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Wyświetlanie 1-15 z 41
Tytuł:
Morphology and properties of the graphene layer on the copper substrate
Autorzy:
Pietrzak, K.
Olesińska, W.
Strąk, C.
Siedlec, R.
Gładki, A.
Powiązania:
https://bibliotekanauki.pl/articles/778091.pdf
Data publikacji:
2015
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
copper
graphene
graphene oxide
reduced graphene oxide
Opis:
The aim of the work presented in the article was to clarify controversial comments about anti-corrosion and mechanical properties of graphene coatings, deposited on copper substrates. It was designed special experimental cycle comprising: preparation of graphene forms and copper, the observation of layers Cu / GO (rGO) after the thermal reduction processes and oxidative test in air at 150°C temperature and 350 h in time. The resulting coatings and graphene layers were subjected to tribological test for hardness. The observed differences in the continuity of the coverage copper surface by graphene forms, allowed to understand the macroscopic effect of increased hardness and wear resistance layers rGO/Cu.
Źródło:
Polish Journal of Chemical Technology; 2015, 17, 4; 104-108
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Graphene oxide and green-synthesized reduced graphene oxide in chitosanbased nanocomposites
Autorzy:
Kosowska, K.
Domalik-Pyzik, P.
Chłopek, J.
Powiązania:
https://bibliotekanauki.pl/articles/284287.pdf
Data publikacji:
2017
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
graphene oxide
reduced graphene oxide
chitosan
hydroxyapatite
biomaterial
Opis:
The first part of the paper concerns synthesis and characterization of two types of nanomaterials: graphene oxide (GO) prepared by modified Marcano method and reduced graphene oxide (rGO) synthesized using green reductant, L-ascorbic acid. Their structural properties were investigated by attenuated total reflection Fourier-transform infrared spectroscopy (ATR-FTIR) and X-ray diffraction (XRD). Results confirmed that L-ascorbic acid is an effective reducing agent. Intensity of the oxygen-groups decreased dramatically what resulted in reduction of the GO interlayer spacing from 0.8 nm to 0.4 nm. The second part of the research was concentrated on the properties of chitosan nanocomposites modified with GO and rGO. Films were prepared by mixing of the chitosan solution with the nanoparticles dispersion. Scanning electron microscopy (SEM) was used to investigate the microstructure of the composites surface. In addition, wettability and pore size of the freeze-dried scaffolds were evaluated. Results of the mechanical tests (increase in Young’s modulus) and structural characterization confirmed that chitosan solution and GO dispersion can be mixed homogeneously. Reduction of GO during composite synthesis resulted in better dispersion of the nanosheets what increased surface roughness, wettability and stability in distilled water, PBS and Ringer’s solution compared to composite with GO. After detailed biological examination, rGO-modified nanocomposites can be potentially applied in tissue engineering.
Źródło:
Engineering of Biomaterials; 2017, 20, 142; 11-16
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Metody syntez i badania właściwości grafenu
Methods of synthesis and testing properties of graphene
Autorzy:
Jonik, J.
Purchała, M.
Grajek, H.
Powiązania:
https://bibliotekanauki.pl/articles/270836.pdf
Data publikacji:
2016
Wydawca:
Centralny Ośrodek Badawczo-Rozwojowy Aparatury Badawczej i Dydaktycznej, COBRABiD
Tematy:
tlenek grafitu
tlenek grafenu
zredukowany tlenek grafenu
graphite oxide
graphene oxide
reduced graphene oxide
Opis:
Grafen i jego pochodne są materiałami o unikalnych właściwościach biochemicznych, elektrycznych, optycznych i mechanicznych, co wzbudza zainteresowanie w wielu ośrodkach badawczych. Z tego powodu, na podstawie dostępnej literatury, podjęliśmy próbę zestawienia i interpretacji wyników badań uprzednio wymienionych materiałów otrzymanych różnymi metodami. Analizując wyniki badań różnych materiałów grafenopodobnych, można przypuszczać, że najbardziej ekonomiczną metodą otrzymywania grafenu jest zmodyfikowana metoda Hummersa. Najlepszymi technikami pomiarowymi są spektroskopia Ramana i rentgenowska spektroskopia fotoelektronów. Obydwie techniki umożliwiają ocenę składu chemicznego badanych próbek oraz stopnia ich zdefektowania. W pracy przedstawiono również niektóre z licznych zastosowań tych materiałów oraz wnioski.
