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Wyświetlanie 1-15 z 16
Tytuł:
Spark Plasma Sintering of Boron Carbide Ceramics Using Different Sample Geometries and Dimensions
Autorzy:
Cengiz, M.
Yavas, B.
Celik, Y.
Goller, G.
Yucel, O.
Sahin, F.
Powiązania:
https://bibliotekanauki.pl/articles/1216387.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Ev
81.05.Je
Opis:
$B_4C$ ceramics were fabricated by spark plasma sintering technique at 1700°C-1800C for 5 min under applied pressure of 50 MPa under vacuum atmosphere. Two different grades of $B_4C$ powder from H.C. Starck Company namely HP grade and HS grade were used in all related experiments. Effect of sample geometry and dimensions as well as sample thickness on sintering parameters were analyzed. Samples having 5 mm thickness and 50 mm diameter, 8 mm thickness in circular geometries and 50 × 50 square cross-section, 8 mm thickness were fabricated. Using the powder, which provided the densest sample, yttrium oxide $(Y_2O_3)$ was added, mixed and sintered. Optimization of SPS method production parameters for pure $B_4C$ samples and $B_4C$ samples with 5 wt% yttrium oxide additive were accomplished. The effect of geometry on density, Vickers hardness, fracture toughness, and microstructure were examined. The hardness and fracture toughness values of the samples were evaluated by the Vickers indentation technique.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 260-262
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Grain Growth in Sintered Natural Hydroxyapatite
Autorzy:
Hababi, E.
Harabi, A.
Foughali, L.
Chehlatt, S.
Zouai, S.
Mezahi, F.
Powiązania:
https://bibliotekanauki.pl/articles/1401312.pdf
Data publikacji:
2015-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Je
81.20.Ev
Opis:
Hydroxyapatite $(HA: Ca_{10}(PO_4)_6(OH)_2)$ can be synthesized using several methods or manufactured from natural materials such as coral or bone after removal of the organic matter by heating (denoted as NHA). The "in vitro" and "in vivo" studies showed that the natural apatite was well tolerated and has better osteoconductive properties than synthetic HA. In addition, the exploitation of natural source represents an economical way of synthesizing NHA by means of sintering, rather than by sol-gel techniques. For these reasons, the NHA was manufactured from cortical bovine bones in all our studies. Moreover, there has been much effort to improve the mechanical properties of HA by introducing foreign oxides or finding out other alternative processes such as grain growth control. Indeed, encouraging lower AGS instead of exaggerated grain growth may be jugged useful for many applications. Since the works carried out on the correlation between AGS and physico-chemical properties of NHA were very limited, the present study was mainly focused on its grain growth. A carful combination between the main parameters controlling NHA production such as milling techniques, compacting pressure, sintering temperature and holding time may lead to an interesting NHA based bio-ceramics. In this way, a simple and energetically vibratory multidirectional milling system using bimodal distribution of highly resistant ceramics has been used for obtaining sub-micron sized NHA powders. For example, the AGS was ranged between 0.75 and 1.40 μm (using intercept method) when NHA samples were sintered at 1250°C for 15 and 480 min, respectively.
Źródło:
Acta Physica Polonica A; 2015, 127, 4; 1161-1163
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Spark Plasma Sintering of Silicon Carbide Ceramics Using Alumina
Autorzy:
Unlu, M.
Goller, G.
Yucel, O.
Sahin, F.
Powiązania:
https://bibliotekanauki.pl/articles/1216300.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Ev
81.05.Je
Opis:
SiC ceramics were fabricated by spark plasma sintering technique with the use of $Al_2O_3$ additive. The sintering process was carried out at three different temperatures in the range of 1700-1800C applying two different pressures 40 and 80 MPa under vacuum atmosphere. The effect of additive, different temperatures and pressures on densification behaviour, density, Vickers hardness, fracture toughness, and microstructure were examined. The hardness and fracture toughness of the samples were evaluated by the Vickers indentation technique. Microstructure of spark plasma sintered SiC samples were characterized by using scanning electron microscopy technique. The highest value of fracture toughness $5.9 ± 0.2$ MPa $m^{1/2}$ was achieved with the addition of 5 vol.% $Al_2O_3$.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 257-259
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanochemical Modification of V-Mo-Zr Oxide Compositions
Autorzy:
Khalameida, S.
