.
    Zielińska-Lipiec, A.
    Kowalska, J.
    Ratuszek, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/350948.pdf
    Data publikacji:
    2014
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    high-manganese austenitic steel hot-rolling
    spinodal decomposition
    carbides
    microstructure
    wysokomanganowa stal austenityczna
    rozpad spinodalny
    węgliki
    mikrostruktura
    Opis:
    Microstructural changes in the age-hardenable Fe-28wt.%Mn-9wt.%Al-1wt.%C steel during ageing at 550°C for various times have been investigated by transmission electron microscopy (TEM) and X-ray diffraction (XRD). The steel was produced in an induction furnace and the ingot, after homogenization at 1150°C for 3 hours under a protective argon atmosphere, was hot-rolled and subsequently cold-rolled up to 23% reduction. The sheet was then aged at 550°C for various times in an argon atmosphere and cooled in air. XRD analysis and TEM observations revealed a modulated structure and superlattice reflections produced by spinodal decomposition, which occurred during ageing at 550°C. Theexistence of satellites suggests that either (Fe, Mn)3AlCx carbides were formed within the austenite matrix by spinodal decomposition during cooling or chemical fluctuactions occurred between the (Fe, Mn)3AlCx carbides and the austenitic matrix.
    W pracy analizowano zmiany mikrostruktury w stali Fe-28%wt. Mn-9%wt. Al-1%wt.C zachodzące podczas starzenia w temperaturze 550°C w różnych czasach. Stal Fe-28Mn-9Al-1C wytopiono w próżniowym piecu indukcyjnym. Po odlaniu wlewek homogenizowano w temperaturze 1150°C przez 3 godziny w atmosferze argonu. Wlewek walcowano na gorąco a następnie na zimno do 23 % odkształcenia. Próbki po odkształceniu starzono w temperaturze 550°C dla różnych czasów w atmosferze argonu i chłodzono na powietrzu. Obserwacje elektronomikroskopowe starzonej stali Fe-28Mn-9Al-1C ujawniły modulowaną strukturę i refleksy od nadstruktury, co było efektem rozpadu spinodalnego, który miał miejsce podczas procesu starzenia. Występowanie satelitów na zapisach dyfrakcyjnych sugeruje, że węgliki (Fe, Mn)3AlCx powstały w osnowie austenitycznej na skutek rozpadu spinodalnego zachodzącego podczas chłodzenia czy fluktuacji chemicznych występujących pomiędzy węglikami Fe, Mn)3AlCx i osnową austenityczną.
    Źródło:
    Archives of Metallurgy and Materials; 2014, 59, 3; 971-975
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Carbides Analysis of the High Strength and Low Density Fe-Mn-Al-Si Steel
    Autorzy:
    Sozańska-Jędrasik, L.
    Mazurkiewicz, J.
    Borek, W.
    Matus, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/351736.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    high manganese steels
    triplex
    microstructure
    isolates of carbide
    carbides κ
    M7C3
    EBSD
    Opis:
    The work presents the results of investigations into the structure and phase composition of newly developed high manganese steels of the X98MnAlSiNbTi24-11 and X105MnAlSi24-11 type. The average density of such steels is 6.67 g/cm3, which is 15% lower as compared to typical structural steels. An analysis of phase composition and structure allows to conclude that the investigated steels feature an austenitic γ-Fe(Mn,Al,C) structure with uniformly distributed and elongated α-Fe(Mn,Al) ferrite grains on the boundaries of austenite grains and carbides. Examinations by diffraction of back scattered electrons (EBSD) allow to conclude that high-angle boundaries dominate in such steels, having significant influence on mechanical properties. Three types of carbides with differentiated chemical composition and size were identified in steel X98MnAlSiNbTi24-11 with scanning and transmission electron microscopy. κ-(Fe,Mn)3AlC carbides, having a regular, face-centered cubic lattice (fcc), were identified in austenite. Transmission electron microscopy examinations have enabled to identify M7C3-type carbide in ferrite. Nb- and Ti-based complex carbides were identified in steel X98MnAlSiNbTi24-11, both, in ferrite and austenite. (NbTi)C2 carbide precipitates were confirmed in an X-ray qualitative phase analysis. The size of the above-mentioned carbides is within several to several dozens of μm. An X-ray qualitative phase analysis has confirmed the precipitates of M7C3 carbides in both steels.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 1; 265-276
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and High Temperature Oxidation Properties of Fe-Cr-Ni HK30 Alloy Manufactured by Metal Injection Molding
    Autorzy:
    Wi, Dong-Yeol
    Kim, Young-Kyun
    Yoon, Tae-Sik
    Lee, Kee-Ahn
