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    Wyświetlanie 1-6 z 6
    Tytuł:
    Oil identification based on total synchronous spectra
    Autorzy:
    Baszanowska, E.
    Otremba, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/246342.pdf
    Data publikacji:
    2014
    Wydawca:
    Instytut Techniczny Wojsk Lotniczych
    Tematy:
    fluorescence spectroscopy
    total synchronous spectra
    lubricate oil
    vessel engine room
    marine environment
    Opis:
    Contribution of marine carriage in the global transport is in permanent developing. It leads to increase the unintentional oil spills, which may induce serious disturbances in functioning of the natural marine ecosystem, especially when it interferes with other technical activities in the marine space. That fact contributes to increase the interest in searching of new research techniques to protect the natural ecosystem. Therefore, the main task of marine international organisations concentrates on the effective and rapid detection of oil spill and on the possibility of identifying oil pollutants as well as on origin of pollution. The purpose of the study is to characterise the oil belonging to the vessel engine lubricate oils. We analyse the stage results of investigations based on one of types of fluorescence spectroscopy, namely: synchronous spectra. To characterise the oil, the Aqualog Horiba spectrofluorometer was applied, which allows performing precise measurement in a short time. Based on the measured excitation-emission spectra, total synchronous fluorescence spectra for oil were obtained using various wavelength intervals. Total synchronous fluorescence spectra of petroleum substances allow finding wavelength interval typical for particular type of oil. This approach could allow obtaining of complex mixtures, such as oils, more efficient description. We discuss the total synchronous fluorescence spectra for engine oil (Marinol type) dissolved in n-hexane in various concentrations of oil as a possible tool proposed to oil type identification. We present changes and variation of the total synchronous fluorescence spectra for oil with various oil concentrations.
    Źródło:
    Journal of KONES; 2014, 21, 2; 15-20
    1231-4005
    2354-0133
    Pojawia się w:
    Journal of KONES
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Testing of the synchronous fluorescence in application to used lubricate oil characterisation
    Autorzy:
    Baszanowska, E.
    Otremba, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/243560.pdf
    Data publikacji:
    2016
    Wydawca:
    Instytut Techniczny Wojsk Lotniczych
    Tematy:
    marine fleet exploitation
    lubricate oil
    fluorescence spectroscopy
    synchronous fluorescence spectra
    Opis:
    Reliability of the ship propulsion system depends, inter alia, on the quality of lubricate oils. Research indicates that exploitive features of oil are reduced with it runtime in the ship engine circuit. At the present the basic parameters representing exploitive features of oil are: water content, total acid number and total base number or viscosity vs. temperature, anti-wear performance, further: content of additives and their concentrations, reaction products, and other contaminating substances, also magnetically separated large ferromagnetic particles, the size, the shape, the composition and concentration of the abnormal wear particles. Additional properties of oil are described based on atomic emission spectroscopy, granulometry of separated from the lubricant sample by magnets and gravity, permeability changes, as well as rheometric and tribometric characteristics. Complexity of composition of lubricate oil raises the idea to use changes of relative content of any compounds for characterization of oil exploitive features. Fluorescence method is possible to use for oil properties characterisation due to the presence mono and polycyclic compounds in oil that induces fluorescence phenomenon. Therefore identification the fluorescence spectra when exploitation time of oil increases could be novel indicator to monitor of lubricate oil exploitive quality. In this study we present changes of oil fluorescence expressed by synchronous spectra, taking into account working time of exemplary lubricate oil in the ship engine.
    Źródło:
    Journal of KONES; 2016, 23, 2; 39-44
    1231-4005
    2354-0133
    Pojawia się w:
    Journal of KONES
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Light absorption spectra for lubricate oil quality tracking in the combustion engine
    Autorzy:
    Baszanowska, E.