Graphene and its derivatives are the materials with unique biochemical, electric, optical and mechanical properties, which has aroused interest in many research centres. Therefore, on the basis of the accessible literature, we attempt to collate and interpret the results of the aforesaid materials obtained by different methods. Analysing the results for the different graphene-like materials one can suppose, that the most economical method of the graphene synthesis is the modified Hummers’ method. The most useful testing techniques are the Raman spectroscopy and the X-ray photoelectron spectroscopy. Both techniques enable the estimation of the chemical composition and the presence of defect structure in the materials. Some of the many applications of the materials and conclusions are also presented in our review.
Źródło:
Aparatura Badawcza i Dydaktyczna; 2016, 21, 2; 110-117
2392-1765
Pojawia się w:
Aparatura Badawcza i Dydaktyczna
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure and Properties of Nanocomposite Nickel/Graphene Oxide Coatings Produced by Electrochemical Reduction Method
Autorzy:
Cieślak, G.
Trzaska, M.
Powiązania:
https://bibliotekanauki.pl/articles/354431.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
graphene oxide
nanocomposites
electrodeposition
nickel/graphene oxide coatings
corrosion tests
Opis:
The paper presents the results of research on nanocomposite nickel/graphene oxide (Ni/GO) coatings produced by electrochemical reduction method on a steel substrate. Discussed is the method of manufacturing composite coatings with nickel matrix and embedded graphene oxide flakes. For comparative purposes, the studies also included a nanocrystalline Ni coating without embedded graphene oxide flakes. Graphene oxide was characterized by Raman spectroscopy, infrared spectroscopy (FTIR) and transmission (TEM) and scanning (SEM) electron microscopy. Results of studies on the structure of nickel and composite Ni/GO coatings deposited in a bath containing different amount of graphene oxide are presented. The coatings were characterized by scanning electron microscopy, light microscopy, Raman spectroscopy and X-ray diffraction. The adhesion of the prepared coatings to the substrate was examined by the scratch method. The microhardness of the coatings was measured using the Vickers method on perpendicular cross-sections to the surface. Corrosion tests of the coatings were investigated using the potentiodynamic method. The influence of graphene oxide on the structure and properties of composite coatings deposited from baths with different content of graphene oxide was determined.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 4; 1479-1486
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation of functionalized graphene oxide coatings on gold
Autorzy:
Trzaskowski, M.
Ciach, T.
Powiązania:
https://bibliotekanauki.pl/articles/285667.pdf
Data publikacji:
2016
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
gold
coatings
graphene oxide
Źródło:
Engineering of Biomaterials; 2016, 19, 138; 88
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Composite coatings of polylactide with graphene oxide and hydroxyapatite on titanium
Autorzy:
Torcuato, M. S.
Szaraniec, B.
Kąc, S.
Chłopek, J.
Powiązania:
https://bibliotekanauki.pl/articles/284150.pdf
Data publikacji:
2018
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
coatings
graphene oxide
hydroxyapatite
Źródło:
Engineering of Biomaterials; 2018, 21, 148; 116
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Graphene and graphene oxide in the oil and gas industry
Autorzy:
Jamrozik, A.
Powiązania:
https://bibliotekanauki.pl/articles/299253.pdf
Data publikacji:
2017
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
Tematy:
drilling
nanotechnologies
graphene
graphene oxide
Opis:
Presently, nanotechnology and nanomaterials have found a number of applications in drilling, exploration and production (E&P) works, as well as in the area of refinery and distribution of crude oil and natural gas. Nanomaterials enjoy considerable popularity owing to their new and unique features which differentiate them from classical materials. Graphene is a relatively new material. Currently it occupies the seventh position among the most commonly used nanomaterials in oil and gas industry. This paper presents the properties graphene and graphene oxide and gives an insight into the applicability of graphene and graphene oxide in the oil and gas industry.
