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    Wyświetlanie 1-6 z 6
    Tytuł:
    Effect of Borax Pentahydrate Addition to Acid Bath on the Microstructure and Corrosion Resistance of Zn-Co Coating
    Autorzy:
    Karahan, İ.
    Powiązania:
    https://bibliotekanauki.pl/articles/1402495.pdf
    Data publikacji:
    2015-08
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    68.37.-d
    68.55.-a
    81.65.Kn
    Opis:
    In this work, the Zn-Co coatings were synthesized on AISI 4140 steel and aluminum plates by using potentiostatic electrodeposition technique in sulphate-based acidic baths with 0, 20, 40 and 60 gl¯¹ of borax pentahydrate, as additive. The effect of borax pentahydrate on the microstructure of the samples was observed using scanning electron microscopy and X-ray diffractometer. The deposition process was investigated by cyclic voltammetry. The effect of borax pentahydrate on the corrosion resistance of the samples was studied by potentiodynamic polarization technique. The results have demonstrated, that the addition of borax pentahydrate was in favor of the growth of grains. The morphology of pyramidal islands on the surface was changed to a more flat structure. The results have also demonstrated that the effect of borax pentahydrate was not monotonous. With increasing concentration, the corrosion potential was at minimum and the charge transfer resistance $R_{t}$ was at maximum for the sample obtained from the bath with 60 gl¯¹ of borax pentahydate, indicating that this sample showed the best corrosion resistance. It was found that current density first decreased and than increased, due to adsorption of a complex of borax pentahydrate and/or changes in the morphology, however, the initial deposition potential was not affected. The addition of borax pentahydrate to the bath led to formation of the best Zn-Co deposits, composed of coalesced globular fine grains, smaller than ≈2 μm in diameter. In addition, all of the studied Zn-Co deposits consisted of η phases. It is suggested that Zn-Co deposits produced in the bath containing 60 gl¯¹ of borax pentahydrate probably offer sacrificial protection to the steel substrate.
    Źródło:
    Acta Physica Polonica A; 2015, 128, 2B; B-432-B-435
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of Antireflection Structures as a Protective Layer of Solar Cells with Nanoporous Silica Films and Nanoimprinted Moth-Eye Structure
    Autorzy:
    Kim, K.
    Han, J.
    Jang, J.
    Choi, C.
    Choi, S.
    Kim, C.
    Kye, H.
    Cheong, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/1492625.pdf
    Data publikacji:
    2011-12
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.46.-w
    68.37.-d
    68.55.-a
    78.20.-e
    Opis:
    The antireflection structures are fabricated by sol-gel process as a protective layer of solar cells and by hot embossing process with anodized aluminum oxide membrane template on polycarbonate film. The optical properties and morphology of the antireflection structures are analyzed by UV-visible spectroscopy and field emission scanning electron microscopy, respectively. The total conversion efficiency of a polycrystalline Si solar cell module with the protective layer, sol-gel-derived nanoporous antireflection structure, is increased by 2.6% and 5.7% for one-side antireflection coated prismatic matt glass and both-side antireflection coated prismatic matt glass, respectively.
    Źródło:
    Acta Physica Polonica A; 2011, 120, 6A; A-047-A-049
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Structural Characterization of $La_{1-x}Sr_xCoO_3$ Thin Films Deposited by Pulsed Electron Deposition Method
    Autorzy:
    Cieniek, Ł.
    Kopia, A.
    Cyza, A.
    Kowalski, K.
    Kusiński, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1398370.pdf
    Data publikacji:
    2016-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.15.-z
    81.10.Bk
    81.07.Bc
    68.55.-a
    68.55.J-
    68.55.Nq
    68.37.-d
    Opis:
    The aim of the presented research was to investigate the influence of strontium dopant on the structure and composition of $La_{1-x}Sr_{x}CoO_3$ (x=0, 0.1, 0.2) perovskite thin films. Pure and Sr doped LaCoO₃ thin films were grown by pulsed electron deposition technique on crystalline epi-polished Si/MgO substrates. Numerous analytical techniques (scanning electron microscopy, atomic force microscopy, X-ray photoelectron spectroscopy, and X-ray diffraction) were applied to characterize their phase/chemical composition, structure and surface morphology. X-ray diffraction analysis showed the presence of pure LaCoO₃ perovskite phase in the undoped thin film. For Sr doped thin films $La_{0.8}Sr_{0.2}CoO_3$ (x=0.2), $La_{0.9}Sr_{0.1}CoO_3$ (x=0.1) small contents of La₂ O₃ and LaSrCoO₄ phases were noticed. The crystallite sizes, calculated from the Williamson-Hall plots, were about 18 nm for all analyzed films. According to scanning electron microscopy/atomic force microscopy observations, obtained thin films were free from defects and cracks. Atomic force microscopy (tapping mode) analysis revealed the differences in the shape and quantity of surface crystallites for all thin films as a result of Sr doping and different deposition parameters. Atomic force microscopy technique also allowed measurement of roughness parameters for analyzed samples. X-ray photoelectron spectroscopy analyses of chemical states of elements of thin films showed that their chemical state was stable across the film thickness and even at the interface with the MgO substrate. X-ray photoelectron spectroscopy analysis also allowed to evaluate chemical states and atomic concentration of La, Co, and Sr elements within cross-sections of deposited thin films.
