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Wyświetlanie 1-2 z 2
Tytuł:
Analysis of Optimum Temperature and Calcination Time in the Production of CaO Using Seashells Waste as CaCO3 Source
Autorzy:
Dampang, Sarah
Purwanti, Endah
Destyorini, Fredina
Kurniawan, Setyo Budi
Abdullah, Siti Rozaimah Sheikh
Imron, Muhammad Fauzul
Powiązania:
https://bibliotekanauki.pl/articles/1838407.pdf
Data publikacji:
2021
Wydawca:
Polskie Towarzystwo Inżynierii Ekologicznej
Tematy:
characterization
conversion
environment
FTIR
SEM-EDX
TGA
Opis:
Seashells waste is abundant in coastal area, especially in the locations where fisheries are a major occupation. This abundant resource of seashells opens a new opportunity further utilization. Seashells waste is a source of CaCO3, which may be converted into CaO via the calcination process. This study analyzed the characteristics of the CaO produced via calcination process at different temperature and calcination time. The calcination process was carried out at a temperature of 800°C, 900°C, and 1000°C with variation of 2, 3, and 4 hours in time. The Fourier transform infrared spectroscopy (FTIR) result showed that the spectrum of 2513 cm-1 as an indication of the C-H group containing CaO appearing after calcination. The FTIR results suggest that the calcination time did not gave major alteration to the functional groups. The results of X-ray diffraction (XRD) analysis showed that CaO laid at the angle of 58.1° and 64.6°. Scanning Electron Microscopy–Energy Dispersive X-Ray Spectroscopy (SEM-EDS) results showed that the most significant compositional outcome after the calcination process was Ca and O at all temperatures and calcination times. All calcined seashells showed rough surface and irregular shape particles. The result of a Thermogravimetric analysis (TGA) suggested that the highest mass alteration occurred at a temperature of 800°C with 78 mins of calcination time.
Źródło:
Journal of Ecological Engineering; 2021, 22, 5; 221-228
2299-8993
Pojawia się w:
Journal of Ecological Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Formation of Boric Acid by Surface Oxidation of Amorphous Boron Powder: Characterization and Quantitative Estimation
Autorzy:
Nandi, A. K.
Ghosh, M.
Newale, S. P.
Jadhav, A. J.
Prasanth, H.
Pandey, R. K.
Powiązania:
https://bibliotekanauki.pl/articles/358160.pdf
Data publikacji:
2012
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
amorphous boron powder
B2O3
boric acid
FTIR
SEM
EDX
Opis:
Amorphous Boron Powder (ABP) is used as a fuel in air breathing propulsion systems due to its high gravimetric and volumetric heat value. ABP is sensitive to air and undergoes slow oxidation during storage and handling, leading to the formation of a boric acid layer on the particle surface. This paper describes an analytical method for the estimation of boric acid in ABP. In-house samples obtained from the pilot plant of this laboratory, as well as commercial samples, were assayed for their boric acid content. The study is substantiated by characterization of the ABP samples by SEM with EDX and FTIR. The ageing characteristics of in-house boron powder was also studied.
Źródło:
Central European Journal of Energetic Materials; 2012, 9, 4; 387-398
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-2 z 2

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