Temat: SEM, - Katalog OPAC zbiorów

Skocz do pozycji: 1.

Tytuł:: The influence of technological PVD process parameters on the topography, crystal and molecular structure of nanocomposite films containing palladium nanograins
Autorzy:: Rymarczyk, J.
Czerwosz, E.
Kozłowski, M.
Dłużewski, P.
Kowalski, W.
Powiązania:: https://bibliotekanauki.pl/articles/778619.pdf
Data publikacji:: 2014
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:: palladium
carbon
SEM
AFM
TEM
FTIR
Opis:: The paper describes the preparation and characteristics of films composed of Pd nanograins placed in carbonaceous matrix. Films were obtained in PVD (Physical Vapor Deposition) process from two sources containing: the first one – fullerene powder and the second one – palladium acetate. The topographical, morphological and structural changes due to different parameters of PVD process were studied with the use of Atomic Force Microscopy and Scanning Electron Microscopy, whereas the structure was studied with the application of the Transmission Electron Microscopy and Fourier Transform Infrared Spectroscopy methods. It was shown that topographical changes are connected with the decomposition ratio of Pd acetate as well as the form of carbonaceous matrix formed due to this decomposition. Palladium nanograins found in all films exhibit the fcc structure type and their diameter changes from 2 nm to 40 nm depending on the PVD process parameters.
Źródło:: Polish Journal of Chemical Technology; 2014, 16, 3; 18-24
1509-8117
1899-4741
Pojawia się w:: Polish Journal of Chemical Technology
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 2.

Tytuł:: A study on damage to PLA knitted fabrics during scouring and bleaching
Autorzy:: Baig, G. A.
Carr, C. M.
Powiązania:: https://bibliotekanauki.pl/articles/778625.pdf
Data publikacji:: 2014
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:: PLA
Scouring
Bleaching
Weight loss
mechanical properties
SEM
Opis:: Ingeo® PLA (polylactic acid) knitted fabric was scoured through an exhaust technique. The scouring was carried out with sodium carbonate in the presence of a detergent at various concentrations and temperatures. The scoured fabric was bleached with various oxidative bleaching agents. Bleaching was carried out with hydrogen peroxide, sodium chlorite and sodium hypochlorite. Hydrogen peroxide was applied by exhaust and cold pad batch (CPB) techniques. It was observed that during scouring PLA fabric was degraded at high alkali concentrations and processing temperatures. The scouring temperature above 60^oC proved to be deleterious due to the scouring solution penetrating into the polymer structure and damaged the fiber. Sodium chlorite and sodium hypochlorite caused little damage to the mechanical properties of PLA. Hydrogen peroxide when applied by the CPB technique did not reduce strength appreciably but when applied by the exhaust technique decreased the strength significantly. SEM analysis revealed that hydrogen peroxide caused holes and slit formation in the fiber structure.
Źródło:: Polish Journal of Chemical Technology; 2014, 16, 3; 45-50
1509-8117
1899-4741
Pojawia się w:: Polish Journal of Chemical Technology
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 3.

Tytuł:: Study on the improvement of hydrophilic character on polyvinylalcohol treated polyester fabric
Autorzy:: Pitchai, S.
Jeyakodi, M. J.
Swarna, N.
Powiązania:: https://bibliotekanauki.pl/articles/778355.pdf
Data publikacji:: 2014
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:: Polyester fabric
PVA
SEM
FTIR
DSC
hydrophilic charakter
Opis:: Polyester fabric was treated with polyvinyl alcohol in alkaline medium. The moisture regain, water retention and wettability of the PVA treated polyester fabric were tested. The PVA treated PET fabric was dyed with disperse dye. The presence of PVA in the treated PET fabric was assessed by spot test. The treated fabric was also characterized by scanning electron microscope, FTIR and differential scanning calorimetry. The PVA treated poliester fabric showed improved hydrophilic character over intact and sodium hydroxide treated PET fabrics.
Źródło:: Polish Journal of Chemical Technology; 2014, 16, 4; 21-27
1509-8117
1899-4741
Pojawia się w:: Polish Journal of Chemical Technology
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 4.

