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    Wyświetlanie 1-9 z 9
    Tytuł:
    Pack Siliconizing of Ti6Al4V Alloy
    Autorzy:
    Celebi Efe, G.
    İpek, M.
    Bindal, C.
    Zeytin, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1031464.pdf
    Data publikacji:
    2017-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.65.Lp
    81.65.-b
    Opis:
    In this study, it was aimed to produce titanium silicide layer on Ti6Al4V by a simple, cheap and efficient method of pack siliconizing. Siliconizing was performed in a pack containing a mixture composed of SiO₂ powder as siliconizing source, pure Al powder as a reducer for siliconizing, NH₄Cl as an activator and Al₂O₃ powder as filler, at 1000°C for 8, 10 and 12 hours in open atmospheric furnace. Optical microscope and SEM-EDS studies indicate that the morphology of silicide layers has smooth, dense and layered nature. The presence of phases, confirmed by XRD analyses, reveals that the silicide layers formed at 1000°C are composed of TiSi₂, Ti₃Si₅, TiN, TiO₂ and SiO₂ compounds. Silicide layer thickness was increased with increasing process time and ranged from 7.5 to 9.0 μm. Hardness of silicide layers, measured by Vickers indentation, is over 2100 HV.
    Źródło:
    Acta Physica Polonica A; 2017, 132, 3; 760-762
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization of Fe-Nb-B Base Hardfacing of Steel
    Autorzy:
    Kilinc, B.
    Cegil, O.
    Abakay, E.
    Sen, U.
    Sen, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1311693.pdf
    Data publikacji:
    2014-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.65.Kn
    68.55.J-
    81.65.Lp
    Opis:
    Recently hardfacing by welding has become a commonly used technique for improvement of material performance in extreme (high temperature, impact/abrasion, erosion, etc.) conditions. In the present study, three different alloy compositions of the Fe-Nb-B were used for hardfacing of the AISI 1020 steel by tungsten inert gas welding process and analyzed. The coatings were produced from a mixture of ferrous niobium, ferrous boron and iron powders in the range of - 45 μm particle size with different ratio. The coatings' thickness was set to 2-3 mm on the substrate. Microstructure, phase analysis and hardness of the manufactured hardfacing alloys were characterized. Deposition results indicate good quality thick coating and porosity free of the hardfacings. X-ray diffraction analyses showed that the alloyed layers include iron borides, FeNbB and iron phases. It was shown that surface alloyed layer has composite structure including steel matrix and well distributed boride phases.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 2; 656-658
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Wear Properties of TIG Surface Alloyed Steel with 50%Fe-10%W-40%B Alloy
    Autorzy:
    Abakay, E.
    Kilinc, B.
    Sen, S.
    Sen, U.
    Powiązania:
    https://bibliotekanauki.pl/articles/1401223.pdf
    Data publikacji:
    2015-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.20.Vj
    81.05.Bx
    81.40.Pq
    81.65.Lp
    Opis:
    In the present study, AISI 1020 plain carbon steel was surface alloyed with preplaced 50%Fe-10%W-40%B alloying powders using a tungsten-inert gas (TIG) heat source. Microstructure, hardness, and wear resistance of the surface alloyed layer were investigated. Following the surface alloying, conventional characterization techniques such as optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), and X-ray diffraction analysis (XRD) were used to study the phase and microstructural examinations of the alloyed surfaces. Hardness measurements were performed across the alloyed zones, and wear properties of the alloyed surfaces were evaluated using a ball-on-disc wear test method. Hardness values of the phases formed in the alloyed layer are changing between 620±30 $HV_{0.1}$ and 2095±254 $HV_{0.1}$. The major phases formed in the surface alloyed layer were Fe₂B, FeB and FeW₂B₂. Wear test were realized against Alumina ball under the loads of 2.5 N, 5 N and 10 N at the sliding speed of 0.1 m/s for 250 m sliding distance. The friction coefficient of the 50%Fe-10%W-40%B alloyed steel surface is changing between 0.70 and 0.79 depending on applied loads. The wear rates of the surface alloyed steel ranged from $4.01 \times 10^{-5}$ mm³/m to $4.14 \times 10^{-4}$ mm³/m.
