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Tytuł:
Studies into new, environmentally friendly Ag-Cu-Zn-Sn brazing alloys of low silver content
Badania nowych, ekologicznych spoiw twardych Ag-Cu-Zn-Sn o niskiej zawartości srebra
Autorzy:
Wierzbicki, L. J.
Malec, W.
Stobrawa, J.
Cwolek, B.
Juszczyk, B.
Powiązania:
https://bibliotekanauki.pl/articles/354086.pdf
Data publikacji:
2011
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
kadm
srebro
spoiwa ekologiczne
stopy lutownicze
właściwości mechaniczne
mikrostruktura
skład fazowy
cadmium
silver
environmentally friendly alloys
brazing alloys
mechanical properties
microstructure
phase composition
Opis:
The paper present selected results of the research conducted for elimination of toxic cadmium from silver based brazing alloys of Ag-Cu-Zn-Cd type. The investigations were conducted with nine new alloys of constant, low silver content (25%) and diversified copper (38.8-46%), zinc (19-32%) and tin (3-10%) contents. Tin was selected as potentially the best cadmium substitute basing on literature review and analysis of equilibrium systems. For examinations and tests a series of ingots in laboratory scale was manufactured, as well as some ingots in pilot scale for the selected, most promising alloys. Complex metallographic examinations of the brazing alloys samples produced in various conditions were made as well as analyses of their phase composition. Also mechanical properties of the samples both in ambient and in elevated temperatures were examined, and physical and technological properties and usability of the alloys were determined. The last stage of the study covered laboratory trials of brazing using the selected alloys. Basing on the results it can be said that there is a possibility to substitute selected cadmium containing silver-based alloys with environmentally friendly alloys of Ag-Cu-Zn-Sn type of relatively low silver content. Low range of melting point was reached, as preliminary assumed. Mechanical properties of the studied alloys strongly depend on temperature, and present limited plasticity in room temperature, while at high temperature (over 500°C) present superplasticity. The examined alloys show good spreadability and the brazing tests confirmed their good reactions both with copper and brass base in a wide temperature range.
W niniejszym artykule przedstawiono wybrane wyniki prac, których celem jest wyeliminowanie toksycznego kadmu ze srebrowych spoiw twardych typu Ag-Cu-Zn-Cd. Badaniami objęto 9 nowych gatunków stopów o stałej, niskiej zawartości srebra (25%) oraz zróżnicowanej zawartości miedzi (38,8-46%), cynku (19-32%) oraz cyny (3-10%). Cyna została wytypowana, na podstawie analizy literaturowej oraz układów równowagowych, jako potencjalnie najlepszy zamiennik kadmu. Wytworzono szereg wlewków w skali laboratoryjnej oraz dla wybranych, najbardziej obiecujących gatunków spoiw, wlewki w skali półtechnicznej przeznaczone do badań i prób. Przeprowadzono kompleksowe badania metalograficzne próbek spoiw wytworzonych w róznych warunkach oraz dokonano analizy skżadu fazowego. Wykonano także badania wżaściwości mechanicznych próbek zarówno w temperaturze otoczenia jak i podwyższonej oraz badania właściwości fizycznych, technologicznych i użytkowych. W ostatnim etapie pracy przeprowadzono laboratoryjne próby lutowanie przy zastosowaniu wybranych spoiw. Uzyskane wyniki badań pozwalają stwierdzić, że możliwe jest zastąpienie wybranych gatunków spoiw srebrowych kadmowych stopami ekologicznymi z grupy Ag-Cu-Zn-Sn o stosunkowo niskiej zawartości srebra. Uzyskano, zakładany we wstępnym etapie prac, niski zakres temperatury topnienia. Właściwości mechaniczne badanych stopów silnie zależą od temperatury, charakteryzują się one ograniczoną plastycznościa w temperaturze pokojowej, by w wysokiej temperaturze (ponad 500°C) wykazywać cechy nadplastyczne. Badane spoiwa charakteryzują się dobrą rozpływnością, a próby lutowania wykazały, że dobrze reagują zarówno z podłożem miedzianym jak i mosiężnych w szerokim zakresie temperatury.