Źródło:
AGH Drilling, Oil, Gas; 2017, 34, 3; 731-744
2299-4157
2300-7052
Pojawia się w:
AGH Drilling, Oil, Gas
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Chitosan-based nanocomposites modified with reduced graphene oxide prepared via green synthesis
Autorzy:
Kosowska, K.
Domalik-Pyzik, P.
Jagiełło, J.
Lipińska, L.
Chłopek, J.
Powiązania:
https://bibliotekanauki.pl/articles/284680.pdf
Data publikacji:
2017
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
nanocomposites
graphene oxide
green synthesis
Źródło:
Engineering of Biomaterials; 2017, 20, no. 143 spec. iss.; 59
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Equilibrium and kinetics studies for the adsorption of Ni2+ and Fe3+ ions from aqueous solution by graphene oxide
Autorzy:
Konicki, W.
Aleksandrzak, M.
Mijowska, E.
Powiązania:
https://bibliotekanauki.pl/articles/778711.pdf
Data publikacji:
2017
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
nickel
iron
graphene oxide
adsorption
kinetics
Opis:
In this study, the adsorption of Ni2+  and Fe3+  metal ions from aqueous solutions onto graphene oxide (GO) have been explored. The effects of various experimental factors such as pH of the solution, initial metal ion concentration and temperature were evaluated. The kinetic, equilibrium and thermodynamic studies were also investigated. The adsorption rate data were analyzed using the pseudo-first-order kinetic model, the pseudo-second-order kinetic model and the intraparticle diffusion model. Kinetic studies indicate that the adsorption of both ions follows the pseudo-second-order kinetics. The isotherms of adsorption data were analyzed by adsorption isotherm models such as Langmuir and Freundlich. Equilibrium data fitted well with the Langmuir model. The maximum adsorption capacities of Ni2+  and Fe3+  onto GO were 35.6 and 27.3 mg g-1 , respectively. In addition, various thermodynamic parameters, such as enthalpy (ΔHO), entropy (ΔSO) and Gibbs free energy (ΔGO), were calculated.
Źródło:
Polish Journal of Chemical Technology; 2017, 19, 3; 120-129
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Obtaining and Application of New Cellulose- and Graphene Oxide-Based Adsorbents for Treatment of Industrial Waste Containing Heavy Metals
Autorzy:
Fryczkowska, B.
Wyszomirski, M.
Puzoń, M.
Powiązania:
https://bibliotekanauki.pl/articles/125232.pdf
Data publikacji:
2017
Wydawca:
Polskie Towarzystwo Inżynierii Ekologicznej
Tematy:
cellulose
graphene oxide
sorption
galvanizing wastewater
Opis:
The paper presents the results of studies on the preparation and properties of composite granules produced by phase inversion from cellulose (CEL) solutions in 1-ethyl-3-methylimidazole acetate (EMIMAc), containing nano-addition in the form of graphene oxide (GO) in N,N-dimethylformamide (DMF). Water absorption and sorption of such compounds as FeCl3, methylene blue (MB) and bovine serum albumin (BSA) were studied. In addition, attempts were made to investigate the sorption properties of the obtained cellulose granules in terms of metals removal from galvanizing wastewater. Among the many components, iron and lead were found to have the highest concentration (~ 1 mg Fe/dm3; ~2 mg Pb/dm3) in the tested wastewater sample. The qualitative and quantitative composition of the wastewater was examined by UV-Vis spectrophotometry. The studies show that doping of cellulose with Graphene oxide clearly affects the physical properties of this biopolymer. GO improves the water absorption of CEL/GO composite cellulose granules only in the concentration above 0.05% w/w. For a concentration of 0.1% w/w of GO in cellulose, water absorption is increased by ~108% compared to pure cellulose granules. In addition, the use of dry and wet granules in the study changes their sorption properties with respect to all tested substances. Studies on test solutions have shown that the sorption of cellulose granules decreases with increasing molar mass of test compounds, in the following order: FeCl3, methylene blue (MB) and bovine albumin (BSA). This means that the cellulose granules obtained in the experiment are made up of small micropores, which makes the diffusion of compounds of high molecular weight difficult. The best sorption results were obtained for ferric ions and amounted to 66–72% for FeCl3 solution, and ~92% for the wastewater that was sorbed on pure cellulose granules.