    Źródło:
    Acta Physica Polonica A; 2016, 130, 4; 1121-1123
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Influence of Ca Content on the Structure and Properties οf (Co,Ca)O Thin Films Deposited by PLD Technique
    Autorzy:
    Cieniek, L.
    Kac, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1537944.pdf
    Data publikacji:
    2010-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.15.Fg
    81.15.-z
    81.15.Aa
    68.55.-a
    68.60.Bs
    68.37.-d
    68.55.jd
    Opis:
    In this paper the results of investigations of pure and Ca-doped CoO thin films deposited by PLD technique are presented. The studies carried out for variable Ca content allowed to establish optimal conditions for good quality oxide films preparation. The microstructure, chemical/phase composition and morphology of obtained thin films were examined by means of diverse techniques (SEM, EDS, XPS and XRD). For estimation of deposited Ca-doped CoO films quality the nanohardness and scratch tests (adhesion) were performed. Obtained results confirm that using PLD technique it is possible to carry stoichiometric composition of (Co,Ca)O from target to single crystal substrate and allow to conclude that the calcium dopant concentration (chemical composition) influence on the morphology and measured properties of deposited (Co,Ca)O films.
    Źródło:
    Acta Physica Polonica A; 2010, 117, 5; 803-807
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Comparison of Five-Layered ZrO₂ and Single-Layered Ce, Eu, and Dy-Doped ZrO₂ Thin Films Prepared by Sol-Gel Spin Coating Method
    Autorzy:
    Çiçek Bezir, N.
    Evcin, A.
    Kayali, R.
    Özen, M.
    Esen, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/1031178.pdf
    Data publikacji:
    2017-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    68.37.-d
    68.55-a
    68.60-p
    78.20.-e
    81.10.Dn
    71.20.Be
    Opis:
    In order to investigate the influence of the number of layers on the properties of ZrO₂ thin films, we prepared one pure ZrO₂ film sample with five layers and Ce, Eu, and Dy-doped ZrO₂ samples with single layer, by spin-coating sol gel-method. The crystal structures of thin films were determined using X-ray diffraction, morphology of the samples was analyzed by scanning electron microscopy, and the optical properties of the samples were determined by ultraviolet/visible absorbance measurements. The results of these measurements have shown that the concentration of the dopants and the thickness of thin film layers play a vital role in the physical, chemical, and optical properties of the pure and doped ZrO₂ thin films.
    Źródło:
    Acta Physica Polonica A; 2017, 132, 3; 612-616
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Comparison of Pure and Doped TiO₂ Thin Films Prepared by Sol-Gel Spin-Coating Method
    Autorzy:
    Çiçek Bezir, N.
    Evcin, A.
    Kayali, R.
    Özen, M.
    Balyaci, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/1031525.pdf
    Data publikacji:
    2017-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    68.37.-d
    68.55.-a
    68.60.-p
    78.20.-e
    81.10.Dn
    71.20.Be
    Opis:
    In this study, using spin-coating sol-gel method we fabricated TiO₂ thin films, doped with different concentrations (1, 2, and 3 mole %) of Ce, Dy, and Eu. Characterization of the prepared samples was performed by means of the X-ray diffraction, scanning electron microscopy, ultraviolet visible absorption, and differential thermal and thermo gravimetric analysis. X-ray diffraction measurements have shown that in Eu and Dy-doped samples crystal structure consists of mixed rutile and the dominant anatase phases, however the Ce doped samples consist of anatase phase only. Scanning electron microscopy images have revealed that while average thin film thickness of the Dy-doped samples decreases with increasing concentration of Dy, the average film thicknesses of samples doped with Ce and Eu increases with increasing concentrations of these dopants. Ultraviolet visible absorption spectroscopy measurements have shown that while absorbances of the samples doped by 1 and 2 mole % of the dopants have nearly similar properties, these properties differ from each other for 3 mole % of the dopants. Finally, differential thermal and thermo gravimetric analyses have shown that the chemical reactions and weight losses of the samples have occurred at the expected temperatures.
    Źródło:
    Acta Physica Polonica A; 2017, 132, 3; 620-624
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-6 z 6

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