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Wyświetlanie 1-15 z 17
Tytuł:
Simultaneous photooxidation and photoreduction of phenol and Cr(VI) ions using titania modified with nanosilica
Autorzy:
Kądziołka, Daria
Grzechulska-Damszel, Joanna
Schmidt, Beata
Powiązania:
https://bibliotekanauki.pl/articles/2174823.pdf
Data publikacji:
2022
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
photocatalysis
titanium dioxide
nanosilica
water purification
Opis:
The photocatalytic process of phenol oxidation and Cr(VI) reduction in the presence of nano-silica modified titania was carried out. The activity of composites was tested using two different light sources. The photocatalysts with 10% of nanosilica showed the highest activity. The calcination temperature (200–800 °C) significantly determined the sensitivity of the obtained materials to the light source used. Photocatalysts alternately adsorbed and desorbed Cr(VI) ions from the reaction mixture during irradiation. In the one-component mixture, complete oxidation of phenol was observed using material calcined at 650 °C, after 3 h of UV-VIS irradiation. In the reaction mixture of Cr(VI) and phenol, the highest activity was demonstrated by photocatalyst calcined at 300 °C. The concentration of phenol decreased in proportion to the decrease of chromium ions. The obtained titania-silica composites showed oxidizing properties towards phenol and reductive properties toward Cr(VI) ions.
Źródło:
Polish Journal of Chemical Technology; 2022, 24, 4; 23--29
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Degradation of sertraline in water by suspended and supported TiO2
Autorzy:
Rejek, M.
Grzechulska-Damszel, J.
Powiązania:
https://bibliotekanauki.pl/articles/780043.pdf
Data publikacji:
2018
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
photocatalysis
titanium dioxide
pharmaceuticals
sertraline
water treatment
Opis:
Pharmaceutical pollutants have been detected in many countries in surface and ground water after treatment in wastewater treatment plants. The presented studies concern the photocatalytic removal of one of SSRI antidepressants - sertraline from water using TiO2  photocatalyst. The process was conducted using two laboratory installations with periodic and flow reactors. Two forms of TiO2  was used in the photocatalytic reactions: suspended and supported onto a glass fabric. The studies shown that with increasing initial concentration of pharmaceutical, photoactivity decreases. For the initial concentration of 0.025 g/dm3 , the best results – 94% removal – was achieved for the process conducted in the periodic reactor with TiO2  supported onto a glass fabric.
Źródło:
Polish Journal of Chemical Technology; 2018, 20, 2; 107-112
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The influence of sulfur addition on the hazard-type reaction of ilmenite ores with sulfuric acid
Autorzy:
Jabłoński, Maciej
Lubkowski, Krzysztof
Tylutka, Sandra
Ściążko, Andrzej
Powiązania:
https://bibliotekanauki.pl/articles/1849314.pdf
Data publikacji:
2021
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
hazard-type reaction
ilmenite
titanium dioxide pigment
sulfur
Opis:
The paper presents results of thermokinetic investigation of the hazard-type reaction of Norwegian and Australian ilmenite ores with sulfuric acid, modified by the addition of elemental sulfur, to increase the process safety in industrial conditions. In the reactions of both ilmenite ores the addition of sulfur caused a reduction of the thermal power generated in the reaction and a decrease in the value of the thermokinetic parameter ΔTmax/Δτ for almost the whole range of initial concentrations of sulfuric acid. It was also found that the addition of sulfur to the reaction did not negatively affect the degree of ilmenite leaching. The interpretation of the obtained thermokinetic curves allowed to determine safe process conditions for both types of titanium raw materials.