Źródło:
Archives of Metallurgy and Materials; 2011, 56, 1; 147-158
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Damage resistance and microstructure of barley kernels
Autorzy:
Fornal, J.
Sadowska, J.
Ornowski, A.
Jelinski, T.
Velikanov, L.
Powiązania:
https://bibliotekanauki.pl/articles/24723.pdf
Data publikacji:
2000
Wydawca:
Polska Akademia Nauk. Instytut Agrofizyki PAN
Tematy:
microstructure
damage susceptibility
barley
Polish cultivar
endosperm
cell wall
mechanical property
Źródło:
International Agrophysics; 2000, 14, 2
0236-8722
Pojawia się w:
International Agrophysics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure of Archaeological 17th Century Cast Copper Alloys
Autorzy:
Konieczny, J.
Labisz, K.
Głowik-Łazarczyk, K.
Ćwiek, J.
Wierzbicki, Ł.
Powiązania:
https://bibliotekanauki.pl/articles/382152.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metallography
archaeometallurgy
microstructure
excavations
phase analysis
metalografia
archaeometalurgia
mikrostruktura
wykopaliska
Opis:
In Poland, researchers have a very strong interest in archaeometallurgy, which, as presented in classical works, focuses on dating artefacts from the prehistoric and early medieval periods in the form of cast iron and copper castings. This study, extending the current knowledge, presents the results of a microstructure investigation into the findings from the Modern era dating back to the late Middle Ages. The investigated material was an object in the form of a heavy solid copper block weighing several kilograms that was excavated by a team of Polish archaeologists working under the direction of Ms Iwona Młodkowska-Przepiórowska during works on the marketplace in the city of Czestochowa during the summer of 2009. Pre-dating of the material indicates the period of the seventeenth century AD. The solid copper block was delivered in the form of a part shaped like a bell, named later in this work as a “kettlebell”. To determine the microstructure, the structural components, chemical composition, and homogeneity, as well as additives and impurities, investigations were carried out using light microscopy, scanning electron microscopy including analysis of the chemical composition performed in micro-areas, and qualitative X-ray phase analysis in order to investigate the phase composition. Interpretation of the analytical results of the material’s microstructure will also help modify and/or develop new methodological assumptions to investigate further archaeometallurgical exhibits, throwing new light on and expanding the area of knowledge of the use and processing of seventeenth-century metallic materials.
Źródło:
Archives of Foundry Engineering; 2017, 17, 2; 190-196
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Micro- and nanopatterned surfaces for guided adhesion, growth and phenotypic maturation of cells
Autorzy:
Bacakova, L.
Filova, E.
Grausova, L.
Vandrovcova, M.
Parizek, M.
Novotna, K.
Svorcik, V.
Vacik, J.
Rypacek, F.
Kromka, A.
Heitz, J.
Shard, A.
Powiązania:
https://bibliotekanauki.pl/articles/284586.pdf
Data publikacji:
2009
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
surface patterning
microstructure
nanostructure
biofunctionalization
endothelial cells
vascular smooth muscle cells
bone cells
Opis:
Micropatterned surfaces were created by UV light-irradiation of polytetrafluoroethylene through a metallic mask, by successive plasma polymerization of acrylic acid and 1,7-octadiene, or by creation of prominences and grooves by deposition of fullerenes C60 through a metallic mask. All these surface types were capable of inducing regionally-selective adhesion, proliferation and phenotypic maturation of vascular endothelial cells, vascular smooth muscle cells or human bone-derived MG 63 cells. Nanopatterned surfaces created by tethering GRGDSG oligopeptides through polyethylene oxide chains on a polymeric surface promoted spreading, formation of focal adhesion plaques and DNA synthesis in vascular smooth muscle cells. Surfaces nanopatterned with nanocrystalline diamond gave good support for the adhesion, growth and metabolic activity of osteoblast-like MG 63 cells.
Źródło:
Engineering of Biomaterials; 2009, 12, no. 89-91; 18-21
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of primary silicon precipitates on anodized aluminum alloys surface layer properties
Autorzy:
Labisz, K.
