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    Wyświetlanie 1-6 z 6
    Tytuł:
    Spectroscopic Studies of Polyoxometalates and their Complexes with Lanthanide(III) Ions in Solution
    Autorzy:
    Lis, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1945607.pdf
    Data publikacji:
    1996-08
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    42.62.Hk
    78.40.-q
    78.40.Ha
    78.55.-m
    Opis:
    The results of investigations related to physico-chemical properties, synthesis and structure of polyoxometalates and their lanthanide(III) complexes are briefly reviewed. Useful techniques for the verification of polyoxometalate compositions and the determination of components are compared. Complexation of metal ions, especially of lanthanide(III) ions, with polyoxometalates using absorption (in the UV-visible and the near IR region) and luminescence spectroscopy methods are presented. Absorption hypersensitive transitions of certain lanthanide(III) ions and laser-induced europium(III) ion luminescence spectroscopy are shown to be useful in complexation investigations. The significance of some polyoxometalate complexes as potential magnetic resonance imaging agents and in biological studies as antiviral agents are discussed.
    Źródło:
    Acta Physica Polonica A; 1996, 90, 2; 275-283
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Spectroscopic Characterization of Ethylenediamine-di(o-hydroxyphenyl)acetic Acid and its Complexes with Lanthanide(III) Ions
    Autorzy:
    Hnatejko, Z.
    Lis, S.
    Elbanowski, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1945635.pdf
    Data publikacji:
    1996-08
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.55.-m
    42.62.Hk
    78.40.Ha
    78.40.-q
    Opis:
    Binding properties of ethylenediaminedi(o-hydroxyphenyl)acetic acid (EHPG) with lanthanide(III) ions were studied using spectroscopic methods. Luminescence intensity and lifetime of the Tb(III) ion were measured in a wide pH range in order to characterize the Ln-EHPG complexation. The calculated hydration number of the Tb-EHPG system proved the replacement of six water molecules by the EHPG ligand in the inner coordination sphere of Tb(III). Energy transfer from Tb(III) to Eu(III) in the Tb(III)-EHPG-Eu(III) system indicated an existence of only monomeric form of the Tb-EHPG complex. Analysis of the ^1H NMR and FTIR spectra of the EHPG ligand and its complexes with lanthanide(III) ions confirmed the hexadentate manner of EHPG complexation with the lanthanides. The system of Dy(III)-EHPG, showing a linear dependence of luminescence intensity (λ$\text{}_{em}$=578 nm) of Dy(III) on its concentration, in the range of 3.3×10-7 to 1×10-5 mol. l-1, can be applied for spectrofluorimetric determination of Dy(III).
    Źródło:
    Acta Physica Polonica A; 1996, 90, 2; 353-359
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis and Spectroscopic Study of Europium(III) in Heteropolyanion [EuP$\text{}_{5}$W$\text{}_{30}$O$\text{}_{110}$]$\text{}^{12-}$
    Autorzy:
    Lis, S.
    Elbanowski, M.
    But, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1945636.pdf
    Data publikacji:
    1996-08
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.40.Ha
    78.40.-q
    42.62.Hk
    78.55.-m
    Opis:
    The heteropolyanions of Preyssler anion [NaP$\text{}_{5}$W$\text{}_{30}$O$\text{}_{110}$]$\text{}^{14-}$ and its europium-encrypted derivative [EuP$\text{}_{5}$W$\text{}_{30}$O$\text{}_{110}$]$\text{}^{12-}$ were prepared and spectroscopically characterized. The compositions of these heteropolyanions were verified based on the results from elemental and thermogravimetric analysis and the data of spectrophotometric determination of tungsten contents. Absorption in the UV-vis and IR region and luminescence spectra, as well as results of the laser-induced europium ion luminescence spectroscopy, obtained for solid complexes and their solutions, were analysed. Both in solid and solution the europium-encrypted derivative has three water molecules of hydration.
    Źródło:
    Acta Physica Polonica A; 1996, 90, 2; 361-366
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Band Structure and Optical Properties οf the Layered $Hg_{3}TeCl_{4}$ Crystal
    Autorzy:
    Sznajder, M.
    Bercha, D.
    Potera, P.
    Khachapuridze, A.
    Panko, V.