Wieczorek-Ciurowa, K.
Zazhigalov, V.
Powiązania:
https://bibliotekanauki.pl/articles/1375488.pdf
Data publikacji:
2014-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Ev
81.05.Je
81.20.Wk
Opis:
The influence of mechanochemical treatment by high-energy ball milling in two media (water and ethanol) of different $V_{2}O_{5}$/$MoO_{3}$/$ZrO_{2}$ compositions on its structure modification and photocatalytic properties is considered. Milling process in both media leads to final products $Zr(V_{2}O_{7})$ and $Mo_{4}V_{6}O_{25}$. Their subsequent thermal treatment provides to formation of $Zr(MoO_{4})_{2}$ and $V_{2}MoO_{8}$ composition. They show the photocatalytic activity in the dyes degradation process in aqueous solution.
Źródło:
Acta Physica Polonica A; 2014, 126, 4; 963-966
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence on Static Grain Growth and Sinterability of BaO Addition into 8YSZ
Autorzy:
Aktas, B.
Tekeli, S.
Salman, S.
Powiązania:
https://bibliotekanauki.pl/articles/1311666.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Je
81.07.Bc
81.20.Ev
Opis:
In this study, 8 mol.% yttria stabilized cubic zirconia (8YSZ) powders as a matrix material and 0-15 wt% BaO powders as an additive were used in order to determine the effect of BaO addition and amount on the microstructure, sintering and static grain growth properties of the 8YSZ. For these purposes, undoped and BaO-doped 8YSZ specimens were annealed for grain growth at 1400, 1500, and 1600C for 10, 50, and 100 h, respectively. An increase of annealing temperature and holding time resulted in grain growth in all specimens. The grain size of the 8YSZ decreased with the higher level of BaO added. A limited amount of BaO dissolved in 8YSZ, and insoluble BaO reacted with $ZrO_2$ at high sintering temperature and generated the $BaZrO_3$ second sphase compound. Energy dispersive X-ray spectroscopy results showed that the $BaZrO_3$ second phase segregated at the surrounding grains and grain boundaries of the 8YSZ. These $BaZrO_3$ second phases had a pinning effect at the grain boundaries and prevented the migration of the grain boundaries of the 8YSZ. In conclusion, the grain growth results showed that the grain growth in the BaO-doped 8YSZ specimens was controlled by a solid solution drag mechanism.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 652-655
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electrical Conductivity of Boron Oxide-Doped Yttria-Stabilized Cubic Zirconia (8YSZ)
Autorzy:
Aktas, B.
Tekeli, S.
Powiązania:
https://bibliotekanauki.pl/articles/1401428.pdf
Data publikacji:
2015-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Je
81.20.Ev
82.47.Ed
Opis:
The effect of B₂O₃ addition on the electrical conductivity of 8 mol% yttria-stabilized cubic zirconia (8YSZ) was investigated by analyzing the impedance spectra of 0-10 wt.% B₂O₃-doped 8YSZ powders prepared via a colloidal process. The doped powders were then pelletized under a pressure of 200 MPa, and then sintered at 1400°C for 10 h. Measurements of the electrical conductivity of the sintered specimens within a frequency range of 100 mHz-13 MHz, and temperature range of 300-800°C, revealed an increase in conductivity with increasing temperature. Furthermore, the grain interior, grain boundary and total conductivity of 8YSZ were found to be enhanced by the addition of 1 wt.% B₂O₃. This is attributed to the lattice distortion created by the addition of $B^{3+}$ cations to the 8YSZ lattice, which leads to an increase in the concentration of oxygen vacancies, thus ultimately resulting in an enhanced electrical conductivity.