Tytuł:: The influence of mercury content on the structural changes of bioindicator surfaces
Autorzy:: Szynkowska, M.I.
Pawlaczyk, A.
Powiązania:: https://bibliotekanauki.pl/articles/778709.pdf
Data publikacji:: 2007
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:: rtęć
analiza powierzchni
bioindykator
SEM
mercury
surface analysis
bioindicators
Opis:: This work examines the recommended chemical analytical method for the identification and detecting mercury from the environmental media. The aim of this study was to establish a correlation between mercury content in different biological indicators like: human hair, mushrooms, lichen, moss and needle samples, and the changes in the structure of the investigated material. We have explored the possibilities of using the SEM method in environmental studies to investigate a variety of biological samples coming from areas at different pollution state. We have combined the information from the quantity measurements with the qualitative analysis. The total content of Hg was determined using the Automatic Mercury Analyzer SP-3D. The accuracy of the applied method was verified by an analysis of proper certificate materials: Mixed Polish Herbs INCT-MPH-2, Lichen CRM 482, Pine needles 1575a and Human Hair NCS ZC 81002. The obtained results proved a direct influence of the content of mercury and environmental pollution on the damage of the structure of the studied samples.
Źródło:: Polish Journal of Chemical Technology; 2007, 9, 4; 115-120
1509-8117
1899-4741
Pojawia się w:: Polish Journal of Chemical Technology
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 5.

Tytuł:: Inhibitive tendency of zinc gluconate for aluminium alloy in sulphuric acid solution
Autorzy:: Sanni, O.
Loto, C. A.
Popoola, A. P. I.
Powiązania:: https://bibliotekanauki.pl/articles/780091.pdf
Data publikacji:: 2013
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:: aluminium
zinc gluconate
inhibition
weight loss
potentiodynamic polarization
SEM/EDS
Opis:: The corrosion inhibition of aluminium alloy in 0.5M H2SO4 solution in the presence of zinc gluconate at 301 K was investigated using weight loss and an electrochemical method. Surface analysis of the aluminium alloy sample was reviewed by a high resolution scanning electron microscope equipped with energy dispersive spectroscopy (HRSEM/ EDS). The readings were taken after 48 h for 28 days while the concentration of the inhibitor was varied from 0.5 to 2.0% g/v with an interval of 0.5. The result of the investigation shows that zinc gluconate has a good corrosion inhibition effect for aluminium alloy in 0.5 molar sulphuric acid solution and its efficiency attains more than 67% at 1.5% g/v concentration of zinc gluconate at 301 K. The potentiodynamic polarization data showed that zinc gluconate acts as a mixed type corrosion inhibitor. The adsorption of zinc gluconate on aluminium alloy has been found to obey Freundlich adsorption isotherm at all the concentration of zinc gluconate studied. The results obtained from different methods are in good agreement.
Źródło:: Polish Journal of Chemical Technology; 2013, 15, 4; 60-64
1509-8117
1899-4741
Pojawia się w:: Polish Journal of Chemical Technology
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 6.

Tytuł:: Evaluation of colloidal silica obtained via the co-precipitation method using octane as an organic phase
Autorzy:: Jesionowski, T.
Tepper, B.
Krysztafkiewicz, A.
Powiązania:: https://bibliotekanauki.pl/articles/778627.pdf
Data publikacji:: 2007
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:: krzemionka strącana
emulsja
mikroskopia skaningowa
sedymentacja
zwilżalność
precipitated silica
emulsion
PSD
SEM
sedimentation
wettability
Opis:: The studies were conducted on the production of silica from emulsion systems by co-precipitation from solutions of sodium metasilicate and hydrochloric acid and octane were used as an organic medium. The obtained products were subjected to a comprehensive physicochemical analysis in order to define their dispersive and morphological properties. Particle diameters and polydispersity were determined by the NIBS (non-invasive back scattering) method while the shape and morphology of the particles were established using scanning electron microscopy (SEM). In order to determine the adsorptive properties of the obtained monodisperse silicas, isotherms of nitrogen adsorption/desorption on their surfaces were determined. Using the isotherms, also the specific surface area, the diameter and the volume of the pores were established. In order to define the hydrophilic/hydrophobic character of the products, profiles of wettability and of sedimentation in water were examined. The obtained products were well wettable with water and an increase in their weight depended on the amount of the applied surfactants. The particles of the precipitated silicas manifested a defined, spherical shape and showed a relatively low polydispersity.
Źródło:: Polish Journal of Chemical Technology; 2007, 9, 4; 1-4
1509-8117
1899-4741
Pojawia się w:: Polish Journal of Chemical Technology
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 7.

Tytuł:: Application of the TOF-SIMS and SEM-EDS methods to assess the influence of dusting from a phosphate waste deposal place based on hair analysis
Autorzy:: Szynkowska, M.I.
Leśniewska, E.
Pawlaczyk, A.
Rogowski, J.
Paryjczak, T.
Powiązania:: https://bibliotekanauki.pl/articles/778695.pdf
Data publikacji:: 2007
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:: fosfogips
analiza powierzchni
włos
SEM-EDS
ToF-SIMS
phosphogypsum
surface analysis
hair
TOF-SIMS
Opis:: In this work, scanning electron microscopy with energy dispersive X-ray spectrometry (SEM-EDS) and the time-of-flight secondary ion mass spectrometry (TOF-SIMS) were used to study the particles present on the hair surface of the inhabitants of Wislinka (people environmentally exposed due to the closeness of a dump) in order to obtain the information about the possible influence of dusting from a phosphate waste deposal place. Additionally, the morphology and the composition of fresh phosphogypsum were analyzed. Waste phosphogypsum is formed in the process of a wet phosphoric acid production and there is still a problem with its storage. A thorough understanding of the composition and chemistry of phosphogypsum seems to be necessary to evaluate its environmental impact comprehensively. The results obtained from these two techniques turned out to be complementary and revealed the information expected.
Źródło:: Polish Journal of Chemical Technology; 2007, 9, 4; 85-90
1509-8117
1899-4741
Pojawia się w:: Polish Journal of Chemical Technology
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 8.

