Temat: sem/edx - Katalog OPAC zbiorów

Skocz do pozycji: 1.

Tytuł:: Analysis of Optimum Temperature and Calcination Time in the Production of CaO Using Seashells Waste as CaCO3 Source
Autorzy:: Dampang, Sarah
Purwanti, Endah
Destyorini, Fredina
Kurniawan, Setyo Budi
Abdullah, Siti Rozaimah Sheikh
Imron, Muhammad Fauzul
Powiązania:: https://bibliotekanauki.pl/articles/1838407.pdf
Data publikacji:: 2021
Wydawca:: Polskie Towarzystwo Inżynierii Ekologicznej
Tematy:: characterization
conversion
environment
FTIR
SEM-EDX
TGA
Opis:: Seashells waste is abundant in coastal area, especially in the locations where fisheries are a major occupation. This abundant resource of seashells opens a new opportunity further utilization. Seashells waste is a source of CaCO3, which may be converted into CaO via the calcination process. This study analyzed the characteristics of the CaO produced via calcination process at different temperature and calcination time. The calcination process was carried out at a temperature of 800°C, 900°C, and 1000°C with variation of 2, 3, and 4 hours in time. The Fourier transform infrared spectroscopy (FTIR) result showed that the spectrum of 2513 cm-1 as an indication of the C-H group containing CaO appearing after calcination. The FTIR results suggest that the calcination time did not gave major alteration to the functional groups. The results of X-ray diffraction (XRD) analysis showed that CaO laid at the angle of 58.1° and 64.6°. Scanning Electron Microscopy–Energy Dispersive X-Ray Spectroscopy (SEM-EDS) results showed that the most significant compositional outcome after the calcination process was Ca and O at all temperatures and calcination times. All calcined seashells showed rough surface and irregular shape particles. The result of a Thermogravimetric analysis (TGA) suggested that the highest mass alteration occurred at a temperature of 800°C with 78 mins of calcination time.
Źródło:: Journal of Ecological Engineering; 2021, 22, 5; 221-228
2299-8993
Pojawia się w:: Journal of Ecological Engineering
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 2.

Tytuł:: Physical and chemical mechanisms of hydrophobicity of nanoparticle membranes (Mg+Al2O3)
Autorzy:: Wahyudi, Wahyudi
Subagyo, R.
Gapsari, F.
Powiązania:: https://bibliotekanauki.pl/articles/368531.pdf
Data publikacji:: 2019
Wydawca:: Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:: hydrophobic
superhydrophobic
hydrophilic
SEM-EDX
gas bubbles
nanoparticles
membranes
hydrofobowość
superhydrofobowość
hydrofilowość
pęcherze gazowe
nanocząstki
membrany
Opis:: Purpose: Investigate the hydrophobic, superhydrophobic and hydrophilic properties of Alumina (Al2O3) and Magnesium (Mg) nanoparticles. Design/methodology/approach: This research was conducted by SEM-EDX analysis of Magnesium and Alumina nanoparticles, observation of gas bubbles when droplets of water contact with membrane surfaces, measurement of surface roughness and detection of Hydrogen gas production using Gas Chromatography. There are eleven compositions (Al2O3:Mg) membranes used in this study, namely: (0:100; 10:90; 20:80; 30:70; 40:60; 50:50; 60:40; 70:30; 80:20; 90:10; and 100:0). Findings: Successfully found an alloy membrane between Alumina (Al2O3) and Magnesium (Mg) nanoparticles in the composition of Mg:Al2O3 (0:100%) having Hydrophobic properties; Mg:Al2O3 (50:50%) has Superhydrophobic properties and Mg:Al2O3 (100:0%) has hydrophilic properties. Three conditions occur when H2O droplets come in contact with the membrane layer, namely: hydrophobic conditions when the trapped gas pressure is smaller than the droplet pressure. Superhydrophobic conditions when the trapped gas pressure is equal to the droplet pressure. Hydrophilic conditions occur when the trapped gas pressure is greater than the droplet pressure. Research limitations/implications: This research is limited to the hydrophobic nature of Nano Alumina (Al2O3) and Magnesium (Mg) membrane particles. Practical implications: Superhydrophobic properties are very suitable to be applied to membranes that are useful for destiny. Originality/value: The novelty of this study is to find the right mixture of nanoparticles of Alumina and Magnesium in a composition that is capable of creating hydrophobic, superhydrophobic and hydrophilic properties.
Źródło:: Journal of Achievements in Materials and Manufacturing Engineering; 2019, 96, 2; 57-68
1734-8412
Pojawia się w:: Journal of Achievements in Materials and Manufacturing Engineering
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 3.