    Źródło:
    Acta Physica Polonica A; 2015, 127, 4; 957-960
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Corrosion Behavior of Nitride and Cr-Al-N Coatings Formed on AISI D2 Steel
    Autorzy:
    Kılınc, B.
    Demirkiran, S.
    Sen, U.
    Sen, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1399749.pdf
    Data publikacji:
    2013-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.65.Kn
    68.55.J-
    81.65.Lp
    Opis:
    In the present work, the corrosion behavior of Cr-Al-N coating formed on the pre-nitrided AISI D2 cold work tool steel by thermo-reactive diffusion technique in the powder mixture consisting of ferro-chromium, aluminum, ammonium chloride and alumina at 1000C for 2 h was investigated. The phases formed in the coating layers were $Cr_2N$, $(Cr,Fe)_2N_{1-x}$, $AlN$, and $Fe_2N$ which were confirmed by X-ray diffraction analysis. The uncoated, nitrided, and Cr-Al-N coated specimens were placed in corrosive media (3.5 wt% salt solution). A standard saturated calomel electrode was used as a reference and graphite as a counter or auxiliary electrode. The effectiveness of the coatings in preventing corrosion was tested in the NaCl solution by electrochemical impedance studies using the Nyquist plots and potentiodynamic studies as well. Conclusively, the application of nitride and Cr-Al-N layers on AISI D2 steel increased its surface hardness and corrosion resistance. The corrosion resistance of Cr-Al-N coatings is higher than that of uncoated and nitrided steels.
    Źródło:
    Acta Physica Polonica A; 2013, 123, 2; 268-270
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Cathodic Electrolytic Plasma Hardening of Steel and Cast Iron Based Automotive Camshafts
    Autorzy:
    Dayanç, A.
    Karaca, B.
    Kumruoğlu, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/1030309.pdf
    Data publikacji:
    2017-03
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.65.Lp
    82.45.Hk
    81.40.Pq
    Opis:
    Cathodic electrolytic plasma hardening is a novel thermochemical surface modification and hardening process, used to increase wear resistance and surface hardness of metallic components in a local area of interest. The heating efficiency is related with the plasma nozzle design, applied current and electrolyte. The nozzle design is also a critical factor for the hardening of complex shapes, such as gears and camshafts. In this work, lobes of camshafts, fabricated from several cast iron and steel grades were hardened by cathodic electrolytic plasma hardening in aqueous carbonate electrolyte, using a specific plasma nozzle. The camshafts were attached to CNC lathe for turning them in the horizontal axis. In order to optimise heating and to achieve the ideal flowing and wetting by the electrolyte of the lobe case, the ceramic ellipse-shaped nozzle outlet was designed. As a result of preliminary studies, external surface of lobes was heated and subsequently quenched by electrolyte. The hardness of processed surface was in the range of 50-60 HRc for the different camshafts. No distortion was observed on the surface of lobes. Hardness depth was measured to be from 0.1 mm to 5 mm for several lobes.
    Źródło:
    Acta Physica Polonica A; 2017, 131, 3; 374-378
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Phase Composition of the Surface Zone of Nitrided Cast Steels and Their Mechanical Properties
    Autorzy:
    Brzózka, K.
    Budzynowski, T.
    Górka, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/1506569.pdf
    Data publikacji:
    2011-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.66.Dk
    81.65.Lp
    81.40.-z
    76.80.+y
    61.05.cp
    68.37.-d
    81.40.Pq
    Opis:
    Conversion electron Mössbauer spectroscopy and structural X-ray diffractometry have been used to study nitrides formation in the surface layer of cast steels subjected previously to low-temperature nitriding. It has been found that creation of iron-nitrogen phases strongly depends on sample composition. Nitrides: $γ^\prime-Fe_{4}N$ and $\epsilon-Fe_{2-3}N$ arise in the course of the nitriding procedure in most investigated cast steels. Moreover, considerable changes in their microstructure and tribological properties occur. The depth profile of nitrides has been derived for selected cast steel.
    Źródło:
    Acta Physica Polonica A; 2011, 119, 1; 28-32
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Wear Behavior of TiAlN and CrAlN Coatings Deposited by TRD Process on AISI D2 Steel
    Autorzy:
    Kılınc, B.
