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    Wyświetlanie 1-7 z 7
    Tytuł:
    Deposition and Characterization of CdS, CuS and ZnS Thin Films Deposited by SILAR Method
    Autorzy:
    Guzeldir, B.
    Saglam, M.
    Ates, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/1490738.pdf
    Data publikacji:
    2012-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.05.-a
    61.05.cp
    61.72.uj
    Opis:
    Cadmium sulfide, copper sulfide and zinc sulfide films were grown on Si(111) substrate by successive ionic layer adsorption and reaction method at room temperature. The crystalline structure and morphology of obtained films were characterized by X-ray diffraction, scanning electronic microscope and energy dispersive X-ray analysis methods. The films were polycrystalline and showed preferred orientation. The surface morphology of these films looked relatively smooth and homogeneous in the scanning electron microscope image. The energy dispersive X-ray analysis spectra showed that the expected elements exist in the thin films.
    Źródło:
    Acta Physica Polonica A; 2012, 121, 1; 33-35
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characteristics of Ba-Doped PbS Thin Films Prepared by the SILAR Method
    Autorzy:
    Gülen, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/1205230.pdf
    Data publikacji:
    2014-08
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.05.-a
    61.05.cp
    68.55.Ln
    Opis:
    In this material production research, undoped and Ba-doped nanostructured PbS films are fabricated on glass surfaces by SILAR method. The structural, optical and morphological properties of the films are examined via scanning electron microscopy, UV-vis spectrophotometry and X-ray diffraction analysis. Scanning electron microscopy analysis revealed that Ba-doping concentration influences the size of the thin film's nanoparticles. X-ray diffraction results showed that all of the thin films are in a face centered cubic structure. Optical studies, in the room temperature, revealed that the optical band gap of the films increases as Ba-doping concentration is increased. The intercept values on the energy axis in the range of 1.86 eV and 2.12 eV for 1% and 8% Ba-doped PbS films respectively. As a result, it is concluded that the structural, optical and morphological properties of the fabricated thin films are directly depend on the Ba doping ratio.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 3; 763-767
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Focused Ion Beam Imaging of Defects in Multicrystalline Si for Photovoltaic Application
    Autorzy:
    Miyamura, Y.
    Sekiguchi, T.
    Chen, J.
    Li, J.
    Watanabe, K.
    Kumagai, K.
    Ogura, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/1198415.pdf
    Data publikacji:
    2014-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.05.-a
    61.85.+p
    61.72.Ff
    Opis:
    We demonstrate the imaging of the extended defects in Si materials using a focused ion beam instrument. Since Ga-ion beam has small penetration depth and high channeling character compared with electron beam, the secondary electron signal of focused ion beam is more sensitive to the surface morphology and crystallinity. We have tried to use this secondary electron imaging of focused ion beam for observation of various extended defects in Si materials for photovoltaic and semiconductor devices. As for the texture of multicrystalline Si, some grains are imaged darker than the others. It suggests that the crystal orientation gives different channeling effect on the primary Ga-ion beam, resulting in the different secondary electron yield. The grain boundaries and lineage in multicrystalline Si are shown as bright lines and patterns in the image. Although it may reflect the surface morphologies, these contrasts may be attributed to the channeling contrast due to lattice displacement or distortion. The contrast mechanism of FIB imaging is discussed.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 4; 991-993
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Positronium time-of-flight Measurements of Mesoporous Silica Films
    Autorzy:
    Kuang, Peng
    Zhang, Xiao
    He, Chun
    Cao, Xing
    Wang, Bao
    Powiązania:
    https://bibliotekanauki.pl/articles/1029796.pdf
    Data publikacji:
    2018-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.70.Bj
    61.05.-a
    68.47.Mn
    Opis:
    Mesoporous silica films were synthesized with various concentrations of cetyltrimethylammonium bromide (CTAB) in precursor sols through the method of electro-assisted self-assembly (EASA). Oriented pore channels were observed in the films prepared with more CTAB in the precursor sols. Positronium time-of-flight (Ps-TOF) measurements were performed for the silica films with different porous structures. It is demonstrated that the Ps emission intensity and energies are well correlated to the apparent porosity, pore interconnectivity and possibly pore channel orientation. The results indicate that Ps-TOF can be a useful technique for probing the structures of porous films.