    Otremba, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/243648.pdf
    Data publikacji:
    2016
    Wydawca:
    Instytut Techniczny Wojsk Lotniczych
    Tematy:
    lubricate oil
    dissolved oil
    absorption spectroscopy
    absorption coefficient
    engine system
    Opis:
    The important role in the proper functioning of combustion engines plays the quality of lubricates oil. However, the quality of oil changes with the time of exploitation. Therefore, several parameters for examination of oil quality were determined; however, the indicator for quick and efficient tracking of evolution of oil with exploitation time is still searched. Taking into account the complex composition of oils, the ability of oils components to absorb light in various wavelengths is considered. In the article absorption properties of oils is discussed in relation to the time of circulation of oil in the engine lubricate system. For this study, two lubricate oils designated to lubricate the cylinder of vessel engines with different brightness and transparency were used. Oil samples were dissolved in organic solvent –n-hexane and several oil concentration were prepared based on dilution method. Absorbance spectra for eachsamples of oil were registered in the range of wavelength 240-600 nm. Obtained results indicate the changes of value of absorbance in relation to the kind of oil; however, the shape of absorbance spectra is independent from the kind of oil. For studied kinds of oil, characteristic peak independent from the kind of oil located at 260 nm was determined. Based on Lambert-Beer law absorption coefficient was identified as a potential indicator to oil quality evaluation with the time of exploitation in the engine system. Preliminary test for two fresh lubricate oils allow to conclude that absorption coefficient for selected wavelength located at 260 nm could be a sensitive parameter for quick estimating the degree of deterioration of the oil in engine system.
    Źródło:
    Journal of KONES; 2016, 23, 1; 55-60
    1231-4005
    2354-0133
    Pojawia się w:
    Journal of KONES
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Ultraviolet-induced fluorescence of lubricate oils
    Fluorescencja oleju smarnego wzbudzana światłem ultrafioletowym
    Autorzy:
    Baszanowska, E.
    Otremba, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/134176.pdf
    Data publikacji:
    2015
    Wydawca:
    Polskie Towarzystwo Naukowe Silników Spalinowych
    Tematy:
    lubricate oil
    fluorescence
    optical fiber
    olej smarny
    fluorescencja
    sensor optyczny
    Opis:
    The paper describes the study on relationship between the engine lubricate oil quality and fluorescence phenomenon. In order to determine the Excitation-Emission spectra (EEMs) of oil samples, a spectrofluorometer combined with an optical fiber system were applied. Two methods of fluorescence measurement: when oil diluted in non-fluorescent solvent (n-hexane) is placed in the quartz-cuvette inside the spectrofluorometer, and when oil sample is placed outside the spectrofluorometer (then EEMs is measured through the optical fiber sensor) were utilized to analyze the shape of EEMs of lubricate oil. Moreover in the second case of measurement, the optical fiber sensor was placed at an angle of 45 degrees to the oil surface, similarly above the oil surface and beneath the oil surface directly submerged in oil. Preliminary measurement results presented in this paper – on one hand – indicate diversity in the shape of EEMs depending on the method of fluorescence measurement, on the other hand – indicate possibility to measure fluorescence of oil directly in engine lubricate oil circuit.
    W artykule przedstawiono wyniki badań związku pomiędzy jakością oleju smarnego a zjawiskiem fluorescencji. W celu wyznaczenia widm zupełnych fluorescencji próbek oleju wykorzystano spektrofluorymetr połączony ze światłowodowym systemem pomiarowym. Zanalizowano kształt widm odnoszących się do oleju smarnego w dwóch sytuacjach, gdy: olej jest rozpuszczony w niefluoryzującym medium (n-hexan) i umieszczony jest w przyrządzie w kwarcowej kuwecie oraz gdy próbka oleju znajduje się na zewnątrz przyrządu, sygnał jest przenoszony światłowodem. Ponadto przy pomiarach z zastosowaniem światłowodu ustawiona pod kątem 45° głowica pomiarowa zestawu światłowodowego znajduje się, odpowiednio: w powietrzu nad powierzchnią oleju albo pod powierzchnię oleju. Przedstawione w niniejszym artykule wstępne wyniki badań z jednej strony wskazują na zróżnicowanie kształtów widm zupełnych fluorescencji względem metody pomiarowej, z drugiej strony – wskazują na możliwość wyznaczania fluorescencji bez wstępnej obróbki laboratoryjnej, bezpośrednio w silnikowym obiegu oleju smarnego.
    Źródło:
    Combustion Engines; 2015, 54, 4; 21-25
    2300-9896
    2658-1442
    Pojawia się w:
    Combustion Engines
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Spectrum of light absorption as the indicator of lubricate oil dispsersed in the natural water
    Autorzy:
    Baszanowska, E.