    Bercha, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1791361.pdf
    Data publikacji:
    2009-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.20.-e
    78.40.-q
    78.55.-m
    71.20.-b
    Opis:
    First experimental investigations on absorption and photoluminescence of the novel $Hg_{3}TeCl_{4}$ monocrystals grown by the Bridgman method are reported. A comparison of the measurement results with theoretical band structure calculations of the $Hg_{3}TeCl_{4}$ crystal confirmed that $Hg_{3}TeCl_{4}$ is a wide-band-gap photoconductor ($E_{g}$ = 3.64 eV at 24 K) with the effective masses of charge carriers characteristic for semiconductors. Energetic position of the main photoluminescence peak and its temperature dependence indicates the presence of an additional energy level in the energy gap which takes part in the radiative recombination process and whose origin was discussed.
    Źródło:
    Acta Physica Polonica A; 2009, 116, 5; 950-951
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Energy Level Scheme of Nd$\text{}^{3+}$ Ion in Rare Earth Oxyhalides, REOX (X = F, Cl, and Br)
    Autorzy:
    Beaury, L.
    Hölsä, J.
    Korventausta, J.
    Krupa, J.-C.
    Lamminmäki, R.-J.
    Porcher, P.
    Rahiala, H.
    Säilynoja, E.
    Powiązania:
    https://bibliotekanauki.pl/articles/1952823.pdf
    Data publikacji:
    1996-12
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    71.55.-i
    71.70.Ch
    78.40.-q
    78.55.-m
    Opis:
    The energy level schemes of the neodymium oxyhalides (NdOX, X = F, Cl, and Br) were studied and simulated with a phenomenological model accounting simultaneously for both the free ion interactions and the crystal field effect. The former included the electrostatic and interconfigurational interactions as well as the spin-orbit coupling. The simulations were carried out by using the data from the optical absorption and luminescence as well as the inelastic neutron scattering measured at low temperatures between 2.5 and 77 K. The values of the Slater integral F$\text{}^{2}$ describing the electrostatic interactions decrease while F$\text{}^{4}$ and F$\text{}^{6}$ increase as a function of the ionic radius of the halide anion. The strength of the spin-orbit coupling is quite the same in all three matrices. The crystal field effect - measured as the crystal field strength parameter S - is almost twice as strong in the hexagonal NdOF matrix (650 cm$\text{}^{-1}$) than in the tetragonal NdOCI or NdOBr (367 and 378 cm$\text{}^{-1}$, respectively). Similar evolution was obtained for the short-and mid-range crystal field strengths related to the spatial extension of the interaction.
    Źródło:
    Acta Physica Polonica A; 1996, 90, 6; 1203-1213
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Excited State Absorption and Thermoluminescence in Ce and Mg Doped Yttrium Aluminum Garnet
    Autorzy:
    Wiśniewski, K.
    Koepke, Cz.
    Wojtowicz, A. J.
    Drozdowski, W.
    Grinberg, M.
    Kaczmarek, S. M.
    Kisielewski, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/2007834.pdf
    Data publikacji:
    1999-03
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.55.Hx
    78.55.-m
    78.60.Kn
    73.50.Gr
    29.40.Mc
    78.20.-e
    78.20.Wc
    78.40.-q
    Opis:
    In this paper we report preliminary results of optical studies on Y$\text{}_{3}$Al$\text{}_{5}$O$\text{}_{12}$ (YAG) crystals codoped with Ce and Mg. By using measurements of luminescence, absorption, and luminescence excitation spectra we demonstrate that although the basic features introduced to the YAG host by the Ce-doping remain intact, the Mg-codoping imposes some significant changes on other properties of the material. These changes are potentially important for laser and/or scintillator applications of YAG:Ce and are due, most likely, to modifications of defect populations in the material. We characterize them by using the techniques of thermoluminescence and excited state absorption under excimer laser pumping. These techniques, interestingly, yield results that seem inconsistent. While the thermoluminescence signal of the Mg-doped sample is strongly reduced, suggesting that trap concentrations in the presence of Mg are suppressed, the excited state absorption signal, which we also relate to the traps, is higher. We offer a tentative explanation of this contradiction between the two experiments that involves a massive transfer of electrons from the Mg-related defects to the excited state absorption centers caused by the excimer pump itself.
    Źródło:
    Acta Physica Polonica A; 1999, 95, 3; 403-412
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-6 z 6

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