Konieczny, J.
Wierzbicki, Ł.
Ćwiek, J.
Butor, A.
Powiązania:
https://bibliotekanauki.pl/articles/374771.pdf
Data publikacji:
2018
Wydawca:
Politechnika Śląska. Wydawnictwo Politechniki Śląskiej
Tematy:
anodization
aluminium alloys
microstructure
surface layer
wear resistance
anodowanie
stopy aluminium
mikrostruktura
warstwa wierzchnia
odporność na zużycie
Opis:
In this work, we presented the influence of the anodizing method and parameters, as well as the chemical composition of the used aluminium alloys on the properties and microstructure of the anodic layer produced on aluminium alloys, in particular on the size and morphology of the primary silicon precipitates and the homogeneity of the resulting oxide coating. Aluminium alloys AlSi8 and AlSi12, produced using the die-casting method and subsequently subjected to anodic oxidation were used as test material. The microstructure of the obtained surface layer was analyzed by taking into account the primary silicon precipitates. The results of the hardness and abrasive wear test also show the influence of anodizing and electrolyte parameters on the structure and properties of the tested aluminium alloys.
Źródło:
Transport Problems; 2018, 13, 2; 111-120
1896-0596
2300-861X
Pojawia się w:
Transport Problems
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation of faba bean (Vicia faba L.minor) products. Part IV. Effect of hydrothermaltreatment of faba bean on the quality of flour
Otrzymywanie produktów z bobiku (Vicia faba L.minor). Cz. IV Wpływ obróbki hydrotermicznej bobiku na jakość mąki
Autorzy:
Kozłowska, H.
Borowska, J.
Fornal, J.
Schneider, C.
Schmandke, H.
Powiązania:
https://bibliotekanauki.pl/articles/1399389.pdf
Data publikacji:
1989
Wydawca:
Instytut Rozrodu Zwierząt i Badań Żywności Polskiej Akademii Nauk w Olsztynie
Tematy:
faba bean
proteins
trypsin inhibitor activity
microstructure
organoleptic quality of flour
Opis:
The most advantageous parameters of hydrothermal treatment of faba cotyledons were determined. These are: steaming temperature 110°C and tiMc 2 min. and they caused - at relatively smay decrease of protein solubility and slight damage of cotyledons structure (SEM)-a cansiderable lowering of trypsin inhibitors activity and an improvement of organoleptic quality of flour obtained from thus prepared cotyledons.
Dążąc do poprawy jakości preparatów białkowych otrzymywanych z nasion roślin strączkowych liścienie nasion bobiku odmiany Fribo poddano obróbce hydrotechnicznej w temp.100, 110, i 120°C oraz czasie od 1 do 20 min w urządzeniu fluidyzacyjnym. Zastosowana obróbka hydrotermiczna zdecydowanie poprawiła jakość mąki bobikowej. Ustalono wyraźne obniżenie aktywności inhibitorów trypsyny oraz poprawę cech organoleptycznych, przede wszystkim smaku. Obniżenie się aktywności inhibitorów trypsyny, podobnie jak rozpuszczalności azotu było uzależnione od zastosowanej temperatury oraz czasu jej oddziaływania. Zaznaczył się wyraźniej wpływ temperatury, aniżeli czasu na badane wyróżniki jakościowe. Na przykład inaktywację inhibitorów trypsyny do aktywności śladowej uzyskano poddając liścienie ogrzewaniu w temp. 110°C przez 10 min, natomiast ogrzewanie w temp. 100°C przez 20 min spowodowało spadek aktywności o 64%. Wyniki analiz chemicznych znalazły potwierdzenie w obserwacji zmian struktury komórkowej liścieni w skaningowym mikroskopie elektronowym. Spadkowi rozpuszczalności towarzyszyły zmiany ciał białkowych i skrobi widoczne w mikroskopie. Nasilały się one w miarę podwyższania temperatury, bądź też wydłużania czasu jej oddziaływania. Na podstawie uzyskanych wyników ustalono, że temp. 110°C oddziałująca na badany materiał przez 2 min powodowała stosunkowo niewielkie zmiany denaturacyjne białka oraz istotne obniżenie aktywności inhibitorów trypsyny. Mąka otrzymana przy zastosowaniu wymienionych parametrów obróbki hydrotermicznej pozbawiona była całkowicie grochowego smaku i zapachu, co rokuje możliwości jej wszechstronnego zastosowania w żywności.