Źródło:
Acta Physica Polonica A; 2015, 127, 4; 1380-1383
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of Transparent Yttria Ceramics by Spark Plasma Sintering
Autorzy:
Korkmaz, E.
Sahin, F.
Powiązania:
https://bibliotekanauki.pl/articles/1032083.pdf
Data publikacji:
2017-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Je
81.20.Ev
81.40.Tv
42.70.Hj
Opis:
Rapid densification of yttria (Y₂O₃) ceramics without sintering aids via spark plasma sintering at relatively low temperature of 1300°C for 40 minutes at two-step pressure profile, followed by post-annealing at 1050°C for 6 hours in air was attempted. Effect of preload pressure on microstructure, Vickers hardness, fracture toughness and optical in-line transmittance was investigated. Densification during spark plasma sintering did not involve any phase transformation and all phases have shown cubic structure according to X-ray analysis. The highest hardness and fracture toughness value was recorded to be 7.60±0.18 GPa and 1.16±0.07 MPa m^{1/2} with 10 MPa preload and 100 MPa final load. In addition to this, the highest transmittance with a value of 76.7% at a wavelength of 2000 nm was obtained when studied with 10 MPa preload and 100 MPa final load.
Źródło:
Acta Physica Polonica A; 2017, 131, 3; 460-462
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
B₄C-CNT Produced by Spark Plasma Sintering
Autorzy:
Apak, B.
Sahin, F.
Powiązania:
https://bibliotekanauki.pl/articles/1401275.pdf
Data publikacji:
2015-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Ev
81.05.Je
81.05.U-
88.30.rh
Opis:
H.C. Starck HS Grade boron carbide (B₄C) powders with multi-walled carbon nanotube (CNT) were sintered by Spark Plasma Sintering (SPS) method in a vacuum atmosphere to obtain highly dense and fine grained final ceramic products. Powder mixtures were densified by SPS at 1650 and 1725°C using 40 MPa pressure for 5 min. The effects of heating rate, spark plasma sintering temperature and CNT additive on density, hardness, fracture toughness and microstructures of B₄C-CNT samples are investigated. Density measurements were carried out using Archimedes method. Hardness and fracture toughness were examined by Vickers indentation technique. Scanning Electron Microscope (SEM) was used to observe microstructural investigation.
Źródło:
Acta Physica Polonica A; 2015, 127, 4; 1029-1031
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Co₃O₄ on the Fracture Toughness and Microstructure of Yttria-Stabilized Cubic Zirconia (8YSZ)
Autorzy:
Aktas, B.
Tekeli, S.
Powiązania:
https://bibliotekanauki.pl/articles/1401433.pdf
Data publikacji:
2015-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Je
81.20.Ev
81.40.Np
82.47.Ed
Opis:
The effects of the addition of Co₃O₄ to yttria-stabilized zirconia (8YSZ) on fracture toughness and microstructure was investigated using micro-indentation and scanning electron microscopy (SEM). Undoped and 1-15 wt.% Co₃O₄-doped 8YSZ powders were prepared using a colloidal process and then pelletized under a pressure of 200 MPa. The 8YSZ specimens were sintered at 1400°C for 1 h. SEM results showed that Co₃O₄ precipitated as a secondary phase among the primary 8YSZ grains. Furthermore, because of the presence of Co₃O₄ secondary phases at the grain boundaries of 8YSZ, the grain sizes of the 8YSZ samples increased with the addition of 1-15 wt.% Co₃O₄. The fracture toughness values of the undoped and 1 wt.% Co₃O₄-doped 8YSZ were determined to be 1.64 and 2.86 MPa $m^{1//2}$, respectively, indicating the fracture toughness of 8YSZ increased in 1 wt.% Co₃O₄ addition. The fracture toughness of 8YSZ increased upon the addition of 1 wt.% Co₃O₄.
