- Tytuł:
- The 5:7 Member of the Spin-Ladder Series in the Bi-Sr-Ca-Cu-O System
- Autorzy:
-
Zaremba, O.
Shcherban, O.
Akselrud, L.
Gladyshevskii, R.
Banfi, F.
Giannini, E. - Powiązania:
- https://bibliotekanauki.pl/articles/1550056.pdf
- Data publikacji:
- 2010-01
- Wydawca:
- Polska Akademia Nauk. Instytut Fizyki PAN
- Tematy:
-
61.46.-w
61.66.-f - Opis:
- The crystal structure of the $(Bi_{0.02}Sr_{0.39}Ca_{0.59})_{10}Cu_{17}O_{29}$ spin-ladder compound was determined from single-crystal X-ray diffraction data. The precursor powder was prepared from stoichiometric amounts of $SrCO_{3},$ $CaCO_{3},$ $CuO,$ and $Bi_{2}O_{3}$ by calcination at 820°C for 20 h and pressed to form a rod used for the crystal growth. The travelling-solvent-floating-zone method was applied in an image furnace to grow large single crystals. The composite commensurate structure was solved and refined in space group F222, Pearson symbol oF224, a = 11.340(2), b = 12.829(2), c = 19.441(3) Å, Z = 4. The composite incommensurate structure of the $(Bi_{0.02}Sr_{0.39}Ca_{0.59})_{10}Cu_{17}O_{29}$ compound was solved and refined in the (3+1)-space group F222 (00γ), a = 11.340(2), b = 12.829(2), c_1 = 2.7773(4), c_2 = 3.8882(6) Å, q = 0.7143.
- Źródło:
-
Acta Physica Polonica A; 2010, 117, 1; 42-47
0587-4246
1898-794X - Pojawia się w:
- Acta Physica Polonica A
- Dostawca treści:
- Biblioteka Nauki