Tytuł:: Mycoremediation of Heavy Metals Contaminated Soil by Using Indigenous Metallotolerant Fungi
Autorzy:: Akram, Muhammad Bilal
Khan, Ibrar
Ur Rehman, Mujaddad
Sarwar, Abid
Ullah, Najeeb
ur Rahman, Shafiq
Aziz, Tariq
Alharbi, Metab
Alshammari, Abdulrahman
Alasmari, Abdullah F.
Powiązania:: https://bibliotekanauki.pl/articles/27315654.pdf
Data publikacji:: 2023
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:: Mycoremediation
Heavy Metals Contaminated Soil
Korangi Industrial Estate
FTIR
Fourier Transform Infrared Spectroscopy
SEM
Scanning Electron Microscope
Opis:: The present study was aimed to identify the indigenous fungal strains which could possibly be applied to the bioremediation of heavy metal-contaminated soil. The contaminated soil samples of Korangi Industrial Estate Karachi were found to have total concentration of Cu 1.044 mgL1 , and Pb 0.631 mgL–1. A total of eight indigenous strains of the fungus were isolated and screened for bioremediation capacity from heavy metals-contaminated soil. For the bioremediation of Lead (Pb) these same indigenous eight fungal strains were used for biological remediation. All the fungal isolated with enhanced bioremediation capability were through phenotypic and genotypical characterization. The topology of the phylograms established that the fungal isolates used in this study were allocated to: K1 (Penicillium notatum), K2 (Aspergillus parasiticus), K3 (Aspergillus fumigatus), K4 (Aspergillus flavus), K5 (Aspergillus terries), K6 (Fusarium solani), K7 (Penicillium chrysogenum), K8 (Aspergillus niger), K9 (Penicillium piceum) and K10 (Penicillium restrictum). Thus, K8 fungal isolate was found to be more efficient with maximum bioremediation capacity, for copper and lead removal efficiency, and selected for FTIR and SEM to find out the uptake of Cu and Pb which of the functional groups are involved, and further to detect the effects of bioleaching of both heavy metals on to the surface of K8 fungus biomass. The current study indicates that indigenous fungal isolates could be used with high potency to remediate or clean up the heavy metals-contaminated soil either by the technique of in situ or ex-situ bioremediation.
Źródło:: Polish Journal of Chemical Technology; 2023, 25, 3; 1--13
1509-8117
1899-4741
Pojawia się w:: Polish Journal of Chemical Technology
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 9.

Tytuł:: Morphology and mechanical properties of polyamide 12 (PA12)/poly(vinylidene fluoride) (PVDF) blends
Autorzy:: Ratajska, A.M.
Kulak, W.P.
Poeppel, A.
Seyler, A.
Roslaniec, Z.
Powiązania:: https://bibliotekanauki.pl/articles/778730.pdf
Data publikacji:: 2009
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:: mieszaniny
mieszalność
polifluorek winylidenu
właściwości mechaniczne
blends
miscibility
polyamide 12 (PA12)
poly(vinylidene fluoride) (PVDF)
DSC
DMTA
SEM
mechanical properties
Opis:: The morphology, thermal and mechanical properties of polyamide 12 (PA12)/poly(vinylidene fluoride) (PVDF) blends were investigated. These polymers are engineering, semi-crystalline polymers which are reciprocally immiscible. Differential scanning calorimetry (DSC), dynamic mechanical thermal analysis (DMTA) and scanning electron microscopy (SEM) were used to characterize the polymeric materials. Mechanical properties were examined by static tensile test. The investigations demonstrate that blends with higher amount of PVDF, with the morphology of two co-continuous semicristalline phases, exhibit better mechanical properties. The blends with small content of PVDF and prepared by extrusion show the morphology of small separated domains of PVDF and full continuous PA phase. The morphology of these blends is different than the blends prepared by internal mixer and have better mechanical properties too. Thus they can be used in particular applications without a compatibilizing agent.
Źródło:: Polish Journal of Chemical Technology; 2009, 11, 3; 27-34
1509-8117
1899-4741
Pojawia się w:: Polish Journal of Chemical Technology
Dostawca treści:: Biblioteka Nauki

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