    Powiązania:
    https://bibliotekanauki.pl/articles/356708.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    metal injection molding
    HK30
    microstructure
    high temperature oxidation
    Opis:
    This study investigated the microstructure and high temperature oxidation properties of Fe-25Cr-20Ni-1.5Nb, HK30 alloy manufactured by metal injection molding (MIM) process. The powder used in MIM had a bi-modal size distribution of 0.11 and 9.19 μm and had a spherical shape. The initial powder consisted of γ-Fe and Cr23C6 phases. Microstructural observation of the manufactured (MIMed) HK30 alloy confirmed Cr23C6 along the grain boundary of the γ-Fe matrix, and NbC was distributed evenly on the grain boundary and in the grain. After a 24-hour high temperature oxidation test at air atmospheres of 1000, 1100 and 1200°C, the oxidation weight measured 0.72, 1.11 and 2.29 mg/cm2, respectively. Cross-sectional observation of the oxidation specimen identified a dense Cr2O3 oxide layer at 1000°C condition, and the thickness of the oxide layer increased as the oxidation temperature increased. At 1100°C and 1200°C oxidation temperatures, Fe-rich oxide was also formed on the dense Cr2O3 oxide layer. Based on the above findings, this study identified the high-temperature oxidation mechanism of HK30 alloy manufactured by MIM.
    Źródło:
    Archives of Metallurgy and Materials; 2019, 64, 2; 525-530
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Forming of the microstructure in Fe-C-V alloys
    Kształtowanie mikrostruktury stopów Fe-C-V
    Autorzy:
    Kawalec, M.
    Fraś, E.
    Powiązania:
    https://bibliotekanauki.pl/articles/264061.pdf
    Data publikacji:
    2011
    Wydawca:
    Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
    Tematy:
    stopy Fe-C-V
    eutektyka
    żeliwo wysokowanadowe
    mikrostruktura
    Fe-C-V alloys
    eutectic
    high-vanadium cast iron
    microstructure
    Opis:
    The study presents the results of microstructural examinations of the volume solidifying Fe-C-V alloys containing carbon in the range of 1.45-2.23% and vanadium in the range of 7.33-15.08%. Attention was focussed on near-eutectic alloys. The Fe-C-V eutectic crystallising in these alloys is composed of ferrite and vanadium carbides of VC1-x type, and as such is included in the group of fibrous eutectics. During research, the experimental eutectic lines were plotted for Fe-C-V alloys, and a formula enabling calculation of the eutectic saturation ratio of these alloys was proposed.
    W pracy przedstawiono wyniki badań mikrostruktury stopów Fe-C-V, o zawartości węgla w zakresie 1,45-2,23% i wanadu w zakresie 7,33-15,08%, krystalizujących w sposób objętościowy, przy czym szczególną uwagę zwrócono na stopy okołoeutektyczne. Krystalizująca w stopach Fe-C-V eutektyka składa się z ferrytu i węglików wanadu typu VC1-x i jest zaliczana do grupy eutektyk włóknistych. W pracy określono eksperymentalnie przebieg linii eutektycznej dla stopów Fe-C-V oraz wyznaczono zależność na stopień nasycenia eutektycznego dla tych stopów.
    Źródło:
    Metallurgy and Foundry Engineering; 2011, 37, 1; 17-24
    1230-2325
    2300-8377
    Pojawia się w:
    Metallurgy and Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Crystallization of Eutectics in Fe-C-V-Si Alloys
    Autorzy:
    Kawalec, M
    Powiązania:
    https://bibliotekanauki.pl/articles/381286.pdf
    Data publikacji:
    2014
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    theory of crystallization
    Fe-C-V-Si alloys
    high-vanadium cast iron
    microstructure
    eutectic grain
    teoria krystalizacji
    stopy Fe-C-V-Si
    żeliwo wysokowanadowe
    mikrostruktura
    eutektyka
    Opis:
    This article addresses the results of microstructural examinations of the volume solidifying Fe–C–V–Si alloys containing carbon in the range of 1.39÷1.76%, vanadium in the range of 6.77÷7.77% and silicon in the range of 0.02÷3.10. The melting charge was Armco iron, ferro-vanadium with 81.7 wt.%V, spectrally pure graphite and technically pure silica. It was shown that with increasing the silicon content, the microstructure of the resulting alloy changing. These changes include both a matrix the shape of the primary carbides and type of crystallizing eutectic. In the studied alloys was observed following eutectic: fibrous (crystallize as non-faceted/ non-faceted eutectic), complex regular (crystallize as faceted/ non-faceted eutectic), spiral (crystallize as faceted/ faceted eutectic). The results illustrated by the images of the microstructures made with an optical microscope and a scanning electron microscope.
