- Tytuł:
- Improved Synthesis of Glycidyl Nitrate in the Presence of 5-Aminotetrazolium Nitrate: a New Method Optimised Using the Taguchi Method
- Autorzy:
-
Bayat, Y.
Mohammadi, M. M. - Powiązania:
- https://bibliotekanauki.pl/articles/358882.pdf
- Data publikacji:
- 2016
- Wydawca:
- Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
- Tematy:
-
glycidyl nitrate
5-aminotetrazolium nitrate
chloro-epoxy-propane
Taguchi method - Opis:
- This paper describes a method for increasing the yield of glycidyl nitrate from chloro-epoxypropane and dilute nitric acid, in the presence of 5-aminotetrazolium nitrate. The presence of 5-aminotetrazolium nitrate as catalyst and co-nitrating agent, enabled glycidyl nitrate to be produced smoothly and in excellent yield under mild condition. The optimal reaction conditions were obtained by the Taguchi method, increasing the yield from 66 to 81%. The product was characterized by FTIR and 1H NMR spectroscopy.
- Źródło:
-
Central European Journal of Energetic Materials; 2016, 13, 3; 579-591
1733-7178 - Pojawia się w:
- Central European Journal of Energetic Materials
- Dostawca treści:
- Biblioteka Nauki
Artykuł