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Wyświetlanie 1-5 z 5
Tytuł:
Magnetic Resonance Study of MnO/ZnO Nanopowders
Autorzy:
Guskos, N.
Zolnierkiewicz, G.
Typek, J.
Sibera, D.
Narkiewicz, U.
Łojkowski, W.
Powiązania:
https://bibliotekanauki.pl/articles/1492782.pdf
Data publikacji:
2011-12
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Tt
76.30.Fc
76.50.+g
Opis:
Fine particles n(MnO)/-(1-n)ZnO (n = 0.05 to 0.95) were prepared by wet chemistry method. According to X-ray diffraction analysis the obtained samples with n = 0.95, 0.90, 0.80, 0.70, 0.60 contained $Mn_3O_4$ and $ZnMn_2O_4$ phases, while samples with n = 0.05, 0.10, 0.20, 0.30, 0.40 and 0.50 contained $ZnMnO_3$ and ZnO phases. The mean crystalline size of $ZnMnO_3$ varied from 8 to 13 nm. The magnetic resonance investigations have been carried out at room temperature. Slightly asymmetric, broad and intense magnetic resonance line is recorded for all samples. The magnetic resonance spectra parameters showed marked differences depending on the composition index n. This could be explained by the variation of the magnetic susceptibility and a much slower evolution of spin relaxation, associated with the interaction of crystal field and superexchange interactions. Taking into account the values of magnetic resonance parameters, the investigated samples could be divided into two groups: these with the composition index n<0.50 and those with n>0.50. A detailed discussion of the magnetic properties of different phases in the n(MnO)/-(1-n)ZnO system is presented.
Źródło:
Acta Physica Polonica A; 2011, 120, 6; 1074-1079
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure and Magnetic Properties of Nanocrystalline $NiFe_{2}O_{4}$ Prepared via Precipitation Route
Autorzy:
Žák, T.
David, B.
Ćosović, A.
Ćosović, V.
Živković, D.
Talijan, N.
Powiązania:
https://bibliotekanauki.pl/articles/1378217.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
75.50.Tt
81.07.Bc
81.07.Wx
Opis:
Nanocrystalline Ni-ferrite was synthesized by modified precipitation method in which soluble starch is used as dispersing agent and $Na_{2}CO_{3}$ as a precipitating agent. $NiSO_{4}·6H_{2}O$ and $Fe(NO_{3})_{3}·9H_{2}O$ were used as precursors for nickel and ferric oxide, respectively. The obtained nanocrystalline Ni-ferrite was analysed and discussed through structural, compositional and magnetic characterization. Formation of pure $NiFe_{2}O_{4}$ phase with average crystallite size of 21 nm has been confirmed by X-ray diffraction analysis (XRD). The determined phase composition was additionally supported by results of $\text{}^{57}Fe$ Mössbauer phase (MS) analysis and material's nanocrystalline structure by field emission scanning electron microscopy (FE-SEM). Thermomagnetic behaviour was studied up to 800 °C. The obtained room temperature magnetic hysteresis loop, recorded by means of a vibrating sample magnetometer (VSM), exhibits characteristic "S" shape of the soft magnetic material with the measured coercivity of about 10 kA/m and the specific moment up to 40 $Am^{2}$/kg.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 142-143
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
FMR Study of Temperature Dependence of Magnetic Properties of Nanocrystalline $0.90(Fe_2O_3)$/0.10ZnO
Autorzy:
Guskos, N.
Glenis, S.
Zolnierkiewicz, G.
Typek, J.
Sibera, D.
Narkiewicz, U.