Źródło:
Journal of Ecological Engineering; 2017, 18, 6; 43-52
2299-8993
Pojawia się w:
Journal of Ecological Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Applications of chitosan–graphene oxide nanocomposites in medical science: a review
Autorzy:
Pieklarz, Katarzyna
Tylman, Michał
Modrzejewska, Zofia
Powiązania:
https://bibliotekanauki.pl/articles/1034405.pdf
Data publikacji:
2018
Wydawca:
Sieć Badawcza Łukasiewicz - Polskie Towarzystwo Chitynowe
Tematy:
biopolymers
chitosan
graphene
graphene oxide
nanomedicine
Opis:
Combinations of biopolymers with nanostructured carbon materials have been the subject of interest of many scientists in recent years. Particularly significant are nanocomposites made of chitosan, which is a linear aminopolysaccharide obtained in the process of deacetylation of chitin, and graphene oxide (GO). These systems, due to the atypical properties of both components such as non-toxicity, biocompatibility with human tissues and organs as well as bacteriostaticity, are characterised by a wide range of biomedical applications. They may be used in emergency medicine as dressing materials which accelerate wound healing, as well as carriers of drugs/genes and biological macromolecules, for example proteins, peptides and nucleic acids. In addition, CS-GO systems can potentially be used in regenerative medicine as scaffolds for cell culture. For this reason, the current publication presents the possibilities of the application of chitosan–graphene oxide nanocomposites in medicine considering the characteristics of the system components.
Źródło:
Progress on Chemistry and Application of Chitin and its Derivatives; 2018, 23; 5-24
1896-5644
Pojawia się w:
Progress on Chemistry and Application of Chitin and its Derivatives
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The sensitivity of sensor structures with oxide graphene exposed to selected gaseous atmospheres
Autorzy:
Pustelny, T.
Drewniak, S.
Setkiewicz, M.
Maciak, E.
Urbańczyk, M.
Procek, M.
Gut, K.
Opilski, Z.
Jagiello, J.
Lipinska, L.
Powiązania:
https://bibliotekanauki.pl/articles/200229.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
graphene
graphene oxide
gas sensors
resistive sensors
Opis:
The paper presents the results of investigations on the resistive structure with a graphene oxide (GO) sensing layer. The effects of dangerous gases (hydrogen and nitrogen dioxide) on the structure were studied; the resistance changes were examined during the flow of the selected gas in the atmosphere of synthetic air. Measurements were performed with a special emphasis on the detection of low concentrations of the analyzed gases. The reactions of the sensing structure to the effect of nitrogen and synthetic air at different humidity were also tested. Much attention was also paid to the fast response of the sensor to the changes in the gas atmosphere. The thin palladium layer (~2 nm) has been applied in order to improve the sensing properties of the structure. The investigations were performed in the temperature range from RT to 120°C and the analyzed gases in synthetic air were batched alternately with pure synthetic air.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2013, 61, 3; 705-710
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation and properties of cellulose membranes with graphene oxide addition
Autorzy:
Fryczkowska, B.
Wiechniak, K.
