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Wyświetlanie 1-15 z 47
Tytuł:
Omówienie norm ASTM stosowanych w badaniach mikrostruktury
Autorzy:
Hubner, K. J.
Powiązania:
https://bibliotekanauki.pl/articles/274225.pdf
Data publikacji:
2013
Wydawca:
Roble
Tematy:
normy ASTM
standardy międzynarodowe
badania mikrostruktury
mikrostruktura
ASTM norms
international standards
microstructure investigation
microstructure
Źródło:
LAB Laboratoria, Aparatura, Badania; 2013, 18, 1; 52-55
1427-5619
Pojawia się w:
LAB Laboratoria, Aparatura, Badania
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball Milling
Autorzy:
Lee, H.-E.
Kim, Y. S.
Park, J. K.
Oh, S.-T.
Powiązania:
https://bibliotekanauki.pl/articles/355552.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high energy ball milling
Ni-base ODS superalloy
particle and crystalline size
microstructure
Opis:
Microstructure evolution of Ni-based oxide dispersion-strengthened alloy powders with milling time is investigated. The elemental powders having a nominal composition of Ni-15Cr-4.5Al-4W-2.5Ti-2Mo-2Ta-0.15Zr-1.1Y2O3 in wt % were ball-milled by using horizontal rotary ball milling with the change of milling velocity. Microstructure observation revealed that large aggregates were formed in the early stages of ball milling, and further milling to 5 h decreased particle size. The average crystalline size, estimated by the peak broadening of XRD, decreased from 28 nm to 15 nm with increasing milling time from 1 h to 5 h. SEM and EPMA analysis showed that the main elements of Ni and Cr were homogeneously distributed inside the powders after ball milling of 5 h.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1253-1255
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Image based analysis of complex microstructures of engineering materials
Autorzy:
Wejrzanowski, T.
Spychalski, W. L.
Różniatowski, K.
Kurzydłowski, K. J.
Powiązania:
https://bibliotekanauki.pl/articles/908046.pdf
Data publikacji:
2008
Wydawca:
Uniwersytet Zielonogórski. Oficyna Wydawnicza
Tematy:
analiza obrazu
opis ilościowy
mikrostruktura
image analysis
quantitative description
microstructure
Opis:
The paper presents various methods for quantitative description of material structures. The main focus is on direct methods of description based on image analysis. In particular, techniques for the estimation of the size, shape and spatial distribution of structural elements observed by different microscopic techniques are described. The application of these methods for the characterization of the structures of engineering materials is demonstrated on a stainless steel used in petrochemical installations. It is shown that the methods applied are useful for the assessment of service degradation of materials.
Źródło:
International Journal of Applied Mathematics and Computer Science; 2008, 18, 1; 33-39
1641-876X
2083-8492
Pojawia się w:
International Journal of Applied Mathematics and Computer Science
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Development of Rapidly Solidified Magnesium – Copper Ribbons
Autorzy:
Pastuszak, M.
Cieślak, G.
Dobkowska, A.
Mizera, J.
Kurzydłowski, K. J.
Powiązania:
https://bibliotekanauki.pl/articles/958209.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
magnesium-based alloys
rapid solidification
microstructure
mechanical properties
corrosion properties
Opis:
The aim of the present work was to plan and carry out an experiment consisting of amorphization of industrial magnesium alloy WE 43 (Mg - 4 Y - 3 RE - 0.5 Zr) modified by the copper addition. Investigated alloy modified with 20% of copper was rapidly quenched with the use of melt spinning technique. The effects of cooling rate on the structure and properties of the obtained material were extensively analyzed. The structure and phase analysis of samples were examined using X-ray diffraction method (XRD) while the thermal stability of the samples was determined by differential scanning calorimetry (DSC). Microstructure observations were also conducted. The microhardness tests (HV0.02) and corrosion resistance tests were carried out to investigate the properties of the material. Corrosion resistance measurements were held using a typical three-electrode system. As the result of the research, the effect of cooling rate on microstructure and properties of investigated alloy was determined.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2B; 1083-1088
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Comparison of the Microstructure and Corrosion Resistance of Sand Cast Aluminum Alloys
Autorzy:
Dobkowska, A.