    Cegil, O.
    Sen, S.
    Sen, U.
    Powiązania:
    https://bibliotekanauki.pl/articles/1219208.pdf
    Data publikacji:
    2014-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.15.-z
    46.55.+d
    81.65.Lp
    Opis:
    The wear properties of uncoated, chromium aluminum nitride (CrAlN) and titanium aluminum nitride (TiAlN) coated AISI D2 steel were investigated and compared using ball-on-disc method at 0.3 m/s sliding speed and under the loads of 2.5 N, 5 N, and 10 N against $Si_3N_4$ ball as a counter material. Steel samples were nitrided at 575C for 8 h in the first step of the coating process, and then titanium aluminum nitride coating and chromium aluminum nitride were performed by thermoreactive deposition (TRD) process at 1000C for 2 h. Coated samples were characterized by X-ray diffraction analysis, scanning electron microscopy, microhardness, and ball on disk wear tests. The results of friction coefficient and wear rate of the tested materials showed that the TiAlN coating presents the lowest results.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 2; 362-364
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The law of growth of nitrided layer in 31CrMoV9 steel
    Autorzy:
    Syla, N.
    Aliaj, F.
    Dalipi, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/1068250.pdf
    Data publikacji:
    2016-07
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.05.cp
    81.65.Lp
    Opis:
    The law of growth of nitrided layers produced by gaseous nitriding of 31CrMoV9 alloy steel at different process parameters is described. 31CrMoV9 steel specimens were subjected to nitriding process in ammonia gas at three different temperatures: 510, 550 and 590°C, and for each temperature four different nitriding times were used. This way twelve specimens were produced. Nitrided specimens were investigated with optical microscopy, electron probe micro-analysis and x-ray diffraction. The nitrogen depth concentration profiles, deduced from electron probe micro-analysis, in conjunction with results of optical microscopy, were used to determine the thickness of the nitrided layers, i.e. the diffusion depth of nitrogen. From the dependence of the nitrided layer thickness on process parameters (temperature and time) it was possible to deduce the law that governs the growth of the nitrided layer for 31CrMoV9 alloy steel. Through this law, then, it is possible to predetermine the layer thickness for every real process parameter in nitriding of 31CrMoV9 steel, which is very important for technological applications.
    Źródło:
    Acta Physica Polonica A; 2016, 130, 1; 83-86
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Properties of Cr-Al-N Based Coatings Formed on AISI D2 Steel by Thermo-Reactive Diffusion Technique
    Autorzy:
    Kılınc, B.
    Sen, U.
    Sen, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1399772.pdf
    Data publikacji:
    2013-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.15.-z
    62.20.Qp
    68.55.J-
    81.65.Lp
    Opis:
    In this study, chromium aluminum nitride coating was applied on pre-nitrided AISI D2 steel by the thermo-reactive deposition technique in a powder mixture consisting of ferrochromium, aluminum, ammonium chloride, and alumina at 1000C for 2 h. Steels were gas nitrided for the purpose to enrich the surfaces with nitrogen of the steels in a nitrogen and ammonia atmosphere at 560C for 8 h. The effect of aluminum content in the powder mixture on the Cr-Al-N layer properties was investigated. The coated samples were characterized by X-ray diffraction analysis, scanning electron microscope, and micro-hardness tests. Chromium aluminum nitride layer formed on the pre-nitrided AISI D2 steel was compact and homogeneous. Electron dispersive spectrometer results showed that coating layer includes chromium, aluminum, and nitrogen. X-ray studies showed that the phases formed in the coating layers on the steel surfaces are $Cr_2N$, $(Cr,Fe)_2N_{1-x}$, $AlN$, and $Fe_2N$. The depth of the Cr-Al-N layer ranged from 10.01 ± 1.2 to 13.2 ± 1.7 μm, depending on the aluminum content. The hardness of the coated layers produced on AISI D2 steel are changing from 1743 ± 150 $HV_{0.01}$ to 2067 ± 160 $HV_{0.01}$ depending on bath compositions.
    Źródło:
    Acta Physica Polonica A; 2013, 123, 2; 271-273
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-9 z 9

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