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Wyświetlanie 1-3 z 3
Tytuł:
Study of Ga$\text{}_{2}$O$\text{}_{3}$ Nanobelts Synthesized by the Thermal Annealing of GaN Powders
Autorzy:
Kim, Hyoun Woo
Kim, Nam Ho
Powiązania:
https://bibliotekanauki.pl/articles/2041772.pdf
Data publikacji:
2005-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.07.-b
81.05.Hd
Opis:
We synthesized the uniform monoclinic gallium oxide (Ga$\text{}_{2}$O$\text{}_{3}$) nanobelts by a simple thermal annealing of GaN powders. The as-syn-thesized nanobelts were rectangular in cross-sectional shape with width ranging from 100 to 700 nm. The length direction of the nanobelt was along [010]. Photoluminescence measurement under excitation at 325 nm showed that the Ga$\text{}_{ }$2O$\text{}_{3}$ nanobelts had a blue emission at around 454 nm.
Źródło:
Acta Physica Polonica A; 2005, 107, 2; 346-350
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanochemically Synthesized CuFeSe₂ Nanoparticles and Their Properties
Autorzy:
Dutková, E.
Škorvánek, I.
Sayagués, M.
Zorkovská, A.
Kováč, J.
Baláž, P.
Powiązania:
https://bibliotekanauki.pl/articles/1032137.pdf
Data publikacji:
2017-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Hd
81.07.Wx
81.20.Wk
Opis:
The mechanochemical synthesis of nanocrystalline CuFeSe₂ particles prepared by high-energy milling in a planetary mill in an argon atmosphere from copper, iron, and selenium for 60 min is reported for the first time. The CuFeSe₂ nanoparticles crystallize in tetragonal structure with mean crystallite size of about 32±1 nm. High resolution transmission electron microscopy measurements confirmed the presence of agglomerates which are formed by small nanocrystalline domains (5-40 nm). The magnetic data revealed that paramagnetic CuFeSe₂ nanoparticles coexist with a small amount of ferromagnetic impurities at room temperature. The magnetic transition towards a weak ferromagnetic or ferrimagnetic behavior occurs in CuFeSe₂ at approximately 79 K. The band gap of the CuFeSe₂ particles is 0.95 eV which is wider than the band gap in bulk materials (0.16 eV), which could be in many aspects of application more beneficial.
Źródło:
Acta Physica Polonica A; 2017, 131, 4; 1156-1158
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanochemically Synthesized Nanocrystalline $Sb_2S_3$ Particles
Autorzy:
Dutková, E.
Sayagués, M.
Real, C.
Zorkovská, A.
Baláž, P.
Šatka, A.
Kováč, J.
Ficeriová, J.
Powiązania:
https://bibliotekanauki.pl/articles/1375343.pdf
Data publikacji:
2014-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Hd
81.07.Bc
81.20.Wk
Opis:
Nanocrystalline $Sb_2S_3$ particles have been synthesized from Sb and S powders by high-energy milling in a planetary mill using argon protective atmosphere. X-ray diffraction, particle size analysis, scanning electron microscopy, energy dispersive X-ray spectroscopy, transmission electron microscopy, electron diffraction, high resolution transmission electron microscopy, UV-VIS, and differential scanning calorimetry methods for characterization of the prepared particles were applied. The powder X-ray diffraction pattern shows that $Sb_2S_3$ nanocrystals belong to the orthorhombic phase with calculated crystallite size of about 36 nm. The nanocrystalline $Sb_2S_3$ particles are constituted by randomly distributed crystalline nanodomains (20 nm) and then these particles are forming aggregates. The monomodal distribution of $Sb_2S_3$ particles with the average hydrodynamic parameter 210 nm was obtained. The quantification of energy dispersive X-ray spectroscopy analysis peaks give an atomic ratio of 2:3 for Sb:S. The optical band gap determined from the absorption spectrum is 4.9 eV, indicating a considerable blue shift relative to the bulk $Sb_2S_3$. Differential scanning calorimetry curves exhibit a broad exothermic peak between 200 and 300°C, suggesting recovery processes. This interpretation is supported by X-ray diffraction measurements that indicate a 23-fold increase of the crystallite size to about 827 nm as a consequence of application of high temperature process. The controlled mechanochemical synthesis of $Sb_2S_3$ nanoparticles at ambient temperature and atmospheric pressure remains a great challenge.
Źródło:
Acta Physica Polonica A; 2014, 126, 4; 943-946
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-3 z 3

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