Powiązania:
https://bibliotekanauki.pl/articles/778535.pdf
Data publikacji:
2017
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
cellulose
ionic liquid
graphene oxide
membranes
transport properties
Opis:
The paper presents results of research on the preparation of cellulose membranes with graphite oxide addition (GO/CEL). Initially, a cellulose (CEL) solution in 1-ethyl-3-methylimidazole acetate (EMIMAc) was obtained, to which graphene oxide (GO) dispersed in N,N-dimethylformamide (DMF) was added. From this solution, composite membranes were formed using phase inversion method. It was observed that the GO addition influences the physico-chemical properties of GO/CEL composite membranes, resulting in an increase in their mass per unit area, thickness and density, and a decrease in sorption properties. In addition, the study of transport properties has shown that GO/CEL membranes do not absorb BSA particles on their surface, which prevents the unfavorable phenomenon of fouling. An important feature of the obtained membranes is the specific permeate flux which reaches high values (~124 L/m2 ×h) at 3.8% of the GO addition to the cellulose matrix.
Źródło:
Polish Journal of Chemical Technology; 2017, 19, 4; 41-49
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of expanded graphite (EG) and graphene oxide (GO) on physical properties of PET based nanocomposites
Autorzy:
Paszkiewicz, S.
Nachman, M.
Szymczyk, A.
Špitalský, Z.
Mosnáček, J.
Rosłaniec, Z.
Powiązania:
https://bibliotekanauki.pl/articles/778760.pdf
Data publikacji:
2014
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
in situ polymerization
PET
graphene oxide
expanded graphite
Opis:
This work is the continuation and refinement of already published communications based on PET/EG nanocomposites prepared by in situ polymerization1, 2. In this study, nanocomposites based on poly(ethylene terephthalate) with expanded graphite were compared to those with functionalized graphite sheets (GO). The results suggest that the degree of dispersion of nanoparticles in the PET matrix has important effect on the structure and physical properties of the nanocomposites. The existence of graphene sheets nanoparticles enhances the crystallization rate of PET. It has been confirmed that in situ polymerization is the effective method for preparation nanocomposites which can avoid the agglomeration of nanoparticles in polymer matrices and improve the interfacial interaction between nanofiller and polymer matrix. The obtained results have shown also that due to the presence of functional groups on GO surface the interactions with PET matrix can be stronger than in the case of exfoliated graphene (EG) and matrix.
Źródło:
Polish Journal of Chemical Technology; 2014, 16, 4; 45-50
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Bioactive Membranes from Cellulose with a Graphene Oxide Admixture
Autorzy:
Machnicka, A.
Fryczkowska, B.
Powiązania:
https://bibliotekanauki.pl/articles/123371.pdf
Data publikacji:
2018
Wydawca:
Polskie Towarzystwo Inżynierii Ekologicznej
Tematy:
cellulose
graphene oxide
membranes
bactericidal properties
fungicidal properties
Opis:
The paper presents the results of microbiological tests of composite membranes made of cellulose (CEL) with graphene oxide (GO) admixture. At the beginning, the antibacterial properties of the GO in aqueous solutions of various concentrations (0.001; 0.01; 0.1% w/w) were studied, and the obtained results allowed to use GO as an additive to cellulose membranes. The solution used to prepare the membranes was a 5% cellulose solution (CEL) in 1-ethyl-3-methylimidazolium acetate (EMIMAc), into which various amounts of graphene oxide (GO) dispersed in N,N-dimethylformamide (DMF) were added (0.5÷28.6% of GO). From this solution, composite membranes were formed using phase inversion method. It was observed that the GO addition influences the process of membrane formation and their physicochemical properties. The obtained membranes were subjected to microbiological tests using the Gram-negative bacteria (Escherichia coli), Gram-positive bacteria (Staphylococcuc aureus) and fungi (Candida albicans). It was observed that the GO addition to the cellulose membrane (GO/CEL) inhibited the growth of bacteria and fungi, and the biological activity as dependent on the type of living organism and the size of GO particles.
Źródło:
Journal of Ecological Engineering; 2018, 19, 6; 231-240
2299-8993
Pojawia się w:
Journal of Ecological Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 41

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