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    Wyświetlanie 1-5 z 5
    Tytuł:
    Influence of the Introduction of Copper into Amorphous $As_2Se_3$ Matrix on Its Thermal and Structural Characteristics
    Autorzy:
    Štrbac, G.
    Lukić-Petrović, S.
    Štrbac, D.
    Čajko, K.
    Turyanytsa, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/1399717.pdf
    Data publikacji:
    2013-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    64.70.kj
    64.70.P-
    65.60.+a
    Opis:
    This paper describes the results of the determination of some thermal and structural parameters of glasses from the $Cu_{x}(As_2Se_3)_{100-x}$ system for x=0, 1, 5, 10 and 15 at.%. Based on the differential scanning calorimetry curves taken at different heating rates, glass transition temperature $T_{g}$, onset temperature of crystallization $T_{onset}$, and melting temperature $T_{m}$ of crystalline units formed are determined. The values of activation energy $E_{g}$ of glass transition process are calculated. These characteristic temperatures served as the basis for the calculation of the parameters of thermal stability of the glasses towards crystallization.
    Źródło:
    Acta Physica Polonica A; 2013, 123, 2; 256-258
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Kinetic Analysis of Thermal Processes in Ag-As-S-Se System Based on DSC Measurements
    Autorzy:
    Čajko, K.
    Lukić-Petrović, S.
    Štrbac, G.
    Ivetić, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/1398711.pdf
    Data publikacji:
    2016-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    65.60.+a
    64.70.kj
    64.70.P-
    64.70.kg
    Opis:
    Thermal properties of glasses from the system $Ag_x(As_{40}S_{30}Se_{30})_{100-x}$ for x=0, 0.5, 1, 3, and 5 at.% were investigated by differential scanning calorimetry. The DSC curves were obtained under non-isothermal conditions which allowed determination of the glass transition temperature $T_{g}$ (onset temperature), crystallization temperature $T_{p}$ (corresponding to the crystallization peak maximum), melting temperature $T_{m}$, crystallization enthalpy $H_{c}$, and melting enthalpy $H_{m}$. The DSC curves obtained at the same heating rate were analyzed in order to study the variation of glass transition temperature with Ag concentration. Observed $T_{g}$ shift toward higher values, with increase in the heating rate, is in agreement with the Lasocka equation. Samples with 3 at.% and 5 at.% Ag were further thermally treated at different heating rates with the aim of analyzing kinetic processes of crystallization. The Moynihan and Kissinger models were used to calculate the activation energy of glass transition and activation energy of crystallization. For the samples that showed the crystallization processes an assessment of the thermal stability was done based on different criteria.
    Źródło:
    Acta Physica Polonica A; 2016, 129, 4; 509-513
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Solid State Polymorphism and Dynamics οf 2,2-Dimethylbutan-1-ol as Studied by Adiabatic Calorimetry and Dielectric Spectroscopy
    Autorzy:
    Juszyńska-Gałązka, E.
    Zieliński, P.
    Massalska-Arodź, M.
    Krawczyk, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1399009.pdf
    Data publikacji:
    2013-12
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    65.60.+a
    77.22.Gm
    64.70.P-
    Opis:
    2,2-dimethylbutan-1-ol, known as neohexanol, was studied by adiabatic calorimetry and dielectric spectroscopy. Details of complex solid state polymorphism and relaxational dynamics were identified and described. System of phases of neohexanol was found to be monotropic with three orientationally disordered crystalline phases besides isotropic liquid and ordered crystal. Moreover, two subsequent glass transition anomalies of heat capacity $C_{p}(T)$ were detected on heating in one of the supercooled orientationally disordered crystalline phases. Thermodynamical properties of neohexanol are described in relation to the dielectric relaxation processes found.
    Źródło:
    Acta Physica Polonica A; 2013, 124, 6; 917-925
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study of Glass Transition and Crystallization Behavior in $Ga_{15}Se_{85 - x}Pb_x$ (0 ≤ x ≤ 6) Chalcogenide Glasses
    Autorzy:
    Khan, Z.
    Khan, S.
    Alvi, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1400308.pdf
    Data publikacji:
    2013-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.43.Dq
    61.05.cp
    64.70.p
    64.70.dg
    65.60.+a
    Opis:
    There has been a growing interest in the synthesis and characterization of amorphous chalcogenide glasses due to their importance in preparing electronic memories, grating, switching devices and their optical applications as good IR transmitting materials. The study of the glass transformations and crystallization processes in the amorphous systems is interesting not only from the fundamental aspect of establishing the reaction mechanism of crystal nucleation and growth, but also from a technological point of view. The present research work is concentrated on the study of glass transition and crystallization behavior in $Ga_{15}Se_{85 - x}Pb_x$ with x=0, 3, and 6 chalcogenide glasses by differential scanning calorimetry. Their amorphous nature has been verified by X-ray diffraction. The differential scanning calorimetry experiments were performed at different continuous heating rates (5 to 25 K/min). The glass transition temperature (T_{g}) and crystallization temperature $(T_{c})$ of these glasses has been determined from differential scanning calorimetry thermograms. The dependence of $T_{g}$ and $T_{c}$ on the heating rate (β) has been used for the determination of different crystallization parameters such as the activation energy of crystallization (Δ $E_{c}$), the activation energy for structural relaxation (Δ $E_{t}$) and the order parameter (n). The results of crystallization were discussed on the basis of different models such as Kissinger's approach and modification for non-isothermal crystallization in addition to Johnson, Mehl, Ozawa and Avrami.
    Źródło:
    Acta Physica Polonica A; 2013, 123, 1; 80-86
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Acoustic Emission During Firing of the Illite-Based Ceramics with Fly Ash Addition
    Autorzy:
    Knapek, M.
    Húlan, T.
    Dobroň, P.
    Chmelík, F.
    Trník, A.
    Štubňa, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/1402156.pdf
    Data publikacji:
    2015-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    64.70.ph
    61.43.Fs
    65.60.+a
    81.70.Pg
    43.40.Le
    Opis:
    In this work, illite-based ceramic body with power plant fly ash addition (60 wt.% of illite, 30 wt.% of fly ash and 10 wt.% of illite fired at 1100°C) was investigated by the thermal analysis techniques (differential thermal analysis, thermodilatometry and thermogravimetry) and the acoustic emission technique. The green body was heated up to 1100°C at three different rates 2.5, 5, 10 K/min. The most intense acoustic emission was recorded at the highest rate 10 K/min. Mutual correlations between thermal analyses and acoustic emission data were also examined. The first acoustic emission response appears at 430°C, corresponding to a small endotherm on the DTA curve, where the thermal decomposition of mineral portlandite takes place. In the temperature range from 600 to 900°C, high acoustic emission activity correlates with dehydroxylation and expansion of the sample. At temperatures higher than 800°C, the source of acoustic emission signals is the thermal decomposition of calcite. The amorphous phase created from illite at 920°C becomes pyroplastic, therefore it is not documented by the acoustic emission technique.
    Źródło:
    Acta Physica Polonica A; 2015, 128, 4; 783-786
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-5 z 5

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