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    Wyświetlanie 1-7 z 7
    Tytuł:
    Influence of Type of Alcohol as the Process Control Agent on Ti-20Ta-20Nb Alloy Preparation by Mechanical Alloying
    Autorzy:
    Adamek, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/1375069.pdf
    Data publikacji:
    2014-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.07.+b
    81.40.+z
    Opis:
    In this paper the influence of alcohols as the process control agents on β-Ti alloys preparation using mechanical alloying process was investigated. Three types of alcohols: methanol, ethanol and isopropanol were used in mechanical alloying of Ti-20Ta-20Nb. Pure Ti, Ta, Nb powders and process control agents were alloyed under argon atmosphere in shaker type mill (Spex 8000). Using X-ray diffraction technique, there has been observed the β phase formation after 3 h of mechanical alloying process. Using alcohols as process control agent it is possible to obtain nanocrystalline powders of titanium alloys. The milled powder was sintered in vacuum using hot pressing with high frequency induction heating. It has been shown that sintering process of powders prepared with alcohols as process control agents results in oxides and carbides formation in the alloy structure. Moreover some part of alcohol could evaporate leaving open spaces which results in relatively high porosity of the sinters.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 4; 875-878
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Mechanical Alloying of Ti-20Ta-20Nb-(10÷20)Mg Alloys
    Autorzy:
    Adamek, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/1374912.pdf
    Data publikacji:
    2014-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.07.+b
    81.40.+z
    Opis:
    In this paper preparation of new β-Ti alloys using mechanical alloying process has been shown. β -Ti alloys are the best metallic biomaterials because of their excellent properties: biocompatibility, low Young moduli and corrosion resistance. Ti-20Ta-20Nb biocompatible alloy was investigated. Mg was used as alloying element, as well (10, 15 and 20 wt%). Pure Ti, Nb, Ta and Mg powders were alloyed under argon atmosphere in shaker type mill (Spex 8000). There was no problem with cold welding in the mechanical alloying of titanium alloys containing Mg. In the paper a possibility of porous materials preparation by sintering in temperature higher than boiling temperature of Mg has been shown. This thermal dealloying method could be an alternative to space holder technique.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 4; 871-874
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Laser Assisted Au Nanocrystal Formation in Conditions of Surface Plasmon Resonance
    Autorzy:
    Fedorenko, L.
    Snopok, B.
    Yusupov, M.
    Lytvyn, O.
    Burlachenko, Yu.
    Powiązania:
    https://bibliotekanauki.pl/articles/1807920.pdf
    Data publikacji:
    2009-06
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.16.Mk
    81.07.-b
    Opis:
    The possibility of the calibrated Au nanoparticles formation in conditions of surface plasmon resonance at irradiation of the Au film/glass structure by pulsed $YAG:Nd^{3+}$-laser radiation is investigated. Sizes of the Au fragments and their surface distribution were studied by the atom force microscopy. The effect of Au nanofragmentation was observed only at the second harmonic irradiation (λ = 0.532 μm). The large difference in the average values of Au nanoparticles sizes -[δ] and distributions between created in the resonance conditions, R = $R_{min}$, -[δ] ∼ 80 nm and in case out of resonance R ≠ $R_{min}$, -[δ] ∼ 1350 nm was established. A high degree of the height sizes homogeneity of Au nanoparticles has been shown by the histogram obtained from the atom force microscopy data. There was verified the conclusion about determining contribution of the plasmon subsystem field in nanofragmentation process of the Au film in the SPR conditions at high laser levels.
    Źródło:
    Acta Physica Polonica A; 2009, 115, 6; 1075-1077
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Solvent effects on the optical properties of PEG-SH and CTAB capped gold nanorods
    Autorzy:
    Wielgus, M.
    Gordel, M.
    Samoć, M.
    Bartkowiak, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/1058757.pdf
    Data publikacji:
    2016-12
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.20.-e
    81.05.Bx
    81.07.-b
    Opis:
    Cetyltrimethylammonium bromide (CTAB) and (11-mercaptoundecyl)tetra(ethylene glycol) (PEG-SH) capped gold nanorods were prepared and dispersed in water and dimethyl sulfoxide (DMSO). Transmission electron microscopy images reveal that changing the solvent from water to DMSO cause that nanoparticles tend to organize (PEG-SH ligand) or aggregate (CTAB ligand). UV-vis absorbance spectra reveal that ligand as well as solvent exchange cause positive solvatochromic shifts and changes in the relative extinction values. After the transfer of nanorods from a solvent of lower to higher refraction index a red shift of the longitudinal surface plasmon resonance band is observed. This effect is more pronounced in the case of PEG-SH capped nanorods. Time resolved pump-probe measurements revealed that both ligand and solvent exchange influence the excited state relaxation times, however, a more pronounced change is induced by the ligand exchange. Two-photon excited fluorescence spectra of PEG-SH covered nanorods showed a slight intensity increase when moving from water to DMSO solvent.