Źródło:
Acta Alimentaria Polonica; 1989, 15(39), 2; 161-169
0137-1495
Pojawia się w:
Acta Alimentaria Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Numerical analysis of soil settlement prediction and its application in large-scale marine reclamation artificial island project
Autorzy:
Zhao, J.
Bao, L.
Wang, G.
Powiązania:
https://bibliotekanauki.pl/articles/259183.pdf
Data publikacji:
2017
Wydawca:
Politechnika Gdańska. Wydział Inżynierii Mechanicznej i Okrętownictwa
Tematy:
microstructure
consolidation
creep
artificial island
settlement
Opis:
In an artificial island construction project based on the large-scale marine reclamation land, the soil settlement is a key to affect the late safe operation of the whole field. To analyze the factors of the soil settlement in a marine reclamation project, the SEM method in the soil micro-structural analysis method is used to test and study six soil samples such as the representative silt, mucky silty clay, silty clay and clay in the area. The structural characteristics that affect the soil settlement are obtained by observing the SEM charts at different depths. By combining numerical calculation method of Terzaghi’s one-dimensional and Biot’s two-dimensional consolidation theory, the one-dimensional and two-dimensional creep models are established and the numerical calculation results of two consolidation theories are compared in order to predict the maximum settlement of the soils 100 years after completion. The analysis results indicate that the micro-structural characteristics are the essential factor to affect the settlement in this area. Based on numerical analysis of one-dimensional and two-dimensional settlement, the settlement law and trend obtained by two numerical analysis method is similar. The analysis of this paper can provide reference and guidance to the project related to the marine reclamation land.
Źródło:
Polish Maritime Research; 2017, S 3; 4-11
1233-2585
Pojawia się w:
Polish Maritime Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Image based analysis of complex microstructures of engineering materials
Autorzy:
Wejrzanowski, T.
Spychalski, W. L.
Różniatowski, K.
Kurzydłowski, K. J.
Powiązania:
https://bibliotekanauki.pl/articles/908046.pdf
Data publikacji:
2008
Wydawca:
Uniwersytet Zielonogórski. Oficyna Wydawnicza
Tematy:
analiza obrazu
opis ilościowy
mikrostruktura
image analysis
quantitative description
microstructure
Opis:
The paper presents various methods for quantitative description of material structures. The main focus is on direct methods of description based on image analysis. In particular, techniques for the estimation of the size, shape and spatial distribution of structural elements observed by different microscopic techniques are described. The application of these methods for the characterization of the structures of engineering materials is demonstrated on a stainless steel used in petrochemical installations. It is shown that the methods applied are useful for the assessment of service degradation of materials.
Źródło:
International Journal of Applied Mathematics and Computer Science; 2008, 18, 1; 33-39
1641-876X
2083-8492
Pojawia się w:
International Journal of Applied Mathematics and Computer Science
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Contribution of titanium, chromium and carbon buffer interlayers to bio-tribological properties of multilayer composites
Autorzy:
Major, Ł.
Janusz, M.
Lackner, J. M.
Major, B.