Adamczyk–Cieślak, B.
Mizera, J.
Kurzydłowski, K. J.
Kiełbus, A.
Powiązania:
https://bibliotekanauki.pl/articles/352870.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminium-silicon-magnesium alloys
microstructure
corrosion
Opis:
The influence of different types of precipitation on the corrosion behavior was investigated in three aluminum-siliconmagnesium alloys. The microstructures of the alloys were studied through optical (OM) and scanning electron microscopy (SEM). The structures consisted of an α-Al solid solution matrix, Si eutectic crystals, secondary phases AlFeSi and AlMgFeSi (Chinese script), as well as Mg2Si. The corrosion behavior was examined with the use of a potentiodynamic polarization test followed by a SEM surface analysis. The results indicate that all the analyzed samples were in the passive state and AlSi10Mg was less reactive in the corrosive environment.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 209-212
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Properties of Cu-Nb Wire Composites
Mikrostruktura i własności drutów kompozytowych Cu-Nb
Autorzy:
Głuchowski, W. J.
Rdzawski, Z.M.
Stobrawa, J. P.
Marszowski, K. J.
Powiązania:
https://bibliotekanauki.pl/articles/351916.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
fibrous composite
copper alloy
mechanical properties
electrical conductivity
microstructure
kompozyty włókniste
stop miedzi
właściwości mechaniczne
przewodnictwo elektryczne
mikrostruktura
Opis:
Nowadays, there is much activity all over the world in development of Cu-Nb composites for their potential use as conductors in high field magnets. This study was aimed at investigation of microstructure, mechanical and electrical properties of Cu-Nb composite wires. The investigated materials have been processed by vacuum furnace melting and casting, and then hot forging and cold drawing. Initial results of research into Cu-Nb composite material obtained using repeated iterative drawing of niobium wires compacted into copper tube, have been also presented in this article. The ultimate tensile strength versus cold deformation degree has been presented. These changes have been discussed in relation to microstructure evolution. It was assumed that repeated drawing of compacted wires is a promising method for fibrous composite production (more than 823,000 Nb fibres of nanometric diameter) characterized by high mechanical properties and electrical conductivity. Original SPD technique applied for Cu-Nb composite deformation result in initial microstructure refinement and improves effectiveness of wire production process.
Aktualnie obserwuje się na świecie intensywny rozwój kompozytów Cu-Nb stosowanych jako przewody nawojowe generatorów silnych pól magnetycznych. Badania miały na celu określenie mikrostruktury oraz właściwości mechanicznych i elektrycznych drutów kompozytowych Cu-Nb. Badane materiały wytworzono przez zastosowanie topienia i odlewania w piecu próżniowym, a następnie kucia na gorąco i ciągnienia. Zaprezentowano także wstępne wyniki badań wytwarzania kompozytu Cu-Nb na drodze iteracyjnego ciągnienia pakietu drutów niobowych w rurze miedzianej. Pokazano wyniki badań wytrzymałości na rozciąganie w zależności od stopnia odkształcenia, w powiązaniu ze zmianami mikrostruktury. Stwierdzono, że wielokrotne ciągnienie pakietu drutów jest obiecująca metoda wytwarzania kompozytów włóknistych (ponad 823000 włókien Nb o przekroju nanometrycznym) o wysokich właściwościach mechanicznych i konduktywności elektrycznej.
Źródło:
Archives of Metallurgy and Materials; 2014, 59, 1; 35-40
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure of Archaeological 17th Century Cast Copper Alloys
Autorzy:
Konieczny, J.
Labisz, K.
Głowik-Łazarczyk, K.
Ćwiek, J.
Wierzbicki, Ł.