Źródło:
Polish Journal of Chemical Technology; 2021, 23, 3; 17-23
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The influence of sulfur addition on the hazard-type reaction of ilmenite ores with sulfuric acid
Autorzy:
Jabłoński, Maciej
Lubkowski, Krzysztof
Tylutka, Sandra
Ściążko, Andrzej
Powiązania:
https://bibliotekanauki.pl/articles/1849319.pdf
Data publikacji:
2021
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
hazard-type reaction
ilmenite
titanium dioxide pigment
sulfur
Opis:
The paper presents results of thermokinetic investigation of the hazard-type reaction of Norwegian and Australian ilmenite ores with sulfuric acid, modified by the addition of elemental sulfur, to increase the process safety in industrial conditions. In the reactions of both ilmenite ores the addition of sulfur caused a reduction of the thermal power generated in the reaction and a decrease in the value of the thermokinetic parameter ΔTmax/Δτ for almost the whole range of initial concentrations of sulfuric acid. It was also found that the addition of sulfur to the reaction did not negatively affect the degree of ilmenite leaching. The interpretation of the obtained thermokinetic curves allowed to determine safe process conditions for both types of titanium raw materials.
Źródło:
Polish Journal of Chemical Technology; 2021, 23, 3; 17-23
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Modyfication of photocatalytic properties of titanium dioxide by mechanochemical method
Autorzy:
Dulian, P.
Buras, M.
Żukowski, W.
Powiązania:
https://bibliotekanauki.pl/articles/778307.pdf
Data publikacji:
2016
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
mechanochemistry
high-energy ball milling
titanium dioxide
photocatalysis
Opis:
The paper presents a simple way to improve the photocatalytic properties of titanium dioxide using mechanochemical method. The TiO2 (Anatase) powders was subjected to high-energy ball milling in dry environment and in methanol. It has been shown that it is possible to induce the phase transformation from Anatase to Rutile and produce a material with a higher photocatalytic activity in the UV light. Physicochemical characteristics of the products were based on the following methods and techniques: X-ray powder diffraction (XRD), IR and UV-Vis (DR) spectroscopy, measurements of specific surface area (BET). The photocatalytic activity of the powders was measured in the decomposition reaction of methyl orange in water.
Źródło:
Polish Journal of Chemical Technology; 2016, 18, 3; 68-71
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The influence of admixtures on the course of hydrolysis of titanyl sulfate
Autorzy:
Grzmil, B.
Grela, D.
Kic, B.
Podsiadły, M.
Powiązania:
https://bibliotekanauki.pl/articles/779042.pdf
Data publikacji:
2008
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
dwutlenek tytanu
hydroliza
hydrate titanium dioxide
hydrolysis
titanyl sulfate
admixtures
Opis:
The study focused on the question how admixtures, such as iron(II), iron(III), magnesium and aluminium salts influence the degree of TiOSO4 conversion to hydrated titanium dioxide (HTD). Titanyl sulfate solution, an intermediate product in the industrial preparation of titanium dioxide pigments by sulfate route was used. The admixtures were added to the solution and their concentration was gradually changed. It was found that hydrolysis clearly depended on Fe(II) and Fe(III) concentrations. The higher the concentration of iron(II) (up to 5 wt %) in the solution was, the higher conversion degree was achieved. A reverse relationship was observed concerning the influence of iron(III) introduced up to 1.5 wt %. The constant rates of both phases of titanyl sulfate hydrolysis (including the formation of an intermediate colloidal TiO2 and final products) depended on iron(II) and iron(III) content in the solution. The concentration of other constituents did not influence hydrolysis in the investigated part of the process (up to 2.6 wt % of Mg and up to 0.3 wt % of Al). However, the size of primary particles of the obtained TiO2źnH2O did not depend on the content of the above-mentioned constituents in the solution.
Źródło:
Polish Journal of Chemical Technology; 2008, 10, 3; 4-12
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Combination of mesoporous titanium dioxide with MoS2 nanosheets for high photocatalytic activity
Autorzy:
Karimi, L.
