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    Wyświetlanie 1-14 z 14
    Tytuł:
    Sintering Behavior and Machinability in Mica Glass-Ceramic of the System $SiO_2-Al_2O_3-MgO-K_2O-B_2O_3-F$
    Autorzy:
    Ercenk, E.
    Yilmaz, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1293704.pdf
    Data publikacji:
    2014-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.05.cp
    68.37.Hk
    81.20.Ev
    81.20.Wk
    81.05.Je
    81.05.Mh
    Opis:
    Mica glass-ceramic was prepared by sintering method from in the $SiO_2-Al_2O_3-MgO-K_2O-B_2O_3-F_2$ system. The sintering behavior and machinability of a glass-ceramic composition were examined. The starting materials were mixed and milled in an alumina ball mill for 2 h. Then the powders were sieved to obtain grain sizes smaller than 75 μm. For the shaping process, disc samples were prepared by pressing at 100 MPa. The pressed discs were sintered at temperatures in the range from 900 to 1200C for 2 h in an electric furnace using a heating rate of 5°C/min. X-ray diffraction analysis, scanning electron microscopy, and machinability tests for characterization were performed on sintered samples. The results showed that all samples exhibited similar phases formation and good machinability.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 2; 629-631
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Bond Strength of Basalt Based Glass-Ceramic Coatings
    Autorzy:
    Bayrak, G.
    Ercenk, E.
    Sen, U.
    Yilmaz, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1194582.pdf
    Data publikacji:
    2014-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.43.Fs
    62.20.-x
    61.05.cp
    Opis:
    In the present study, powders produced from the volcanic basalt rocks were coated on pre-coated AISI 1040 steel with Ni-5% Al bond coat by atmospheric plasma spray coating technique. The coated specimens were characterized by optical microscopy, scanning electron microscopy, metallography and X-ray diffraction. Bonding strength of coatings was evaluated in accordance with the ASTM C-633 method. Coated basalt material from the APS coating system was determined in the glassy amorphous state by X-ray diffraction analysis. The coated samples were heat-treated at 800C for 1-4 h for crystallization. The phases formed in the basalt base glass-ceramic coatings were augite, Fe-diopside, anorthite, and andesine which were detected by X-ray diffraction analysis. Basalt based glass-ceramic coatings include splat, porosity and un-melted particles which were the characteristic of plasma sprayed coatings. Experiment result showed that the crystallization time increase caused the decrease of the bond strengths of the coatings.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 2; 620-622
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Glass and Glass-Ceramics Produced from Fly Ash and Boron Waste
    Autorzy:
    Ercenk, E.
    Sen, U.
    Bayrak, G.
    Yilmaz, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1181592.pdf
    Data publikacji:
    2014-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.43.Fs
    64.70.P-
    61.05.cp
    81.70.Pg
    62.20.Qp
    Opis:
    In the current study, the effect of boron waste addition on some properties of fly ash based glass and glass-ceramics were investigated. The powder compositions including 10, 30, and 50 wt% boron waste was prepared. All the investigated compositions were melted at 1500C by using electrical furnaces. Melting structures were cast into the graphite mold. Thus, fly ash-boron waste based glass materials were produced. To transform the glass-ceramic, crystallization process was performed. Crystallization and glass-transition temperatures were determined by differential thermal analysis. Highly dense and crystalline materials, predominantly composed of diopside and augite together with tincalconite and residual glassy phase, were detected by X-ray diffraction analysis after heat treatment at 800, 900, and 1000C for 1 h. For the glass and glass-ceramic samples, mechanical tests such as hardness and fracture toughness were realized. A boron waste addition has a positive effect on the hardness of the specimens unlike the fracture toughness results. Furthermore, produced glass-ceramic materials were characterized via scanning electron microscopy.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 2; 626-628
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study of Ultrasonically Sprayed ZnO Films: Thermal Annealing Effect
    Autorzy:
    Ozutok, F.
    Demirselcuk, B.
    Sarica, E.
    Turkyilmaz, S.
    Bilgin, V.
    Powiązania:
    https://bibliotekanauki.pl/articles/1490746.pdf
    Data publikacji:
    2012-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.20.Ci
    61.05.cp
    Opis:
    ZnO thin films were deposited on microscope glass substrates by ultrasonic spray pyrolysis technique. The effects of annealing under various temperatures on the optical and structural properties of ZnO thin films were analyzed. The as-deposited and annealed ZnO thin films were investigated by UV/VIS spectrophotometer and X-ray diffractometer. Some of the optical properties of the films such as transmittance, absorbance and band gap energy were investigated by UV/VIS spectrophotometer. The crystallinity levels of the films were investigated, the structural parameters such as diffraction angle, full-width at half maximum, lattice parameters, grain size and dislocation density were calculated and structural properties were analyzed. X-ray diffraction patterns indicated that the ZnO films had a polycrystalline hexagonal wurtzite structure.