Powiązania:
https://bibliotekanauki.pl/articles/352343.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
bio-tribological coatings
wear mechanism
microstructure
Opis:
Research studies on bio-tribological protective coatings of titanium, chromium and carbon based have been performed. Thin films were fabricated by hybrid PLD technique (PLD supported by magnetron sputtering). Coatings consisted of two parts; the inner part (first from the substrate) in each case was formed by titanium or chromium/titanium nitride or chromium nitride (Ti/TiN or Cr/Cr2N). The outer part was formed by pure DLC or multilayer DLC'Ti or Cr. No delamination was found at the interface. Titanium or chromium metallic layer was deposited as a first layer directly on the metallic substrate to avoid delamination. All individual layers were built of columnar nano- crystallites. Mechanisms of the mechanical wear of analyzed systems were presented, focusing on the cracking propagation in ball-on-disc tests using an 1 N and 5 N applied loads for 5 000 cycles. Complex microstmcture analysis of presented nano-multilayer coatings, before and after mechanical tests, were performed by means of transmission electron microscopy (TEM). The highest stress concentration during mechanical uploading was moved through the multilayer coating by breaking only one layer at the time. The microstructure characterization revealed that cracking propagating in the outer part of the coating was stopped at the interface. In the case of the inner part of the coating Ti/TiN; Cr/Cr2N, ceramic layers showed brittle cracking, while metallic (Ti or Cr) ones deformed plastically. Fabricated coatings were subjected under the analysis in the biomechanical system optimized to test for the direct contact with a human whole blood. The study considered physiological conditions mainly related to the temperature and humidity and the frequency of cyclic deformation of the artificial vessel into which the tested sample was introduced.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 3; 1391-1398
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Material investigations of composites and their selected applications in motor transport
Autorzy:
Rudnik, D.
Pietrzak, K.
Wojciechowski, A.
Sobczak, J.
Kowalewski, Z. L.
Powiązania:
https://bibliotekanauki.pl/articles/243917.pdf
Data publikacji:
2008
Wydawca:
Instytut Techniczny Wojsk Lotniczych
Tematy:
metal matrix composites
microstructure
properties
applications
Opis:
The paper presents advances in the range of brake discs and engine pistons production using metal matrix composites and identifies their advantages in comparison to materials traditionally applied. The wear characteristics in the case of brake discs and thermal shock resistance in the case of pistons were determined. The wear was assessed by measurements of friction coefficients in different temperatures. The thermal shock resistance was described as the crack length formed during the tests. The image analysis was used in the quantitative microstructure assessments for determination of synthetic geometrical parameter correlated with composites properties. The two synthetic geometrical variables have been proposed in the microstructure description of a new generation brake discs and pistons. The selected relationships between functional properties and composite microstructure are presented. It was shown that a life of brake discs made from A359 aluminum alloy reinforced by SiC precipitates is much longer in comparison to traditional, made from cast iron. It was ascertained also that the best thermal shock resistance was obtained in the case of AK12 composite with Al2O3 short fibers in cast heat treated. The results may be treated as the base for the recommendations of tested metal matrix composites for applicability in selected vehicle parts and subsets producing.
Źródło:
Journal of KONES; 2008, 15, 2; 399-407
1231-4005
2354-0133
Pojawia się w:
Journal of KONES
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Role of Microstructure in High Temperature Tribology of Iron Alloys
Autorzy:
Krawczyk, J.
Rożniata, E.
Zimowski, S.
Kot, M.
Dąbrowski, R.
Dziurka, R.
Frocisz, Ł.
Powiązania:
https://bibliotekanauki.pl/articles/355366.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
microstructure
tribology
iron alloys
cast steel
wear
cementite
Opis:
The present paper describe the issue of tool materials wear in a high temperature conditions. The investigations were performed at the cast steel tool material at the tribological contact to the structural steel. The investigations aim was to determine the role of microstructure in a tribological properties between the structural steel and tool material. The results of such investigation could be referenced to the industry conditions and could answer about the problems of tool materials wear. The observations of the wear mechanisms were referred to the microstructure of the mill rolls. The laboratory tests ware aimed at evaluating the thermal treatment modification effect on the cast steels properties. A significant role of the morphology of ledeburitic cementite and secondary cementite on the tribological properties was exhibited. The investigations assumed the presence of an austenitic matrix with primary and secondary cementite. Influence of varying morphology carbides was described. in the cast steel microstructure. The investigation results make possible to point to a direction of carbide morphology change with the purpose of obtaining the assumed properties of hot operation tools.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 915-920
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Numerical mesoscopic analysis of fracture in fine-grained concrete
Autorzy:
Skarżyński, Ł.
Tejchman, J.