    Otremba, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/247346.pdf
    Data publikacji:
    2016
    Wydawca:
    Instytut Techniczny Wojsk Lotniczych
    Tematy:
    lubricate oil
    absorption
    absorption spectra of dispersed oil oil-in-water emulsion
    Opis:
    Oil pollutants in the natural water masses – especially in the seawater column – can be found in two forms, namely as dissolved oil or as dispersed one. With a broad set of methods, for studying the complex structure of petroleum products, due to the ability of petroleum products to absorb UV-light, absorbance spectra could be a relevant indicator to oil identification in aquatic environment and could support methods provided by the fluorescence technique. The intention of the study described in this article is to characterise the absorption properties of lubricate oil possible to found in the marine environment. Two types of oil as the representative of lubricate oils using in the ship engines are considered. One form of oil possible to found in the marine environment – oil-in-water emulsion was taken into account for analysis. Dispersed in water lubricate oil samples were prepared for several oil concentration for each type of oil. Spectrofluorometer Aqualog Horiba was used to register the absorbance spectra of oils. Based on the Lambert-Beer law the absorbance spectra were derived and specific parameter – absorption coefficient – for each wavelength of excitation, in the range 240-600 nm, was determined. Obtained results indicate decreasing of the oil absorbance value when excitation wavelength increases. Moreover, basing on the absorbance spectra it could be concluded that the main maximum for this kind of oils is located below 240 nm. However, in the considered range of excitation wavelength small flat peak, centred about 265 nm for both types of oils, was detected. Therefore one could conclude that absorbance of oils could be used as the indicator to detect of oil pollution in the natural environment omitting the labour intensive chemical methodology.
    Źródło:
    Journal of KONES; 2016, 23, 1; 61-66
    1231-4005
    2354-0133
    Pojawia się w:
    Journal of KONES
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Spectrofluorimetric characteristics of used lubricating oil
    Spektrofluorymetryczna charakterystyka zużytego oleju smarnego
    Autorzy:
    Baszanowska, E.
    Otremba, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/328239.pdf
    Data publikacji:
    2014
    Wydawca:
    Polska Akademia Nauk. Polskie Towarzystwo Diagnostyki Technicznej PAN
    Tematy:
    fluorescence
    excitation-emission spectra of oil
    lubricate oil
    ship engine
    fluorescencja
    zupełne widmo fluorescencji
    olej smarny
    silnik okrętowy
    Opis:
    Deterioration of lubricate oil in combustion engines enforces measurements of parameters essential for proper operation of define driving system or to certain engine malfunctions indicate. Since the fluorescence phenomenon is known for oil excited by ultraviolet light - the question arises whether fluorescence spectra evolving with the time of exploitation of oil in the engine. In this paper the introductory studies of excitation-emission spectra (EEMs) for chosen lubricate oil are described. Both fresh and used oil (after 593 h of work in a ship engine), was used to measure EEMs. As a result of comparison of EEMs for both fresh and used lubricate oils more significant transformations in fluorescence spectra of oil caused by their exploitation are indicated. Obtained results allow to predict that spectrofluorimetry method could supplement present methods of used lubricating oil testing.
    Pogarszanie się właściwości oleju smarnego w silniku spalinowym skutkuje koniecznością monitorowania jego eksploatacyjnych parametrów. Z racji wykazywania przez oleje fluorescencji w świetle ultrafioletowym - powstaje pytanie, czy widma fluorescencji ewoluują wraz z czasem przebywania oleju w obiegu smarnym silnika. W artykule opisane są wstępne analizy zmian zupełnych widm fluorescencji (EEMs) dla różnych stężeń wybranego oleju smarnego. Do pomiaru EEMs oleju użyto dwóch form oleju – świeżego i przepracowanego w silniku okrętowym w czasie 593 h. W następstwie porównania widm uzyskanych dla świeżego i przepracowanego oleju wskazano na zachodzące najbardziej znaczące zmiany we fluorescencji oleju smarnego. Uzyskane wyniki pozwalają sądzić, że spektrofluorymetria mogłaby uzupełnić obecne metody testowania przepracowanego oleju.
    Źródło:
    Diagnostyka; 2014, 15, 4; 65-71
    1641-6414
    2449-5220
    Pojawia się w:
    Diagnostyka
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-6 z 6

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