    Źródło:
    Acta Physica Polonica A; 2018, 133, 1; 3-6
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    XRD Analysis of Synthetic Diamond Powders Irradiated with Electrons
    Autorzy:
    Shishonok, E.
    Luhin, V.
    Koltunowicz, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/1402231.pdf
    Data publikacji:
    2015-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.05.-a
    61.43.Gt
    61.50.-f
    61.80.Fe
    Opis:
    Powders of synthetic diamond with low strength were sorted on sets with a different grain size. The synthetic diamond sets had various crushing strengths and morphology. They were irradiated with high energy electrons (6.5 MeV, D=2×10¹⁹ cm¯²) and analyzed using X-ray diffraction (Cu K_α) before and after irradiation. As established from nonlinearity of the a(Θ)=f{R(Θ)} dependences and observed extra splittings in X-ray diffraction patterns (in addition to α₁-α₂ doublets), crystal lattice of synthetic diamond from different sets was variously distorted. Irradiation led to decreasing distortions more significantly, the higher the initial strength of the set was. The made conclusions coincide well with our previous results on synthetic diamond powders which were irradiated under various softer conditions with direct measurements of synthetic diamond crushing strength without X-ray diffraction analysis. X-ray diffraction allows to presort synthetic diamond of critically low relative mechanical strength as well as evaluate resistance of diamond crystal lattice against heavy irradiation and other external impacts.
    Źródło:
    Acta Physica Polonica A; 2015, 128, 5; 912-914
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Requirement for and Use of Coated P92 Steel for Enhanced Structural Integrity at High Temperature
    Autorzy:
    Hoey, T.
    Chen, R.
    McCartney, D.
    Sun, W.
    Mansfield, J.
    Barnard, P.
    Foster, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1402066.pdf
    Data publikacji:
    2015-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.15.Pq
    68.37.-d
    61.05.-a
    64.75.-g
    Opis:
    To achieve climate change targets and to improve the efficiency of fossil fuel power plant the temperature and pressure of operation must be increased. With steam temperatures predicted to rise by 50-100 K in the next 30 years, this presents a number of material challenges, not least for the ferritic steels used for steam pipework. Currently the best in class ferritic steel for power plant steam pipework is P92, a 9-12% Cr advanced martensitic steel that was developed for its superior high temperature creep resistance. This paper will give a brief overview of P92 microstructure, composition and metallurgy and identify experimentally and computationally some key features of the material. As well as failure by creep, P92 at high temperature also suffers from steam oxidation damage. Recent literature suggests that coatings applied to P92 are a very promising solution. A short review of previous work on steam oxidation resistant coatings for P92 is included. A novel Co-Cr-C coating that has not previously been explored for this application is described. Experimental and computational characterisation is included.
    Źródło:
    Acta Physica Polonica A; 2015, 128, 4; 514-519
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Comparative Study of the Microstructure and Phase Composition of Nanoausferritic Ductile Iron Alloy Using SEM, TEM, Magnetometer, and X-Ray Diffraction Methods
    Autorzy:
    Skołek, E.
    Giętka, T.
    Świątnicki, W.
    Myszka, D.
    Powiązania:
    https://bibliotekanauki.pl/articles/1033075.pdf
    Data publikacji:
    2017-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.05.-a
    06.60.Mr
    81.05.Bx
    81.07.Bc
    81.40.-z
    81.40.Ef
    81.40.Gh
    Opis:
    In this paper the microstructure and phase composition of ausferritic ductile iron alloy were investigated by scanning electron microscopy, transmission electron microscopy and X-ray diffraction methods. In order to obtain the nanoausferritic microstructure in the alloy, the austempering heat treatment was performed at relatively low temperature. As a result, a specific kind of microstructure, containing nanocrystalline ausferrite and retained austenite blocks, was obtained in each heat-treated sample. The volume fractions of phases were determined using different methods: MicroMeter software for scanning electron micrographs, stereological analysis for transmission electron micrographs, quantitative analysis of the X-ray diffraction spectra and magnetometer measurements. All methods revealed a high amount of retained austenite which varied as a function of the austempering treatment parameters. It was shown that the quantitative phase composition measured by X-ray diffraction and magnetometer, in all samples investigated, differs significantly from the stereological measurements and image analysis performed through the MicroMeter software. The possible reasons of the observed differences were discussed.
    Źródło:
    Acta Physica Polonica A; 2017, 131, 5; 1319-1323
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-7 z 7

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