Tytuł:: Identification of Natural Dyes on 18th Century Liturgical Textiles from Dubrovnik
Identyfikacja naturalnych barwnik w na XVIII-to wiecznych tekstyliach liturgicznych z Dubrownika
Autorzy:: Jemo, D.
Parac-Osterman, D.
Powiązania:: https://bibliotekanauki.pl/articles/231754.pdf
Data publikacji:: 2017
Wydawca:: Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
Tematy:: natural dyes
liturgical textile
UV/VIS
SEM-EDX
FTIR-ATR
HPLC
Dubrovnik
barwniki naturalne
szaty liturgiczne
chromatografia
Dubrownik
Opis:: In this paper researches were carried out on fragments of textiles from the 18th century from Dubrovnik, for which, based on the design and art-historical analysis, it was determined that it was a part of an object (pluvial, cope) from liturgical vestments (ecclesiastical textiles) of the Dubrovnik diocese. Using modern non-destructive and micro-destructive methods we conducted the identification of green, blue and red as the dominant tones on the artefacts of historical textiles from Dubrovnik. The identification was based on the application of modern complementary techniques: UV / VIS, HPLC, SEM-EDX and FTIR-ATR. We analysed samples of coloured fiber, as well as ones obtained by the extraction of dyes from the dyed fibers. Archival data on natural dyes used in the Dubrovnik region in the period 14-19th century was taken into account in the identification of the historical textile dyes.
W artykule opisano badania przeprowadzone na fragmentach XVIII-to wiecznych szat liturgicznych z Dubrownika. Stosując nowoczesne metody nieinwazyjne i mało niszczące przeprowadzono identyfikację zielonego, niebieskiego i czerwonego koloru, jako dominujących tonów na artefaktach tkanin historycznych. Identyfikacja oparta była na zastosowaniu nowoczesnych technik uzupełniających: UV/VIS, HPLC, SEM-EDX oraz FTIR-ATR. Analizowano próbki włókien dokonując ekstrakcji barwników. Wyniki badań porównano z archiwalnymi danymi dotyczącymi stosowania naturalnych barwników w regionie Dubrownika w okresie XIV-XIX wieku.
Źródło:: Fibres & Textiles in Eastern Europe; 2017, 1 (121); 113-120
1230-3666
2300-7354
Pojawia się w:: Fibres & Textiles in Eastern Europe
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 4.

Tytuł:: Powstawanie apatytu na elastycznym kompozycie kościozastępczym
Apatite formation on flexible bone substitute
Autorzy:: Borkowski, L.
Ginalska, G.
Ślósarczyk, A.
Paszkiewicz, Z.
Powiązania:: https://bibliotekanauki.pl/articles/285812.pdf
Data publikacji:: 2011
Wydawca:: Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:: bioaktywność
biokompatybilność
hydroksyapatyt węglanowy (CHAP)
kompozyt kościozastępczy
SBF
SEM-EDX
bioactivity
biocompatibility
bone substitutes
carbonated hydroxyapatite (CHAP)
simulated body fluid (SBF)
Opis:: Podstawowe cechy materiałów kościozastępczych takie jak bioaktywność i biokompatybilność, mogą być badane in vitro przy wykorzystaniu roztworu imitującego płyn tkankowy tzw. płyn SBF. Dwufazowy kompozyt, przeznaczony do wypełniania ubytków kostnych, został wykonany z granul hydroksyapatytu węglanowego i polimeru polisacharydowego. Biomateriał testowano pod kątem zdolności tworzenia warstwy apatytu w roztworze SBF przez okres 30 dni. Po tym czasie powierzchnię próbek i płyn po inkubacji, poddano analizie z wykorzystaniem SEM-EDX. Wykazano tworzenie warstwy apatytowej na powierzchni kompozytu kościozastępczego.
Biocompatibility and bioactivity, elementary characteristics of bone substitute materials, can be examined in vitro using solution that simulates body fluids. Two-phase composite, intended for filling bone defects, was made of carbonated hydroxyapatite granules and polysaccharide polymer. Biomaterial was tested whether it can form apatite layer during soaking in SBF solution for 30 days. After that time, the surface of composite samples and the fluid were analyzed using SEM-EDX. Our observations indicate the ability of a bone substitute biomaterial to form apatite layer on its surface.
Źródło:: Engineering of Biomaterials; 2011, 14, no. 106-108; 105-109
1429-7248
Pojawia się w:: Engineering of Biomaterials
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 5.

Tytuł:: Microstructure, SDAS and Mechanical Properties of A356 alloy Castings Made in Sand and Granulated Blast Furnace Slag Moulds
Autorzy:: Jinugu, B. R.
Inampudi, N. M.
Powiązania:: https://bibliotekanauki.pl/articles/379468.pdf
Data publikacji:: 2017
Wydawca:: Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:: silica sand
slag
CO2 process
casting aluminium alloys
SEM-EDX
mechanical properties
piasek kwarcowy
żużel
proces CO2
odlew ze stopów aluminium
właściwości mechaniczne
Opis:: Investigations were carried out to ensure the granulated blast furnace (GBF) slag as an alternative mould material in foundry industry by assessing the cast products structure property correlations. Sodium silicate-CO₂ process was adopted for preparing the moulds. Three types of moulds were made with slag, silica sand individually and combination of these two with 10% sodium silicate and 20 seconds CO₂ gassing time. A356 alloy castings were performed on these newly developed slag moulds. The cast products were investigated for its metallography and mechanical properties. Results reveal that cast products with good surface finish and without any defects were produced. Faster heat transfers in slag moulds enabled the cast products with fine and refined grain structured; and also lower Secondary Dendrite Arm Spacing (SDAS) values were observed than sand mould. Slag mould casting shows improved mechanical properties like hardness, compression, tensile and impact strength compared to sand mould castings. Two types of tensile fracture modes, namely cleavage pattern with flat surfaces representing Al−Si eutectic zone and the areas of broken Fe-rich intermetallic compounds which appear as flower-like morphology was observed in sand mould castings. In contrast, GBF slag mould castings exhibit majority in dimple fracture morphology with traces of cleavage fracture. Charpy impact fractured surfaces of sand mould castings shows both transgranular and intergranular fracture modes. Only intergranular fracture mode was noticed in both GBF slag and mixed mould castings.
Źródło:: Archives of Foundry Engineering; 2017, 17, 1; 179-191
1897-3310
2299-2944
Pojawia się w:: Archives of Foundry Engineering
Dostawca treści:: Biblioteka Nauki

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