Powiązania:
https://bibliotekanauki.pl/articles/382152.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metallography
archaeometallurgy
microstructure
excavations
phase analysis
metalografia
archaeometalurgia
mikrostruktura
wykopaliska
Opis:
In Poland, researchers have a very strong interest in archaeometallurgy, which, as presented in classical works, focuses on dating artefacts from the prehistoric and early medieval periods in the form of cast iron and copper castings. This study, extending the current knowledge, presents the results of a microstructure investigation into the findings from the Modern era dating back to the late Middle Ages. The investigated material was an object in the form of a heavy solid copper block weighing several kilograms that was excavated by a team of Polish archaeologists working under the direction of Ms Iwona Młodkowska-Przepiórowska during works on the marketplace in the city of Czestochowa during the summer of 2009. Pre-dating of the material indicates the period of the seventeenth century AD. The solid copper block was delivered in the form of a part shaped like a bell, named later in this work as a “kettlebell”. To determine the microstructure, the structural components, chemical composition, and homogeneity, as well as additives and impurities, investigations were carried out using light microscopy, scanning electron microscopy including analysis of the chemical composition performed in micro-areas, and qualitative X-ray phase analysis in order to investigate the phase composition. Interpretation of the analytical results of the material’s microstructure will also help modify and/or develop new methodological assumptions to investigate further archaeometallurgical exhibits, throwing new light on and expanding the area of knowledge of the use and processing of seventeenth-century metallic materials.
Źródło:
Archives of Foundry Engineering; 2017, 17, 2; 190-196
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Heat Treatment on the Microstructure and Tensile Deformation Behavior of Oxide Dispersion Strengthened Alloys Manufactured by Complex Milling Process
Autorzy:
Kim, Y.-K.
Kim, J.-H.
Gwon, J.-H.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/352535.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ball milling
oxide dispersion strengthening
microstructure
tensile deformation behavior
Opis:
This study attempted to manufacture an ODS alloy by combining multiple milling processes in mechanical alloying stage to achieve high strength and fracture elongation. The complex milling process of this study conducted planetary ball milling, cryogenic ball milling and drum ball milling in sequential order, and then the microstructure and tensile deformation behavior were investigated after additional heat treatment. The oxide particles distributed within the microstructure were fine oxide particles of 5~20 nm and coarse oxide particles of 100~200 nm, and the oxide particles were confirmed to be composed of Cr, Ti, Y and O. Results of tensile tests at room temperature measured yield strength, tensile strength and elongation as 1320 MPa, 2245 MPa and 4.2%, respectively, before heat treatment, and 1161 MPa, 2020 MPa and 5.5% after heat treatment. This results indicate that the ODS alloy of this study gained very high strengths compared to other known ODS alloys, allowing greater plastic zones.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1335-1340
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ordering of alfa-FeCo phase in the nanocrystalline Fe83-xCoxNb3B13Cu1 (x = 6, 25 or 41.5) alloy
Autorzy:
Zbroszczyk, J.
Młyńczyk, A.
Olszewski, J.
Ciurzyńska, W.
Wysłocki, B.
Perduta, K.
Lelątko, J.
Nabiałek, M.
Powiązania:
https://bibliotekanauki.pl/articles/148219.pdf
Data publikacji:
2007
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
nanocrystalline alloys
microstructure
ordering
Mössbauer spectroscopy
Opis:
The microstructure and ordering of alfa-FeCo phase of the nanocrystalline Fe83 xCoxNb3B13Cu1 (x = 6, 25 or 41.5) alloys were investigated. We have stated that á-FeCo phase is atomically ordered in the Fe83 xCoxNb3B13Cu1 (x = 25 or 41.5) samples crystallized by the heat treatment in a furnace. However, after flash annealing (by current or laser) that phase is disordered. Moreover, we have found that Co concentration in the crystalline alfa-FeCo phase strongly depends on Co content in the as-quenched ribbons. The annealing conditions influence also the grain diameter of the crystalline phase. In the nanocrystalline alloys obtained by a flash annealing of the amorphous ribbons finer grains are present.
Źródło:
Nukleonika; 2007, 52, supl. 1; 29-32
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of High-Strength Gray Cast Iron Using Permanent Magnet Scrap
Autorzy:
Park, S.-Y.
Kim, J. H.
Seo, S. J.