Powiązania:
https://bibliotekanauki.pl/articles/230197.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
kruszywo
beton
metoda elementów skończonych
strefa przejściowa międzyfazowa
mikrostruktura
aggregate
concrete
finite element method
interfacial transition zone
microstructure
Opis:
This paper presents numerical two-dimensional results for fine-grained concrete under quasi-static three-point bending at meso-scale. Concrete was modelled as a random heterogeneous three-phase material. The simulations for notched concrete beams were carried out with the standard finite element method using an isotropic damage constitutive model enhanced by a characteristic length of micro-structure by means of a non-local theory. The effect of the volume fraction, shape, size, statistical distribution and stiffness of aggregate was analysed. Moreover, the effect of the bond thickness, notch size and characteristic length of micro-structure on the material behaviour was numerically investigated. The FE results were compared with own laboratory test results and other meso-scale calculations for three-phase concrete elements.
Źródło:
Archives of Civil Engineering; 2012, 58, 3; 331-361
1230-2945
Pojawia się w:
Archives of Civil Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Contribution of TiN/Ti/a-C:H multilayers architecture to biological and mechanical properties
Autorzy:
Major, L.
Lackner, J. M.
Kot, M.
Janusz, M.
Major, B.
Powiązania:
https://bibliotekanauki.pl/articles/200944.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
microstructure
smooth muscle cells adhesion
cracking
Opis:
Complex microstructure analysis of TiN/Ti/a-C:H multilayer coatings, subjected to mechanical and biological tests, were performed by means of transmission electron microscopy (TEM) and confocal scanning laser microscopy (CSLM), respectively. Influence of interface numbers and phase ratios on coating properties was studied. Thin films were fabricated by a hybrid PLD technique (PLD supported by magnetron sputtering). The a-C:H phase was characterized by an amorphous structure, while TiN was built of columnar crystallites. Multilayer coatings contained sequentially deposited TiN and a-C:H layers with thin metallic Ti inter- layers deposited at each interface. Mechanisms of mechanical wear of analyzed systems were presented focusing on the cracking propagation revealed in the scratch test. Biological tests were done basing on smooth muscle cells adhesion to coating surfaces. An increase of TiN phase in the coating led to improvement of mechanical properties, while the carbon phase improved the biological behavior. Coatings comprising a higher rate of the carbon (a-C:H) revealed brittleness and were prone to delaminating. Optimal properties from the mechanical and biological point of view were stated for 8xTiN/Ti/a-C:H coating with 1:1 phase ratio (TiN to a-C:H).
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2014, 62, 3; 565-570
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and mechanical properties of Mg-2.5%Tb-0.78%Sm alloy after ECAP and ageing
Mikrostruktura i właściwości mechaniczne stopu Mg-2.5%Tb-0.78%Sm po procesie ECAP i starzeniu
Autorzy:
Bryła, K.
Dutkiewicz, J.
Rokhlin, L. L.
Lityńska-Dobrzyńska, L.
Mroczka, K.
Kurtyka, P.
Powiązania:
https://bibliotekanauki.pl/articles/351672.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
magnesium alloys with rare earth metals
ECAP
microstructure
ageing
mechanical properties
stopy magnezu z metalami ziem rzadkich
mikrostruktura
starzenie
właściwości mechaniczne
Opis:
The influence of ageing and Equal Channel Angular Pressing (ECAP) on the microstructure and mechanical properties of Mg-2.5%Tb-0.78%Sm alloy has been examined. The microhardness changes during ageing at 200ºC show a slight increase. The aged microstructure at maximum hardness contains Mg12(Tb,Sm) - metastable β’ phase of size about 2-10 nm as dispersed precipitates. The orientation relationship between β’ phase and the matrix was found as follows: (0001) Mg || (110) β′, [2110] Mg || [116] β′. The ECAP passes were performed by two procedures: “I” - four passes at 350ºC; “II” - one pass at 370ºC, second pass at 340ºC and third pass at 310ºC. The grain size was reduced about 200 times as a results of ECAP process according “I” and “II” procedure. The grain refinement by ECAP improves significantly the compression yield strength and hardness. The Hall-Petch relationship was confirmed basing on microhardness measurements and the grain size after ECAP. The Mg 24 (Tb,Sm) 5 and Mg 41 (Sm,Tb) 5 particles smaller than 150 nm are located mainly at grain and subgrain boundaries and they prevent grain growth during ECAP processing. The microstructure evolution during ECAP can be described as dynamic recovery and continuous and discontinuous dynamic recrystallization.