    Źródło:
    Acta Physica Polonica A; 2012, 121, 1; 53-55
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Properties of~Rf Plasma Nitrided Silicon Thin Films at Different Rf Plasma Processing Powers
    Autorzy:
    Mohamed, S.
    Raaif, M.
    Abd El-Rahman, A.
    Shaaban, E.
    Powiązania:
    https://bibliotekanauki.pl/articles/1493713.pdf
    Data publikacji:
    2011-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.15.Dj
    61.05.cp
    73.61.-r
    78.66.-w
    Opis:
    Nitrided surfaces and composition gradients in thin films exhibit interesting mechanical, electrical and optical properties. Therefore, silicon (Si) thin films were prepared by electron beam evaporation and nitrided by an inductively coupled rf plasma. The effects of successive plasma processing power on structural and optical properties as well as electrical resistivity were examined by different characterization techniques. The Si thin films were transformed gradually into nitrides compound thin films and the amount of nitrogen in the film increased with increasing the rf processing power. The Si nitrided films showed structural, optical and electrical properties that depend on the nitriding power. Increasing the rf plasma processing power caused amorphization, reduced the thickness, increased transmittance, increased resistivity and decreased the reflectance of the Si films. The electrical resistivity increased about eight orders of magnitude when the sample nitrided at 500 W. Different optical band gap were determined indicating the presence of different competing phases in the same film. The decrease in refractive index with plasma treatment power is attributed to the possible change in the bucking density as well as to the increase in the band gap.
    Źródło:
    Acta Physica Polonica A; 2011, 120, 3; 552-557
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    LSMO Films with Increased Temperature of MI Transition
    Autorzy:
    Španková, M.
    Chromik, Š.
    Dobročka, E.
    Štrbík, V.
    Sojková, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1368201.pdf
    Data publikacji:
    2014-07
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.05.cp
    75.47.Lx
    81.15.Cd
    81.15.Fg
    Opis:
    Epitaxial $La_{0.67}Sr_{0.33}MnO_{3}$ thin films with a significant increased temperature of metal-insulator transition (~450 K) are prepared on single crystal MgO (001) substrates using different deposition techniques - a dc magnetron sputtering or a pulsed laser deposition. The crystalline perfection of the films is characterized by X-ray diffraction technique (rocking curve measurements and reciprocal space maps). As a consequence of different methods of the film preparation we show various types of the LSMO crystal structure. Our results indicate that all the LSMO layers grown on the MgO substrate with a lattice misfit of about 8% are relaxed.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 1; 212-213
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization of n-ZnO/p-GaN Heterojunction for Optoelectronic Applications
    Autorzy:
    Wachnicki, L.
    Gieraltowska, S.
    Witkowski, B.
    Figge, S.
    Hommel, D.
    Guziewicz, E.
    Godlewski, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1399138.pdf
    Data publikacji:
    2013-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    85.30.Kk
    61.05.cp
    81.05.Dz
    Opis:
    An important feature of zinc oxide and gallium nitride materials are their similar physical properties. This allows to use them as a p-n junction materials for applications in optoelectronics. In earlier work we presented use of ZnO as a transparent contact to GaN, which may improve external efficiency of LED devices. In this work we discuss properties of a n-ZnO/p-GaN heterostructure and discuss its optimization. The heterostructure is investigated by us for possible applications, e.g. in a new generation of UV LEDs or UV light detectors.
    Źródło:
    Acta Physica Polonica A; 2013, 124, 5; 869-872
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Deterioration of Mechanical Properties of MBE-Grown, Metastable Semiconductor Layer with Time: the Case of Zinc Blende MnTe
    Autorzy:
    Adamiak, S.
    Dynowska, E.
    Dziedzic, A.
    Szmuc, K.
    Janik, E.
    Wiater, M.
    Wojtowicz, T.
    Szuszkiewicz, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/1185914.pdf
    Data publikacji:
    2016-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.05.cp
    62.20.-x
    64.60.My
    Opis:
    Several few μm thick (001)-oriented, metastable MnTe layers with the zinc blende structure grown onto (001)GaAs substrate by MBE during different periods for the last twenty years were investigated by the scanning electron microscopy, atomic force microscopy, X-ray diffraction, and nanoindentation methods. A partial decomposition of the oldest investigated layers was demonstrated. An important decrease of Young's modulus from about 34 GPa to about 17 GPa, resulting from a deterioration of the crystal structure of such layers, was found.