Źródło:
Acta Physica Polonica A; 2015, 127, 4; 1384-1387
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure and Hyperfine Interactions in Aurivillius $Bi_{9}Ti_{3}Fe_{5}O_{27}$ Conventionally Sintered Compound
Autorzy:
Mazurek, M.
Lisińska-Czekaj, A.
Surowiec, Z.
Jartych, E.
Czekaj, D.
Powiązania:
https://bibliotekanauki.pl/articles/1506653.pdf
Data publikacji:
2011-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Je
81.20.Ev
31.30.Gs
76.80.+y
Opis:
The structure and hyperfine interactions in the $Bi_{9}Ti_{3}Fe_{5}O_{27}$ Aurivillius compound were studied using X-ray diffraction and Mössbauer spectroscopy. Samples were prepared by the conventional solid-state sintering method at various temperatures. An X-ray diffraction analysis proved that the sintered compounds formed single phases at temperature above 993 K. Mössbauer measurements have been carried out at room and liquid nitrogen temperatures. Room-temperature Mössbauer spectrum of the $Bi_{9}Ti_{3}Fe_{5}O_{27}$ compound confirmed its paramagnetic properties. However, low temperature measurements revealed the additional paramagnetic phase besides the antiferromagnetic one.
Źródło:
Acta Physica Polonica A; 2011, 119, 1; 72-74
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Sintering Behavior and Machinability Properties of Industrial Waste Materials Based Glass-Ceramics
Autorzy:
Bayrak, G.
Ercenk, E.
Yilmaz, S.
Powiązania:
https://bibliotekanauki.pl/articles/1401375.pdf
Data publikacji:
2015-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Fs
81.05.Je
81.05.Mh
81.20.Ev
81.20.Wk
Opis:
Glass-ceramics were produced by sintering method from industrial waste materials such as fly ash, blast furnace slag and boron waste. The sintering behavior and machinability of glass-ceramic compositions were investigated. Additives were added to waste materials for enhancement of machinability and sintering properties. All starting materials were mixed by ball milling for 2 h using alumina media. The mixed and milled powders were sieved to grain sizes smaller than 75 μm and pressed at 100 MPa. The pressed samples were sintered at 900°C, 1000°C and 1100°C for 1 h in an electric furnace using a heating rate of 5°C/min. Some characterization tests such as X-ray diffraction (XRD), scanning electron microscopy (SEM) and machinability tests were performed on sintered samples. The results indicated that all samples exhibit good sintering and machinability properties.
Źródło:
Acta Physica Polonica A; 2015, 127, 4; 1346-1348
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effect of Perlite Addition on Erosive Wear Behavior of Alumina Ceramics
Autorzy:
Tas, S.
Ercenk, E.
Yilmaz, S.
Powiązania:
https://bibliotekanauki.pl/articles/1182871.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Je
81.05.Mh
46.55.+d
62.20.F-
81.20.Ev
Opis:
In this study, the effects of perlite addition on mechanical properties and wear resistance of alumina ceramics were investigated. Alumina powders including perlite 5%, 10%, 15%, 20% and perlite free were prepared. These powders were shaped as rectangular by using uniaxial pressing system under the load of 100 MPa. The samples were sintered at 1400°C-1550C for 2 h and were subjected to some mechanical tests such as hardness and fracture toughness. X-ray diffraction analysis was employed to determine the crystalline phases. Bulk densities of the samples were measured. In addition, erosive wear test was performed to investigate the erosive wear resistance of the samples. The wear test results were presented depending on different sliding speed and sintering temperature. These results showed that perlite addition has a positive effect on erosive wear resistance of the alumina ceramics, generally.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 632-634
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Processing, Microstructure and Dielectric Properties of the $Bi_5Ti_3FeO_{15}$ Ceramic
Autorzy:
Rymarczyk, J.