Powiązania:
https://bibliotekanauki.pl/articles/1492781.pdf
Data publikacji:
2011-12
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Tt
76.30.Fc
76.50.+g
Opis:
The nanocrystalline mixed system $0.90(Fe_2O_3)$/-0.10ZnO has been prepared by coprecipitation and calcination processes. The phase composition of samples was determined by X-ray diffraction. The studied nanocrystalline sample is dominated by phase $Fe_2O_3$ but very small amounts of ZnO and $ZnFe_2O_4$ phases were also identified. The ferromagnetic resonance investigations of the obtained sample have been carried out in the temperature range from liquid helium to room temperature. The asymmetrical and very intense magnetic resonance line was recorded at all temperatures. A significant shift of spectra towards lower magnetic fields with decreasing temperature was observed. A very good fitting by two Lorentzian functions has been obtained which suggested the existence of a strong anisotropic magnetic interaction. Some similarities in behaviour of ferromagnetic resonance parameters of the present sample and the $0.95Fe_2O_3Fe2O3$/0.05ZnO sample were noticed but the parameters values were essentially different. The gradients Δ $H_{r}$/Δ T (where $H_{r}$ is the resonance field), the broadening processes of the resonance lines as well as the line amplitudes were changing more intensely changing with temperature in comparison to sample $0.95Fe_2O_3Fe2O3$/0.05ZnO. The following values Δ $H_{r}$/Δ T are obtained: 16.7(1) Gs/K and 20.7(1) Gs/K over the 60 K temperatures where below 40 K is 41.5(1) Gs/K and 56.0(1) Gs/K. The reorientation processes were more active at low temperatures for smaller concentrations of magnetic nanoparticles.
Źródło:
Acta Physica Polonica A; 2011, 120, 6; 1070-1073
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Nanocrystalline ZnO Doped with Fe$\text{}_{2}$O$\text{}_{3}$ - Magnetic and Structural Properties
Autorzy:
Kuryliszyn-Kudelska, I.
Hadžić, B.
Sibera, D.
Kilanski, L.
Romčević, N.
Romčević, M.
Narkiewicz, U.
Dobrowolski, W.
Powiązania:
https://bibliotekanauki.pl/articles/2048113.pdf
Data publikacji:
2011-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Tt
81.05.Dz
75.50.Lk
75.50.Vv
Opis:
We have studied the magnetic properties of ZnO nanocrystals doped with Fe$\text{}_{2}$O$\text{}_{3}$ in the magnetic dopant range from 5 to 70 wt%. The nanocrystals were synthesized by wet chemical method. The detailed structural characterization was performed by means of X-ray diffraction and micro-Raman spectroscopy measurements. The results of systematic measurements of magnetic AC susceptibility as a function of temperature and frequency are presented. We observed different types of magnetic behavior. For ZnO samples doped with low content of Fe$\text{}_{2}$O$\text{}_{3}$, the results of low-field AC susceptibility are satisfactorily explained by superparamagnetic model including inter-particle interactions. With the increase of magnetic Fe$\text{}_{2}$O$\text{}_{3}$ content, the spin-glass-like behavior is observed.
Źródło:
Acta Physica Polonica A; 2011, 119, 5; 689-691
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of the Grain Size on Polaron Transport in Nanostructured La$\text{}_{2}\text{}_{/}\text{}_{3}$ Ca$\text{}_{1}\text{}_{/}\text{}_{3}$ MnO$\text{}_{3}$ Evidenced by EPR
Autorzy:
Raita, O.
Grecu, M. N.
Filip, X.
Toloman, D.
Giurgiu, L. M.
Idziak, S.
Hoffmann, S. K.
Powiązania:
https://bibliotekanauki.pl/articles/2043406.pdf
Data publikacji:
2005-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Tt
73.63.Bd
76.50.+g
Opis:
We report an electron paramagnetic resonance investigation of the grain size effects on the polaron transport in the paramagnetic regime of nanosized La$\text{}_{2}\text{}_{/}\text{}_{3}$ Ca$\text{}_{1}\text{}_{/}\text{}_{3}$ MnO$\text{}_{3}$ manganites. The temperature dependences of the EPR integral intensity were analyzed in terms of spin-spin exchange interaction and small polaron hopping scenarios. The polaron activation energy decreases with the reduction of the grain size. A discussion is given concerning the factors which could explain the observed change.
Źródło:
Acta Physica Polonica A; 2005, 108, 1; 113-118
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-5 z 5

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