    Źródło:
    Acta Physica Polonica A; 2016, 130, 5; 1248-1250
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Time-Resolved Pump-Probe Diffraction Experiment at SOLEIL Synchrotron: Photoinduced Spin Transition in the Molecular Crystal [TPA Fe(III) TCC] $PF_6$
    Autorzy:
    Laulhé, C.
    Ravy, S.
    Fertey, P.
    Elkaim, E.
    Legrand, F.
    Féret, P.
    Hollander, Ph.
    Hustache, S.
    Bordessoule, M.
    Ricaud, J.
    Collet, E.
    Lorenc, M.
    Buron-Le Cointe, M.
    Cailleau, H.
    Tissot, A.
    Boillot, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1489972.pdf
    Data publikacji:
    2012-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.50.Ks
    61.05.cp
    31.70.Ks
    78.47.J-
    Opis:
    We present the first time-resolved pump-probe experiment performed at synchrotron SOLEIL at the CRISTAL diffraction beamline. The time-resolved setup will be used in the near future for sub-ns time resolution experiments. We studied spin state switching in a [TPA Fe(III) TCC] $PF_6$ single crystal as induced by a ≈6 ns laser pulse (1064 nm), by measuring the 3D diffraction volume of the 002 Bragg reflection as a function of time after excitation. The intensity profiles (rocking curves) are found to evolve at two characteristic timescales, namely hundreds of ns and few μs, exhibiting subtle profile changes and peak broadenings. Consistently with previous studies, we interpret these features as due to structural inhomogeneities related to laser-induced deformation wave propagation and heat diffusion, which both start from the absorbing sites.
    Źródło:
    Acta Physica Polonica A; 2012, 121, 2; 332-335
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Epitaxial ZnO Films Grown at Low Temperature for Novel Electronic Application
    Autorzy:
    Wachnicki, Ł.
    Dużyńska, A.
    Domagala, J.
    Witkowski, B.
    Krajewski, T.
    Przeździecka, E.
    Guziewicz, M.
    Wierzbicka, A.
    Kopalko, K.
    Figge, S.
    Hommel, D.
    Godlewski, M.
    Guziewicz, E.
    Powiązania:
    https://bibliotekanauki.pl/articles/1492723.pdf
    Data publikacji:
    2011-12
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.15.Aa
    61.05.cp
    81.05.Dz
    Opis:
    Monocrystalline films of zinc oxide were grown at 300C by atomic layer deposition. ZnO layers were grown on various substrates like ZnO bulk crystal, GaN, SiC and $Al_2O_3$. Electrical properties of the films depend on structural quality. Structural quality, surface morphology and optical properties of ZnO films were characterized using X-ray diffraction, scanning electron microscopy, and photoluminescence, respectively. High resolution X-ray diffraction spectra show that the rocking curve FWHM of the symmetrical 00.2 reflection equals to 0.058° and 0.009° for ZnO deposited on a gallium nitride template and a zinc oxide substrate, respectively. In low temperature photoluminescence sharp excitonic lines in the band-edge region with a FWHM equal to 4 meV, 5 meV and 6 meV, for zinc oxide deposited on gallium nitride, zinc oxide and sapphire substrate, respectively.
    Źródło:
    Acta Physica Polonica A; 2011, 120, 6A; A-007-A-010
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Nanoquasicrystalline Phase in Mechanically Alloyed and Heat-Treated $Al_{73}Cu_{11}Cr_{16}$
    Autorzy:
    Sviridova, T.
    Shevchukov, A.
    Shelekhov, E.
    Diakonov, D.
    Gorshenkov, M.
    Kaloshkin, S.
    Tcherdyntsev, V.
    Li, Z.
    Fan, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/1373670.pdf
    Data publikacji:
    2014-08
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.44.Br
    64.70.kd
    61.05.cp
    61.05.J-
    Opis:
    X-ray diffraction analysis, scanning and transmission electron microscopy, thermal analysis and measurement of chemical composition were implemented to determine structure, thermal stability and chemical composition of the decagonal quasicrystal in $Al_{73}Cu_{11}Cr_{16}$ alloy produced by long-term mechanical alloying of elemental powders followed by annealing at 700°C. According to the TEM investigation such a technique permits to produce a single-phase nanostructural quasicrystal with grain size about 60 nm. Differential thermal analysis revealed that the decagonal phase does not exist above 923°C and undergoes incongruent two-stage melting coming to the end at 1100°C.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 2; 599-602
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Magnetic Properties of the Nanocrystalline $DyMnO_{3}$ Compound
    Autorzy:
    Dyakonov, V.
    Szytuła, A.