    Źródło:
    Acta Physica Polonica A; 2016, 130, 6; 1380-1384
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Mechanical and Structural Properties of High Purity Al Processed by ECAP
    Autorzy:
    Kvačkaj, T.
    Kočiško, R.
    Pokorný, I.
    Bidulská, J.
    Kvačkaj, M.
    Kováčová, A.
    Bidulský, R.
    Lityńska-Dobrzyńska, L.
    Dutkiewicz, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1418957.pdf
    Data publikacji:
    2012-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.07.-b
    81.20.Hy
    81.40.-z
    Opis:
    The mechanical properties and substructure formation of high purity aluminium (99.999%) processed by severe plastic deformation method (equal channel angular pressing) were studied. The equal channel angular pressing process was carried out at room temperature by route C (sample rotation around the axis about 180° after each pass) in a die with two channels intersecting at an angle of Φp = 90. The softening mechanism through dynamic recovery was recognized up to 6th equal channel angular pressing pass, however, after that the mechanical strengthening was revealed. The samples after equal channel angular pressing processing were annealed in different temperature and time conditions. The influence of annealing temperature and time on microhardness as well as diameter of grain size were investigated in samples processed by the 4th equal channel angular pressing pass.
    Źródło:
    Acta Physica Polonica A; 2012, 122, 3; 557-560
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Post SPD Materials Recovery in Thermal Exposition
    Autorzy:
    Kvačkaj, T.
    Kováčová, A.
    Kočiško, R.
    Powiązania:
    https://bibliotekanauki.pl/articles/1402127.pdf
    Data publikacji:
    2015-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.07.-b
    81.20.Hy
    81.40.Cd
    Opis:
    The mechanical and thermo-physical properties of Cu-Cr-Zr alloys in dependence on processing conditions were studied. The processing conditions consisted of solution annealing at temperature of 1020°C for 60 min followed by water quenching. This was followed by one equal channel angular pressing pass carried out at ambient temperature, ageing treatment ($T_{AT}$∈ (20;480⟩°C, $t_{AT}$∈ ⟨30;150⟩ min) and cooling in water. The maximal strengthening effect coming from dislocations & grain size refinement & precipitation strengthening of ΔHV0.1=130 was achieved at $T_{AT}$=480°C and for $t_{AT}$=120 min. From differential scanning calorimetry analysis, two partial exothermal peaks were recognized and classified as major and minor, these peaks are used to determination the stored energy coming from recrystallization and precipitation ($\Delta H_R$ and $\Delta H_P$). The maximal value in stored energy of $H_{1 \times \text{ECAP}} = 2.923 J//g$ was obtained after 1st ECAP pass.
    Źródło:
    Acta Physica Polonica A; 2015, 128, 4; 689-692
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Particle Impact Angle, Erodent Particle Size and Acceleration Pressure on the Solid Particle Erosion Behavior of 3003 Aluminum Alloy
    Autorzy:
    Yıldıran, Y.
    Avcu, E.
    Şahin, A.
    Fidan, S.
    Yetiştiren, H.
    Sınmazçelik, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/1195082.pdf
    Data publikacji:
    2014-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.70.-q
    68.35.B-
    68.35.-p
    42.79.Ls
    68.37.Hk
    07.85.Nc
    Opis:
    This study aims to examine solid particle erosion behavior of 3003 aluminum alloy. 3003 aluminum alloy samples were eroded in erosion test rig under various particle impingement angles (15°, 30°, 45° and 60°) and acceleration pressures (1.5, 3 and 4 bar) by using 80 mesh and 180 mesh sized erodent particles (garnet). The erosion rates of aluminum alloy samples were calculated depending on the erosion parameters. The erosion rates of the samples have varied dramatically depending on particle impingement angle, acceleration pressure and erodent particle size. The maximum erosion rates were observed at 15° impingement angles at all acceleration pressures and particle sizes. Moreover, erosion rates of the samples were increased with increases in acceleration pressure at all particle impingement angles and particle sizes. On the other hand, erosion rates of the samples decrease with increase in erodent particle sizes. Hence, maximum erosion was observed when the aluminum alloy eroded at 15° impingement angle and 4 bar pressure by using 180 mesh erodent particles. Finally, the eroded surfaces of the samples were analyzed by using scanning electron microscope. The surfaces of the samples were also investigated by using energy dispersive X-ray analysis in scanning electron microscopy studies. Microcutting and microploughing erosion mechanisms were observed at 15° and 30° impingement angles, while deep cavities and valleys formed due to plastic deformation were observed at 45° and 60° impingement angles. Moreover, embedded erodent particles were clearly detected on the surfaces of the samples by energy dispersive X-ray analysis.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 2; 523-525
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-7 z 7

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