On, J. S.
Lim, K. M.
Powiązania:
https://bibliotekanauki.pl/articles/352204.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gray cast iron
rare earth element
Nd-Fe-B magnet scrap
graphite formation
microstructure
Opis:
In this study, we have developed the manufacturing technology for high strength gray cast irons by using the spent permanent magnet scraps. The cast specimen inoculated by using a spent magnet scraps showed the excellent tensile strength up to 306MPa. This tensile strength value is 50MPa higher than that of the specimen cast without inoculation, and is similar to that of the specimen inoculated by using the expensive misch-metal. These superior mechanical properties are attributed to complex sulfides created during solidification that promote the formation and growth of Type-A graphite. It is therefore concluded that spent magnets scrap can provide an efficient and cost-effective inoculation agent for the fabrication of high-performance gray cast iron.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1113-1117
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of primary silicon precipitates on anodized aluminum alloys surface layer properties
Autorzy:
Labisz, K.
Konieczny, J.
Wierzbicki, Ł.
Ćwiek, J.
Butor, A.
Powiązania:
https://bibliotekanauki.pl/articles/374771.pdf
Data publikacji:
2018
Wydawca:
Politechnika Śląska. Wydawnictwo Politechniki Śląskiej
Tematy:
anodization
aluminium alloys
microstructure
surface layer
wear resistance
anodowanie
stopy aluminium
mikrostruktura
warstwa wierzchnia
odporność na zużycie
Opis:
In this work, we presented the influence of the anodizing method and parameters, as well as the chemical composition of the used aluminium alloys on the properties and microstructure of the anodic layer produced on aluminium alloys, in particular on the size and morphology of the primary silicon precipitates and the homogeneity of the resulting oxide coating. Aluminium alloys AlSi8 and AlSi12, produced using the die-casting method and subsequently subjected to anodic oxidation were used as test material. The microstructure of the obtained surface layer was analyzed by taking into account the primary silicon precipitates. The results of the hardness and abrasive wear test also show the influence of anodizing and electrolyte parameters on the structure and properties of the tested aluminium alloys.
Źródło:
Transport Problems; 2018, 13, 2; 111-120
1896-0596
2300-861X
Pojawia się w:
Transport Problems
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Właściwości magnetyczne wybranych nanokompozytów
Magnetic properties of chosen nanocomposites
Autorzy:
Ślusarek, B.
Chwastek, K.
Szczygłowski, J.
Wilczyński, W.
Powiązania:
https://bibliotekanauki.pl/articles/159855.pdf
Data publikacji:
2012
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Elektrotechniki
Tematy:
nanokompozyty
właściwości magnetyczne
modelowanie
mikrostruktura
nanocomposities
magnetic properties
modelling
microstructure
Opis:
W pracy scharakteryzowano właściwości magnetyczne rdzeni z nowoczesnych nanokompozytów. Aproksymowano zależność energii traconej podczas cyklu przemagnesowania w funkcji częstotliwości. Energia związana z prądami wirowymi generowanymi w różnych skalach czasowo-przestrzennych została opisana za pomocą prawa potęgowego o ułamkowym wykładniku.
Magnetic properties of cores made of modern nanocomposites have been characterized in the paper. The dependence of energy dissipated per cycle as function of frequency has been approximated. Energy term related to eddy currents generated in different time-spatial scales has been described usin a power law with a fractional exponent.
Źródło:
Prace Instytutu Elektrotechniki; 2012, 258; 89-98
0032-6216
Pojawia się w:
Prace Instytutu Elektrotechniki
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and properties of tin bronzes produced by the SPD method
Autorzy:
Sobota, J.
Rodak, K.
Nowak, M.