Powiązania:
https://bibliotekanauki.pl/articles/778657.pdf
Data publikacji:
2017
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
MoS2 nanosheet
mesoporous titanium dioxide
photocatalytic
ultrasound
direct green 6
Opis:
This study presents a facile approach for the preparation of MoS2  nanosheet decorated by porous titanium dioxide with effective photocatalytic activity. Mesoporous titanium dioxide nanostructures first synthesized by a hydrothermal process using titanium (III) chloride and then the MoS2 /TiO2  were prepared through mixing of MoS2  nanosheet with mesoporous titanium dioxide under ultrasonic irradiation. The synthesized nanocomposite was characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission scanning electron microscopy (FE-SEM), and Brunauer-Emmett-Teller (BET) analysis. The results showed that the nanocomposite has mesoporous structure with specific surface area of 176.4 m2 /g and pore diameter of 20 nm. The as-prepared MoS2 /TiO2  nanocomposites exhibited outstanding photocatalytic activity for dye degradation under sunlight irradiation, which could be attributed to synergistic effect between the molybdenum disulfide nanosheet and mesoporous titanium dioxide. The photocatalytic performance achieved is about 2.2 times higher than that of mesoporous TiO2  alone. It is believed that the extended light absorption ability and the large specific surface area of the 2D MoS2  nanosheets in the nanocomposite, leading to the enhanced photocatalytic degradation activity.
Źródło:
Polish Journal of Chemical Technology; 2017, 19, 2; 56-60
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects of processing parameters on hydrolysis of TiOSO4
Autorzy:
Grzmil, B.
Grela, D.
Kic, B.
Powiązania:
https://bibliotekanauki.pl/articles/778719.pdf
Data publikacji:
2009
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
dwutlenek tytanu
hydroliza
siarczan tytanylu
hydrate titanium dioxide
hydrolysis
titanyl sulfate
Opis:
The influence of both TiOSO4 concentrations in the starting solution and a way of conducting hydrolysis on the degree of titanyl sulphate conversion to hydrated titanium dioxide were studied. Titanyl sulphate solution, an intermediate product in the commercial preparation of titanium dioxide pigments by sulphate method, was used. The continuous method of conducting hydrolysis was applied using one or two reactors connected in series. It was found that the degree of hydrolysis markedly depends on the studied parameters. It was also found that TiOSO4 hydrolysis using the continuous method should be conducted: i) at a possibly low concentration of free sulfuric acid in the solution and; ii) in two or more rectors connected in series.
Źródło:
Polish Journal of Chemical Technology; 2009, 11, 3; 15-21
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preliminary studies of photocatalytic activity of gypsum plasters containing TiO2 co-modified with nitrogen and carbon
Autorzy:
Janus, M.
Bubacz, K.
Zatorska, J.
Kusiak-Nejman, E.
Czyżewski, A.
Morawski, A. W.
Powiązania:
https://bibliotekanauki.pl/articles/778867.pdf
Data publikacji:
2015
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
titanium dioxide
gypsum
TiO2/N
self-cleaning
Reactive Red 198
Opis:
The conducted studies were focused on the development of the gypsum material exhibiting self-cleaning properties. To this end, the raw gypsum was mixed with unique TiO2-based photocatalysts, previously modified by nitrogen and/ or carbon doping. The photocatalytic activity of the obtained gypsum plasters was evaluated trough the degradation of model organic compound (Reactive Red 198) under UV-vis irradiation. The impact of the photocatalysts presence on the physicochemical properties of the obtained gypsum plasters was evaluated. Furthermore, the role of non-metals presence on the photocatalytic properties of the TiO2 was determined. It was confirmed that the addition of N,C co-modified titanium dioxide into gypsum bestows this material with self-cleaning properties. The highest dye removal rate was displayed by the gypsum plaster containing optimal amount (10 wt%) of co-modified TiO2/N,C photocatalyst, after 20 hours of UV-vis irradiation.
Źródło:
Polish Journal of Chemical Technology; 2015, 17, 2; 96-102
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of titanium dioxide modification on the antibacterial properties
Autorzy:
Rokicka, P.
Markowska-Szczupak, A.
Kowalczyk, Ł.
Kowalska, E.
Morawski, A. W.
