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Wyświetlanie 1-5 z 5
Tytuł:
Microstructure and magnetic properties of amorphous Fe51Co12Si16B8Mo5P8 alloy
Autorzy:
Hasiak, M.
Miglierini, M.
Amini, N.
Bujdoš, M.
Powiązania:
https://bibliotekanauki.pl/articles/147218.pdf
Data publikacji:
2017
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
microstructure
Mössbauer spectroscopy
magnetic properties
Curie point
Opis:
Microstructure and thermomagnetic characteristics of the amorphous Fe51Co12Si16B8Mo5P8 alloy in the as-quenched state and after 1 h of annealing at 573 K and 773 K are studied. The structural investigations performed by Mössbauer spectroscopy and X-ray diffractometry confirmed the amorphous structure of the analysed materials. An increase in the annealing temperature up to 773 K does not lead to crystallization of the amorphous alloy. Only structural rearrangement that causes changes in the topological short-range order and annealing out of free volume is observed. This behaviour was confi rmed by modifications of the shapes of hyperfi ne field distributions derived from the corresponding Mössbauer spectra of the investigated alloys. The Curie temperatures of the as-quenched and annealed Fe51Co12Si16B8Mo5P8 alloy at 573 and 773 K are 400, 405 and 421 K, respectively.
Źródło:
Nukleonika; 2017, 62, 2; 85-89
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Soft Magnetic Properties of Fe-Zr-(Pt)-Nb-Cu-B Amorphous Alloys
Autorzy:
Gondro, J.
Błoch, K.
Nabiałek, M.
Walters, S.
Powiązania:
https://bibliotekanauki.pl/articles/356965.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
amorphous alloys
Mössbauer spectroscopy
magnetic susceptibility
Curie temperature
magnetic properties
Opis:
This paper presents the results of investigations into the microstructure and magnetic properties of Fe86Zr7Nb1Cu1B5, Fe82Zr7Nb2Cu1B8 and Fe81Pt5Zr7Nb1Cu1B5 alloys. The alloys were investigated in their as-quenched state, in the form of thin ribbons with approximate dimensions as follows: width 3 mm and thickness 20 μm. The investigations were performed utilizing Mössbauer spectrometry and X-ray diffractometry. Also, an evaluation of the low-field magnetic susceptibility and measurements of the magnetization versus temperature and magnetizing field were performed.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2A; 707-710
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects of Co, Ni, and Cr addition on microstructure and magnetic properties of amorphous and nanocrystalline Fe86−xMxZr7Nb2Cu1B4 (M = Co, Ni, CoCr, and Cr, x = 0 or 6) alloys
Autorzy:
Łukiewska, A.
Świerczek, J.
Hasiak, M.
Olszewski, J.
Zbroszczyk, J.
Gębara, P.
Ciurzyńska, W.
Powiązania:
https://bibliotekanauki.pl/articles/147169.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
amorphous materials
nanocrystalline materials
Mössbauer spectroscopy
invar effect
Curie temperature
Opis:
Mössbauer spectra and thermomagnetic curves for the Fe86-xMxZr7Nb2Cu1B4 (M = Co, Ni, CoCr, and Cr, x = 0 or 6) alloys in the as-quenched state and after the accumulative annealing in the temperature range 600–800 K for 10 min are investigated. The parent Fe86Zr7Nb2Cu1B4 amorphous alloy is paramagnetic at room temperature, and substitution of 6 at.% of Fe by Co, Ni, and CoCr changes the magnetic structure – the alloys become ferromagnetic, whereas replacing 6 at.% of Fe with Cr preserves the paramagnetic state. After the heat treatment at 600 K, the decrease of the average hyperfi ne fi eld induction, as compared to the as-quenched state, is observed due to the invar effect. After this annealing, the Curie temperature for all investigated alloys decreases. The accumulative annealing up to 800 K leads to the partial crystallization; α-Fe or α-FeCo grains with diameters in the range of 12–30 nm in the residual amorphous matrix appear.
Źródło:
Nukleonika; 2015, 60, 1; 103-108
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Curie Temperature and Microstructural Changes Due to the Heating Treatment of Magnetic Amorphous Materials
Autorzy:
Gondro, J.
Błoch, K.
Brągiel, P.
Nabiałek, M.
Szota, M.
Powiązania:
https://bibliotekanauki.pl/articles/958228.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
amorphous alloys
magnetic properties
magnetic susceptibility
Mössbauer spectroscopy
Curie temperature
Opis:
Three distinct alloys: Fe86Zr7Nb1Cu1B5, Fe82Zr7Nb2Cu1B8, and Fe81Pt5Zr7Nb1Cu1B5 were characterized both magnetically and structurally. The samples, obtained with spinning roller method as a ribbons 3 mm in width and 20 μm thick, were investigated as-quenched and after each step of a multi steps heating treatment procedure. Each sample was annealed at four steps, fifteen minutes at every temperature, starting from 573K+600K up to +700K depending on type of alloy. Mössbauer spectroscopy data and transmission electron microscope (HRE M) pictures confirmed that the as-quenched samples are fully amorphous. This is not changed after the first stages of treatment heating leads to a reduction of free volumes. The heating treatment has a great influence on the magnetic susceptibilities. The treatment up to 600K improves soft magnetic properties: an χ increase was observed, from about 400 to almost 1000 for the samples of alloys without Pt, and from about 200 to 450 at maximum, for the Fe81Pt5Zr7Nb1Cu1B5. Further heating, at more elevated temperatures, leads to magnetic hardening of the samples. Curie temperatures, established from the location of Hopkinson’s maxima on the χ(T) curve are in very good agreement with those obtained from the data of specific magnetization, σ(T), measured in a field of 0.75T. As a critical parameter β was chosen to be equal 0.36 for these calculations, it confirmed that the alloys may be considered as ferromagnetic of Heisenberg type. Heating treatment resulted in decreasing of TC. These changes are within a range of several K.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 451-456
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hyperfine interaction and some thermomagnetic properties of amorphous and partially crystallized Fe70−xMxMo5Cr4Nb6B15 (M = Co or Ni, x = 0 or 10) alloys
Autorzy:
Rzącki, J.
Świerczek, J.
Hasiak, M.
Olszewski, J.
Zbroszczyk, J.
Ciurzyńska, W.
Powiązania:
https://bibliotekanauki.pl/articles/148195.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
Mössbauer spectroscopy
amorphous alloys
magnetic properties
X-ray diffraction
Curie temperature
Opis:
As revealed by Mössbauer spectroscopy, replacement of 10 at.% of iron in the amorphous Fe70Mo5Cr4Nb6B15 alloy by cobalt or nickel has no effect on the magnetic structure in the vicinity of room temperature, although the Curie point moves from 190 K towards ambient one. In the early stages of crystallization, the paramagnetic crystalline Cr12Fe36Mo10 phase appears before α-Fe or α-FeCo are formed, as is confi rmed by X-ray diffractometry and transmission electron microscopy. Creation of the crystalline Cr12Fe36Mo10 phase is accompanied by the amorphous ferromagnetic phase formation at the expense of amorphous paramagnetic one.
Źródło:
Nukleonika; 2015, 60, 1; 121-126
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-5 z 5

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