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Wyświetlanie 1-4 z 4
Tytuł:
On the Structural Phase Transition in a Perovskite-Type Diaminopropanetetrachlorocuprate(II) NH₃(CH₂)₃NH₃CuCl₄ Crystal
Autorzy:
Czupiński, O.
Ingram, A.
Kostrzewa, M.
Przesławski, J.
Czapla, Z.
Powiązania:
https://bibliotekanauki.pl/articles/1033438.pdf
Data publikacji:
2017-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
62.20.D-
77.22.Gm
78.70.Bj
Opis:
Chemical preparation, differential scanning calorimetry and thermal stability differential thermal gravimetry studies, positron annihilation lifetime investigations, optical observations as well as electric properties of the NH₃(CH₂)₃NH₃CuCl₄ crystal are presented. On the basis of the differential scanning calorimetry response the structural phase transition of the first order was observed at 436 K. The enthalpy and entropy of the phase transition are equal to 1120 J/mol and 2.57 J/(mol K), respectively. Differential thermal analysis and thermogravimetric analysis studies confirmed the phase transition at 436 K and one can conclude the chemical and thermal stability of the compound up to about 480 K. Optical observations showed a continuous change of colour from yellow to dark brown above the phase transition to 436 K. Dielectric measurements showed a significant increase of conductivity upon approaching the phase transition regions, with a significant increase above the phase transition temperature. An activation energy dependent on the temperature range, and different for each particular phase, is obtained from measurements of complex impedance.
Źródło:
Acta Physica Polonica A; 2017, 131, 2; 304-310
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Defects in Ultra-Fine Grained Mg and Mg-Based Alloys Prepared by High Pressure Torsion Studied by Positron Annihilation
Autorzy:
Čížek, J.
Procházka, I.
Smola, B.
Stulíková, I.
Kužel, R.
Matěj, Z.
Cherkaska, V.
Islamgaliev, R.
Kulyasova, O.
Powiązania:
https://bibliotekanauki.pl/articles/2043304.pdf
Data publikacji:
2005-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
79.60.Jv
61.72.-y
Opis:
Despite the favourable strength and thermal stability, a disadvantage of the Mg-based alloys consists in a low ductility. Recently it has been demonstrated that ultra fine grained metals with grain size around 100 nm can be produced by high pressure torsion. A number of ultra fine grained metals exhibit favourable mechanical properties consisting in a combination of a very high strength and a significant ductility. For this reason, it is highly interesting to examine microstructure and physical properties of ultra fine grained Mg-based light alloys. Following this purpose, microstructure investigations and defect studies of ultra fine grained pure Mg and ultra fine grained Mg-10%Gd alloy prepared by high pressure torsion were performed in the present work using positron annihilation spectroscopy combined with X-ray diffraction, TEM observations, and microhardness measurements. Positrons are trapped at dislocations in Mg and Mg-10%Gd alloy deformed by high pressure torsion. A number of dislocations increases with the radial distance r from the centre to the margin of the sample. No microvoids (small vacancy clusters) were detected. Mg-10%Gd alloy deformed by high pressure torsion exhibits a homogeneous ultra fine grained structure with a grain size around 100 nm and high dislocations density. On the other hand, pure Mg deformed by high pressure torsion exhibits a binomial type of structure which consists of "deformed regions" with ultra fine grained structure and a high dislocation density and dislocation-free "recovered regions" with large grains. It indicates a dynamic recovery of microstructure during high pressure torsion processing.
Źródło:
Acta Physica Polonica A; 2005, 107, 5; 738-744
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ultra Fine-Grained Metals Prepared by Severe Plastic Deformation: A Positron Annihilation Study
Autorzy:
Čížek, J.
Procházka, I.
Kužel, R.
Matĕj, Z.
Cherkaska, V.
Cieslar, M.
Smola, B.
Stulíková, I.
Brauer, G.
Anwand, W.
Islamgaliev, R. K.
Kulyasova, O.