Powiązania:
https://bibliotekanauki.pl/articles/778569.pdf
Data publikacji:
2016
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
antibacterial properties
Escherichia coli K12
modified photocatalysts
titanium dioxide
visible-responsive photocatalysts
Opis:
Antibacterial properties of 15 titania photocatalysts, mono- and dual-modified with nitrogen and carbon were examined. Amorphous TiO2 , supplied by Azoty Group Chemical Factory Police S.A., was used as titania source (Ar-TiO2 , C-TiO2 , N-TiO2 ;2 and N,C-Ti2 2 calcined at 300°C, 400°C, 500°C, 600°C, 700°C). The disinfection ability was examined against Escherichia coli K12 under irradiation with UV and artificial sunlight and in dark conditions. It has been found the development of new photocatalysts with enhanced interaction ability with microorganisms might be a useful strategy to improve disinfection method conducted under artificial sunlight irradiation. The efficiency of disinfection process conducted under artificial sunlight irradiation with carbon (C-TiO2 ) and carbon/nitrogen (N,C-TiO2 ) photocatalysts was similar as obtained under UV irradiation. Furthermore, during dark incubation, any toxicity of the photocatalyst was noted.
Źródło:
Polish Journal of Chemical Technology; 2016, 18, 4; 56-64
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Water purification using a novel reactor with the photoactive refill
Autorzy:
Grzechulska-Damszel, J.
Morawski, A.W.
Powiązania:
https://bibliotekanauki.pl/articles/779398.pdf
Data publikacji:
2009
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
dwutlenek tytanu
fotokataliza
reaktor przepływowy
barwniki organiczne
titanium dioxide
photocatalysis
flow reactor
photoactive coating
organic dyes
Opis:
The aim of the presented work was the removal of organic dye, Acid Red 18, from water using a novel reactor with the photoactive refill. Titanium dioxide was immobilized on the base material as a thin layer from the alcoholic suspension followed by thermal stabilization. The prepared coating exhibits high stability in repeated cycles of water treatment. The complete removal of colour was achieved in a relatively short time of 14 hours. The proposed reactor with the photoactive refill solves the problem of the necessity of the replacement of the reactor or parts of the reactor when the photocatalysts activity decreases. In the case of activity drop of the photocatalyst, only the photoactivve refill can be easily replaced.
Źródło:
Polish Journal of Chemical Technology; 2009, 11, 1; 61-63
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Removal of organic dye in the hybrid photocatalysis/membrane processes system
Autorzy:
Grzechulska-Damszel, J.
Morawski, A.W.
Powiązania:
https://bibliotekanauki.pl/articles/779880.pdf
Data publikacji:
2007
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
dwutlenek tytanu
fotokataliza
procesy membranowe
barwniki organiczne
układy hybrydowe
titanium dioxide
photocatalysis
membrane processes
organic dyes
hybrid systems
Opis:
The removal of azo dye Acid Red 18 in hybrid photocatalysis/membrane processes systems was investigated. The photocatalytic reactions were conducted in the reactor with photocatalyst suspended in the solution. The reaction solution was recirculated through the ultrafiltration system. A commercially available titanium dioxide (AeroxideŽ P25, Degussa, Germany) was used as a photocatalyst. The solution after the photocatalytic/UF reaction was applied as the feed for the membrane distillation process. The changes of various parameters, including the concentration of the dye, pH and the conductivity of the solution, TOC and TDS content were analyzed during the process. It was found that azo dye Acid Red 18 could be successfully decolourised in the hybrid photocatalysis/UF system. The catalyst particles were retained in the feed solution by means of the ultrafiltration membrane so the obtained permeate was free of TiO2. The application of ultrafiltration together with the photocatalytic process results in the separation of photocatalyst from the treated solution but does not give the complete removal of organic matter from the reaction mixture. Membrane distillation applied with the permeate after the photocatalysis/UF process as a feed gives a complete separation of TOC from the treated solution and the obtained product is practically pure water.
Źródło:
Polish Journal of Chemical Technology; 2007, 9, 2; 94-98
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A preliminary study on antifungal effect of TiO2-based paints in natural indoor light
Autorzy:
Markowska-Szczupak, A.
Ulfig, K.
Grzmil, B.
Morawski, A. W.
