- Tytuł:
- FTIR Study of Nanostructure Perovskite $BaTiO_3$ Doped with Both $Fe^{3+}$ and $Ni^{2+}$ Ions Prepared by Sol-Gel Technique
- Autorzy:
-
Abdel Aal, A.
Hammad, T.
Zawrah, M.
Battisha, I.
Abou Hammad, A. - Powiązania:
- https://bibliotekanauki.pl/articles/1377829.pdf
- Data publikacji:
- 2014-12
- Wydawca:
- Polska Akademia Nauk. Instytut Fizyki PAN
- Tematy:
-
81.20.Fw
81.07.Bc
64.70.kg
61.05.C-
78.30.Ly
81.10.Aj - Opis:
- Pure barium titanate $BaTiO_3 (BT)$ and BT doped with two different transition elements $Fe^{3+}$ and $Ni^{2+}$ at 5 mol.% (BT5Fe and BT5Ni, respectively) as constant concentration in powder form have been prepared by sol-gel method using barium acetate, titanium(IV) n-butoxide, iron and nickel nitrates as precursor materials. The microstructure of BT and the influence of Fe and Ni dopants on it were investigated by X-ray diffraction and Fourier transform infrared spectroscopy. X-ray diffraction shows that tetragonal phase is dominant for pure BT sintered for 4 h at 800°C. Scanning electron microscopy and transmission electron microscopy were used to study surface morphology and particle size distribution for BT5Fe and BT5Ni, respectively. The presence of hydroxyl defects were verified by Fourier transform infrared spectroscopy for $(BaTi_{1-x}Fe_{x}O_{3-x/2}) (BT_xFe)$, where x=0.005, 0.01, 0.05, and 0.07 and $(BaTi_{1-x}Ni_{x}O_{3-x/2}) (BT_xNi)$, where x=0.005, 0.01, 0.03, 0.05, and 0.07.
- Źródło:
-
Acta Physica Polonica A; 2014, 126, 6; 1318-1321
0587-4246
1898-794X - Pojawia się w:
- Acta Physica Polonica A
- Dostawca treści:
- Biblioteka Nauki
Artykuł