W pracy przeprowadzono badania mikrostruktury i właściwosci mechanicznych stopu Mg-2,5%Tb-0,78%Sm po procesie starzenia oraz po odkształceniu plastycznym metoda ECAP. Starzenie stopu w temperaturze 200ºC powoduje niewielki wzrost mikrotwardości. Mikrostruktura stopu starzonego o maksymalnej wartości twardości zawiera metastabilne drobnodyspersyjne wydzielenia Mg12 (Tb,Sm) - β′ o wielkości 2-10 nm. Roztwór stały α-Mg wykazuje następujące zależności krystalograficzne z wydzielonymi cząstkami β′: (0001) Mg || (110) β′, [2110] Mg || [116] β′. Odkształcenie plastyczne metoda ECAP przeprowadzono stosując dwie procedury: „I” - cztery przejścia w 350ºC, „II” - pierwsze w 370ºC, drugie w 340ºC i trzecie przejście w 310ºC. Po procesie ECAP, dla obu procedur, nastąpiło dwustukrotne zmniejszenie wielkości ziarna. Zmniejszenie wielkości ziarna uzyskane metodą ECAP znaczaco poprawia twardość oraz granice plastycznosci przy ściskaniu. Stwierdzono zależność Halla-Petcha pomiędzy wartościami mikrotwardości oraz wielkości ziaren uzyskanymi w wyniku odkształcenia metodą ECAP. Cząstki Mg 24 (Tb,Sm) 5 i Mg 41 (Sm,Tb) 5 mniejsze niż 150 nm wydzielone na granicach ziaren i podziaren zapobiegaja ich wzrostowi podczas procesu ECAP. Zmiany mikrostruktury zachodzące podczas procesu ECAP można opisać procesami dynamicznego zdrowienia oraz dynamicznej rekrystalizacji.
Źródło:
Archives of Metallurgy and Materials; 2013, 58, 2; 481-487
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Carbides Analysis of the High Strength and Low Density Fe-Mn-Al-Si Steel
Autorzy:
Sozańska-Jędrasik, L.
Mazurkiewicz, J.
Borek, W.
Matus, K.
Powiązania:
https://bibliotekanauki.pl/articles/351736.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high manganese steels
triplex
microstructure
isolates of carbide
carbides κ
M7C3
EBSD
Opis:
The work presents the results of investigations into the structure and phase composition of newly developed high manganese steels of the X98MnAlSiNbTi24-11 and X105MnAlSi24-11 type. The average density of such steels is 6.67 g/cm3, which is 15% lower as compared to typical structural steels. An analysis of phase composition and structure allows to conclude that the investigated steels feature an austenitic γ-Fe(Mn,Al,C) structure with uniformly distributed and elongated α-Fe(Mn,Al) ferrite grains on the boundaries of austenite grains and carbides. Examinations by diffraction of back scattered electrons (EBSD) allow to conclude that high-angle boundaries dominate in such steels, having significant influence on mechanical properties. Three types of carbides with differentiated chemical composition and size were identified in steel X98MnAlSiNbTi24-11 with scanning and transmission electron microscopy. κ-(Fe,Mn)3AlC carbides, having a regular, face-centered cubic lattice (fcc), were identified in austenite. Transmission electron microscopy examinations have enabled to identify M7C3-type carbide in ferrite. Nb- and Ti-based complex carbides were identified in steel X98MnAlSiNbTi24-11, both, in ferrite and austenite. (NbTi)C2 carbide precipitates were confirmed in an X-ray qualitative phase analysis. The size of the above-mentioned carbides is within several to several dozens of μm. An X-ray qualitative phase analysis has confirmed the precipitates of M7C3 carbides in both steels.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 265-276
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł

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