Powiązania:
https://bibliotekanauki.pl/articles/778079.pdf
Data publikacji:
2010
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
działanie przeciwgrzybicze
dwutlenek tytanu
naturalne światło w pomieszczeniach
fotokatalizy
antifungal activity
titanium dioxide
natural indoor light
photocatalysis
Opis:
The antifungal activity of four commercial photocatalytic paints (KEIM Ecosil ME, Titanium FA, Photo Silicate and Silicate D) in natural indoor light was investigated. The paints contained TiO2 in rutile and anatase crystalline forms as evidenced by means of the X-ray diffraction analysis. In most cases the paints inhibited growth of fungi viz. Trichoderma viride, Aspergillus niger, Coonemeria crustacea, Eurotium herbariorum, and Dactylomyces sp . The KEIM Ecosil ME paint displayed the highest antifungal effect in the light, which could be explained with the highest anatase content. The paint antifungal activity and the fungal sensitivity to the TiO2- mediated photocatalytic reaction both decreased in the following orders: KEIM Ecosil ME > Titanium FA > Photo Silicate > Silicate D and T. viride > Dactylomyces sp. > A. niger > E. herbariorum.
Źródło:
Polish Journal of Chemical Technology; 2010, 12, 4; 53-57
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Dye decomposition on P25 with enhanced adsorptivity
Autorzy:
Janus, M.
Wawrzyniak, B.
Tryba, B.
Morawski, A.W.
Powiązania:
https://bibliotekanauki.pl/articles/779704.pdf
Data publikacji:
2008
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
fotokatalizator
N-domieszkowanie
dwutlenek tytanu
barwnik azowy
visible-light active photocatalyst
N-doped
titanium dioxide
azo dye
Opis:
The preparation method and the activity of the TiO2-P25/N doped photocatalyst based on commercial titanium dioxide (TiO2 AeroxideŽ P-25 Degussa, Germany) are presented. For the TiO2-P25/N preparation TiO2-P25 and gaseous ammonia were kept in a pressure reactor (10 bars) for 4 hours at the temperature of 200°C. This modification process changed the chemical structure of the TiO2 surface. The formation of NH4+ groups was confirmed by the FTIR measurements. Two bands in the range of ca. 1430 - 1440 cm-1 attributed to bending vibrations of NH4+ could be observed on the FTIR spectra of the catalysts modified with ammonia and the band attributed to the hydroxyl groups at 3300 - 3500 cm-1, which were not reduced after N-doping. The photocatalytic activity of the photocatalysts was checked through the decomposition of two dyes under visible light irradiation. The modified TiO2 thus prepared samples were more active than TiO2-P25 for the decomposition of dyes under visible light irradiation.
Źródło:
Polish Journal of Chemical Technology; 2008, 10, 2; 11-16
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation of cobalt titanates via co-precipitation while using industrial intermediates as titanium precursors
Autorzy:
Przepiera, A.
Płaska, J.
Przepiera, K.
Jabłoński, M.
Konratowska, A.
Powiązania:
https://bibliotekanauki.pl/articles/779320.pdf
Data publikacji:
2009
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
związki tytanu
tytanian kobaltu
otrzymywanie tytanianu kobaltu
siarczan tytanylu
dwutlenek tytanu
titanium compounds
cobalt titanates preparation
titanyl sulfate
hydrous titanium dioxide
Opis:
This paper reports on the results of cobalt titanates preparation by calcination of green bodies obtained by a co-precipitation method. For the investigations were used: as titanium sources, acidic solutions of titanyl sulfate and hydrous titanium dioxide, originating from the production process of titanium dioxide by sulfate method. The composition of the obtained materials was determined using titration methods. The calcined powders were characterized by X-ray diffraction method. It has been found that the obtained products are composed of cobalt methatitanate CoTiO3 or cobalt orthotitanate Co2TiO4 occurring as single phases, and also as cobalt titanates and titanium dioxide phase mixtures. The proposed method of proceeding can be used for the preparation of series of transition metals titanates, such as nickel, iron, zinc, copper and also aluminium titanates.
Źródło:
Polish Journal of Chemical Technology; 2009, 11, 2; 51-54
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 17

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