- Tytuł:
- Optimization of production process of epoxidized soybean oil with high oxygen content through response surface methodology
- Autorzy:
-
Zhang, Fengyan
Dong, Yonglu
Lin, Sudong
Gui, Xuefeng
Hu, Jiwen - Powiązania:
- https://bibliotekanauki.pl/articles/27315650.pdf
- Data publikacji:
- 2023
- Wydawca:
- Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
- Tematy:
-
soybean oil
response surface methodology
epoxidation
oxirane value - Opis:
- The epoxidation process of soybean oil (SBO) and peracid produced by 50 wt% hydrogen peroxide (H2O2) and formic acid (FA) was studied with sulfuric acid (H2SO4) as a catalyst. Three reaction parameters, including reaction temperature, FA-to-SBO ratio, and H2O2-to-SBO ratio, were investigated, along with the combined effect on oxirane value (OV). Based on response surface methodology (RSM), the Box-Behnken design (BBD) was used to optimize the process parameters. According to the results, the calculated OV (7.34%) and the experimental OV (7.31%) were significantly in agreement. The product was con firmed as epoxidized soybean oil (ESO) by IR and NMR characterization methods. These results demonstrated the reliability of RSM to optimize the SBO reaction to produce ESO with high oxygen content.
- Źródło:
-
Polish Journal of Chemical Technology; 2023, 25, 2; 21--29
1509-8117
1899-4741 - Pojawia się w:
- Polish Journal of Chemical Technology
- Dostawca treści:
- Biblioteka Nauki