Dercz, G.
Ilczuk, J.
Powiązania:
https://bibliotekanauki.pl/articles/1811567.pdf
Data publikacji:
2008-12
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
77.84.-s
81.20.Ev
81.05.Je
61.05.cp
68.37.Ef
Opis:
The aim of the present work is the analysis of microstructure, dielectric permittivity and thermal properties analysis of $Bi_5Ti_3FeO_{15}$ ceramics obtained by two methods. The studied $Bi_5Ti_3FeO_{15}$ ceramics were prepared by conventional synthesis and hot uniaxial pressing reaction from the conventional mixture of oxides, viz. $TiO_2$, $Fe_2O_3$, $Bi_2O_3$. The studied material has layered perovskite like structures, first described by Aurivillius in 1949 and Subbaro in 1969. The ceramic $Bi_5Ti_3FeO_{15}$ is known to contain a series of compounds with the general formula: $Bi_{m+1}Fe_{m-3}Ti_3O_{3m+3}$. The X-ray diffraction methods were used for qualitative phase analysis of studied samples. The morphology was analyzed by scanning electron microscopy method. The thermal properties of the studied materials were measured using the differential thermal analysis at a constant heating rate of 15 K/min under an argon protective atmosphere. Thermal dependence of dielectric permittivity was studied between room temperature and 1137 K.
Źródło:
Acta Physica Polonica A; 2008, 114, 6A; A-191-A-197
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Sintering Behavior and Machinability in Mica Glass-Ceramic of the System $SiO_2-Al_2O_3-MgO-K_2O-B_2O_3-F$
Autorzy:
Ercenk, E.
Yilmaz, S.
Powiązania:
https://bibliotekanauki.pl/articles/1293704.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
68.37.Hk
81.20.Ev
81.20.Wk
81.05.Je
81.05.Mh
Opis:
Mica glass-ceramic was prepared by sintering method from in the $SiO_2-Al_2O_3-MgO-K_2O-B_2O_3-F_2$ system. The sintering behavior and machinability of a glass-ceramic composition were examined. The starting materials were mixed and milled in an alumina ball mill for 2 h. Then the powders were sieved to obtain grain sizes smaller than 75 μm. For the shaping process, disc samples were prepared by pressing at 100 MPa. The pressed discs were sintered at temperatures in the range from 900 to 1200C for 2 h in an electric furnace using a heating rate of 5°C/min. X-ray diffraction analysis, scanning electron microscopy, and machinability tests for characterization were performed on sintered samples. The results showed that all samples exhibited similar phases formation and good machinability.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 629-631
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of CaO Addition on the Sintering Behaviour of Anorthite Formed from Kaolin and CaO
Autorzy:
Ouali, A.
Sahnoune, F.
Belhouchet, H.
Heraiz, M.
Powiązania:
https://bibliotekanauki.pl/articles/1032557.pdf
Data publikacji:
2017-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Je
81.05.Mh
81.20.Ev
81.70.Pg
65.40.De
65.60.+a
Opis:
Thermal reactions and sintering behavior of kaolin DD3 (Djebel Debbagh, Algeria) and CaO mixtures to obtain dense anorthite ceramics were investigated. Mixed powders were uniaxially pressed and fired between 850 and 1150°C. Firing the pressed specimens yielded a dense anorthite ceramics. The sintered density increased with increase of CaO content and reached the maximum value of 2.57 g/cm³ for the composition containing 10 wt% CaO and fired at 1150°C. Their coefficient of linear expansion of the sintered samples at 1100°C decreases with the addition of CaO. X-ray diffraction experiments carried out on the samples containing varied amount of CaO and fired at the temperatures higher than 1000°C for 2 h showed the presence of only anorthite phase.
Źródło:
Acta Physica Polonica A; 2017, 131, 1; 159-161
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 16

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