    Baran, S.
    Kravchenko, Z.
    Zubov, E.
    Iessenchuk, O.
    Bazela, W.
    Dul, M.
    Zarzycki, A.
    Szymczak, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/1538453.pdf
    Data publikacji:
    2010-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.05.cp
    75.47.Lx
    75.50.Ee
    75.75.-c
    Opis:
    We report on the X-ray powder diffraction and magnetic measurements of the polycrystalline and the two nanocrystalline samples of $DyMnO_{3}$ compound synthesized at temperatures of 800 and 850°C. All samples at room temperature crystallize in the orthorhombic crystal structure (space group Pnma). The crystal structure parameters determined change only slightly with preparation methods but the average grains size of the nanoparticles determined from X-ray data increases significantly with increasing annealing temperature. Temperature dependence of the magnetic susceptibility indicates the antiferromagnetic order in Dy sublattice at low temperatures.
    Źródło:
    Acta Physica Polonica A; 2010, 117, 4; 607-610
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Investigation of Sediments Causing Damage to Water Meters in a Large Drinking Water Distribution System
    Autorzy:
    Kopeć, M.
    Roman, M.
    Kąc, M.
    Budziak, A.
    Paluszkiewicz, C.
    Zarzycki, A.
    Kąc, S.
    Dutkiewicz, E.
    Cichoń, T.
    Bochnia, T.
    Kwiatek, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/1030652.pdf
    Data publikacji:
    2018-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    89.60.-k
    78.70.En
    61.05.cp
    82.80.-d
    82.80.Gk
    Opis:
    Preliminary studies on the sediments collected from water meters of Krakow water supply system were performed in the cooperation with the Municipal Water Supply and Sewage. Creation and deposition of sediments on the measuring devices installed in the water supply system is a serious technological and economical problem for water companies, defectively operating for this reason water meters must be replaced. It is evident that knowledge of the chemical and phase composition of sediments is an important step towards resolving the problem of impurities in water supply systems. Four different samples of sediments, coming from water meters, were investigated using the proton-induced X-ray emission, the X-ray diffraction, the Fourier transform infrared and Raman spectroscopy. The X-ray methods revealed presence of amorphous and fine-crystalline phases as well as high content of iron-based compounds. As a crystalline phase, the most frequently appeared: goethite, lepidocrocite, iron oxides (hematite, maghemite, magnetite), calcium carbonate, and quartz. In one of the samples, the nanocrystalline phase was found and identified as hydrous iron oxyhydroxide ferrihydrite. Vibrational spectroscopy methods confirmed the composition of crystalline phases as well as enabled to estimate the abundance of amorphous phase in samples.
    Źródło:
    Acta Physica Polonica A; 2018, 133, 2; 296-301
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Structural and magnetic properties of MBE grown (Fe/Pt) (111) multilayers
    Autorzy:
    Marynowska, A.
    Dynowska, E.
    Lewińska, S.
    Seki, T.
    Takanashi, K.
    Kanak, J.
    Pietruczik, A.
    Aleszkiewicz, P.
    Wawro, A.
    Ślawska-Waniewska, A.
    Baczewski, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/1058152.pdf
    Data publikacji:
    2016-12
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.05.cp
    61.05.jh
    68.35.bd
    68.35.Ct
    68.37.Ef
    68.37.Ps
    68.65.Ac
    75.50.Bb
    75.70.Ak
    Opis:
    Series of Al₂O₃(0001)/Pt/(Fe/Pt)ₙ/Pt multilayers with variable number of bilayers n and thicknesses of individual layers were grown using molecular beam epitaxy to investigate influence of buffer layer structure, number of bilayers, and individual layer thickness on their structural and magnetic properties. Both columnar and monocrystalline 10 nm Pt (111) buffer layers were used in the experiment. Structure of Pt buffer layer determined the roughness of Fe/Pt interfaces and consequently magnetic properties of the multilayers. When multilayers were deposited on columnar Pt buffer layer, we observed increase of Fe/Pt interfaces roughness with increasing number of bilayers to values exceeding the nominal Fe/Pt bilayer thickness in the upper part of the sample volume, which resulted in the increment of coercivity in the sample with n=15 determined from hysteresis loops measured for perpendicular orientation of magnetic field. When Fe/Pt multilayers were deposited on monocrystalline Pt buffer layer, Fe/Pt interfaces were smooth regardless the number of bilayers. All samples, despite of the quality of buffer layer, number of bilayers, and individual layer thickness revealed easy magnetisation axis oriented in the sample plane.
    Źródło:
    Acta Physica Polonica A; 2016, 130, 6; 1363-1370
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-14 z 14

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