Powiązania:
https://bibliotekanauki.pl/articles/2043303.pdf
Data publikacji:
2005-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
79.60.Jv
Opis:
Recent investigations of ultra fine-grained metals (Cu, Fe, Ni) performed within a Prague-Rossendorf-Ufa collaboration will be reviewed. The specimens were prepared by severe plastic deformation: the high-pressure torsion and equal channel angular pressing. Positron annihilation spectroscopy was used as the main method including (i) the conventional lifetime and the Doppler broadening measurements with $\text{}^{22}$Na and (ii) the slow-positron implantation spectroscopy with the Doppler broadening measurement. Other methods were also involved: transmission electron microscopy, X-ray diffraction, and microhardness. First, the mean grain size was determined and defects were identified in the as-deformed materials. Defects concentration and spatial distribution were studied in detail. Dislocations situated in distorted regions along grain boundaries, and a few-vacancy clusters distributed homogeneously inside dislocations-free grains, were observed in the ultra fine-grained Cu, Fe, and Ni. Subsequently, the thermal evolution of the ultra fine-grained structures during isochronal annealing was studied.
Źródło:
Acta Physica Polonica A; 2005, 107, 5; 745-752
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positronium for antihydrogen production in the AEGIS experiment
Autorzy:
Consolati, G.
Aghion, S.
Amsler, C.
Bonomi, G.
Brusa, R.
Caccia, M.
Caravita, R.
Castelli, F.
Cerchiari, G.
Comparat, D.
Demetrio, A.
Di Noto, L.
Doser, M.
Evans, C.
Fanì, M.
Ferragut, R.
Fesel, J.
Fontana, A.
Gerber, S.
Giammarchi, M.
Gligorova, A.
Guatieri, F.
Haider, S.
Hinterberger, A.
Holmestad, H.
Kellerbauer, A.
Khalidova, O.
Krasnicky, D.
Lagomarsino, V.
Lansonneur, P.
Lebrun, P.
Malbrunot, C.
Mariazzi, S.
Marton, J.
Matveev, V.
Mazzotta, Z.
Müller, S.
Nebbia, G.
Nedelec, P.
Oberthaler, M.
Pacifico, N.
Pagano, D.
Penasa, L.
Petracek, V.
Prelz, F.
Prevedelli, M.
Ravelli, L.
Rienaecker, B.
Robert, J.
Røhne, O.
Rotondi, A.
Sandaker, H.
Santoro, R.
Smestad, L.
Sorrentino, F.
Testera, G.
Tietje, I.
Widmann, E.
Yzombard, P.
Zimmer, C.
Zmeskal, J.
Zurlo, N.
Powiązania:
https://bibliotekanauki.pl/articles/1057954.pdf
Data publikacji:
2017-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
04.80.Cc
07.77.-n
36.10.Dr
78.70.Bj
Opis:
The primary goal of the Antihydrogen Experiment: Gravity, Interferometry, Spectroscopy (AEGIS) collaboration is to measure for the first time precisely the gravitational acceleration of antihydrogen, H̅, a fundamental issue of contemporary physics, using a beam of antiatoms. Indeed, although indirect arguments have been raised against a different acceleration of antimatter with respect to matter, nevertheless some attempts to formulate quantum theories of gravity, or to unify gravity with the other forces, consider the possibility of a non-identical gravitational interaction between matter and antimatter. We plan to generate H̅ through a charge-exchange reaction between excited Ps and antiprotons coming from the Antiproton Decelerator facility at CERN. It offers the advantage to produce sufficiently cold antihydrogen to make feasible a measurement of gravitational acceleration with reasonable uncertainty (of the order of a few percent). Since the cross-section of the above reaction increases with n⁴, n being the principal quantum number of Ps, it is essential to generate Ps in a highly excited (Rydberg) state. This will occur by means of two laser excitations of Ps emitted from a nanoporous silica target: a first UV laser (at 205 nm) will bring Ps from the ground to the n=3 state; a second laser pulse (tunable in the range 1650-1700 nm) will further excite Ps to the Rydberg state.
Źródło:
Acta Physica Polonica A; 2017, 132, 5; 1443-1449
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-4 z 4

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