Powiązania:
https://bibliotekanauki.pl/articles/355126.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
tin bronzes
KOBO
microstructure
mechanical properties
corrosion
Opis:
In this article the structural and mechanical properties of grain refinement of Cu-Sn alloys with tin content of 10%, 15% and 20% using the KOBO method have been presented. The direct extrusion by KOBO (name from the combination of the first two letters of the names of its inventors – A. Korbel and W. Bochniak) method employs, during the course of the whole process, a phenomenon of permanent change of strain travel, realized by a periodical, two-sided, plastic metal torsion. Moreover the aim of this work was to study corrosion resistance. The microstructure investigations were performed using an optical microscope Olimpus GX71, a scanning electron microscope (SEM) and a scanning transmission electron microscope (STEM). The mechanical properties were determined with INSTRON 4505/5500 machine. Corrosion tests were performed using «Autolab» set – potentiostat/galvanostat from EcoChemie B.V. with GPES software ver. 4.9. The obtained results showed possibility of KOBO deformation of Cu-Sn casting alloys. KOBO processing contributed to the refinement of grains and improved mechanical properties of the alloys. The addition of tin significantly improved the hardness. Meanwhile, with the increase of tin content the tensile strength and yield strength of alloys decrease gradually. Ductility is controlled by eutectoid composition and especially δ phase, because they initiate nucleation of void at the particle/matrix interface. No significant differences in the corrosion resistance between cast and KOBO processed materials were found.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 1; 95-102
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure of Commercial Purity Titanium Subjected to Complex Loading by the Kobo Method
Autorzy:
Kawałko, J.
Bieda, M.
Sztwiertnia, K.
Powiązania:
https://bibliotekanauki.pl/articles/353076.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Commercial Purity Titanium
plastic deformation
SPD
KOBO
microstructure
EBSD
Opis:
Observations of refined microstructure of Commercial Purity titanium for applications in biomedical devices has been carried out. Refinement of titanium microstructure has been performed in process with complex strain scheme. Materials investigated in this work were: Commercial Purity titanium grade 2 and grade 4. Samples of as received materials were subjected to plastic deformation in complex loading process of extrusion combined with oscillation twisting (KoBo extrusion). Both types of samples were deformed in single step of extrusion, in temperature of 450 °C, with extrusion ratio 19.14 and 12.25 for grade 2 titanium and grade 4 titanium, respectively. Initial mean grain diameter for both types of materials was approximately 30 μm. Samples were investigated by means of crystal orientation microscopy. In both cases considerable microstructure refinement has been observed. Microstructures of deformed samples are heterogenous and consist of both elongated and fine equiaxed grains. Elongated grains (lamellae) are separated by High Angle Grain Boundaries and feature internal structure with subgrains and dislocation walls. Grain refinement is stronger in material with higher extrusion ratio and mean grain diameter in this case is equal to 1.48 μm compared to 8.07 μm. in material with lower extrusion ratio. Mean misorientation angle (24° and 27° for grade 4 and grade 2 titanium) indicates high fraction of HAGBs in microstructures of KoBo deformed samples. Misorientation fluctuations inside grains have been analyzed and distinct curvature of crystal lattice have been observed. Hardness of samples after plastic deformation increased from 174.6±3.4 and 234.9±3.5 to 205.0±3.2 and 251.2±2.2 for titanium grade 2 and grade 4 respectively.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 31-36
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Primary Creep Behaviour of Two-Phase Titanium Alloy with Various Microstructure
Autorzy:
Ziaja, W.
Motyka, M.
Kubiak, K.
Sieniawski, J.
Powiązania:
https://bibliotekanauki.pl/articles/351523.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
two-phase titanium alloys
microstructure
finite element method
primary creep
Opis:
Creep and fatigue properties of two-phase titanium alloys show strong dependence on microstructure, especially morphology of the α and β phases which can be controlled to certain extent by proper selection of hot working and heat treatment conditions. In the paper the creep behaviour of Ti-6Al-2Mo-2Cr alloy (VT3-1) at elevated temperature was modelled. Finite element analyses of primary creep stage were carried out taking into account some microstructural features of the two-phase alloy that were included in the physical model and different properties of α and β phases. In order to verify results of calculations distinct types of microstructure were developed in the alloy by heat treatment and creep tests were carried out at elevated temperature (450°C) at various stress levels. Based on the FEM simulations the effect of changes of some microstructure features on primary creep strain development was estimated.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 683-688
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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