    Źródło:
    Archives of Foundry Engineering; 2014, 14, 1 spec.; 143-146
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and Chemical Composition of Fe-Cr Alloy Tempered in High Temperature and Atmosphere Containing Ar-SO2
    Autorzy:
    Radziszewska, A.
    Kranzmann, A.
    Dörfel, I.
    Mosquera Feijoo, M.
    Solecka, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/354072.pdf
    Data publikacji:
    2016
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    microstructure
    high-temperature corrosion
    X20Cr13 steel
    Opis:
    The paper presents the microstructure, chemical and phase composition of thin scale, obtained as a result of high-temperature corrosion of X20Cr13 stainless steel. Samples were exposed to gas atmosphere of the following composition: 0.25 vol.% of SO2 and 99.75 vol.% of Ar at 600 °C for 5 h. As a consequence, thin compact scale was formed on steel surface. This scale consisted of three different zones. An amorphous zone was formed close to steel surface. Then, nanocrystalline zone could be observed. Finally, larger grains were formed during the corrosion process. The analysis of the chemical composition revealed higher concentration of chromium near steel surface. In contrast, to chromium, the content of iron, increased near the scale surface. It was found out that the (Cr, Mn, Fe)5O12 phase appeared in the thin scale.
    Źródło:
    Archives of Metallurgy and Materials; 2016, 61, 3; 1607-1612
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Maximum Piston Velocity on Internal Homogeneity of AlSi9Cu3(Fe) Alloy Processed by High-Pressure Die Casting
    Autorzy:
    Matejka, Marek
    Bolibruchowá, Dana
    Podprocká, R.
    Powiązania:
    https://bibliotekanauki.pl/articles/2203939.pdf
    Data publikacji:
    2022
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Si-Cu alloy
    high-pressure die casting
    porosity
    Brinell hardness
    microstructure
    stop Al-Si-Cu
    odlewanie wysokociśnieniowe
    porowatość
    twardość Brinella
    mikrostruktura
    Opis:
    High-pressure die casting results in a high quality surface and good mechanical properties of castings. Under the effect of pressure, integral and solid castings are achieved without a large number of foundry defects. The correct and proper setting of technological parameters plays a very important role in minimizing casting defects. The aim of the presented article is to determine the optimum maximum piston velocity for a casting in the high-pressure casting process with two height variants, depending on their internal quality. It is because the internal quality of particular castings is important in terms of proper functionality in operations where the biggest problem is the porosity of the casting. The main cause of porosity formation is the decreasing solubility of gases (most often hydrogen) during the melt solidification. Solubility represents the maximum amount of gas that can dissolve in a metal under equilibrium conditions of temperature and pressure. Macroporosity and microporosity were determined from the sections of the surfaces in the determined zones of the castings. Here, the results was that the macroporosity decreased with increasing piston velocity. Ideal microstructure was evaluated at a piston velocity of 3 m/s for both types of castings. On the other hand, the increase in tube size has shown that velocities of 3 m/s and higher, the tube is more prone to macroporosity formation. The highest hardness was achieved at the piston velocity of 2 m/s at both tube lengths.
    Źródło:
    Archives of Foundry Engineering; 2022, 22, 4; 34--40
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of High-Strength Gray Cast Iron Using Permanent Magnet Scrap
    Autorzy:
    Park, S.-Y.
    Kim, J. H.
    Seo, S. J.
    On, J. S.
    Lim, K. M.
    Powiązania:
    https://bibliotekanauki.pl/articles/352204.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    gray cast iron
    rare earth element
    Nd-Fe-B magnet scrap
    graphite formation
    microstructure
    Opis:
    In this study, we have developed the manufacturing technology for high strength gray cast irons by using the spent permanent magnet scraps. The cast specimen inoculated by using a spent magnet scraps showed the excellent tensile strength up to 306MPa. This tensile strength value is 50MPa higher than that of the specimen cast without inoculation, and is similar to that of the specimen inoculated by using the expensive misch-metal. These superior mechanical properties are attributed to complex sulfides created during solidification that promote the formation and growth of Type-A graphite. It is therefore concluded that spent magnets scrap can provide an efficient and cost-effective inoculation agent for the fabrication of high-performance gray cast iron.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1113-1117
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
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