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Wyszukujesz frazę "high-temperature microscope" wg kryterium: Temat


Wyświetlanie 1-2 z 2
Tytuł:
Thermal characterization of halloysite materials for porous ceramic preforms
Autorzy:
Kujawa, M.
Suwak, R.
Dobrzański, L.A.
Gerle, A.
Tomiczek, B.
Powiązania:
https://bibliotekanauki.pl/articles/2175810.pdf
Data publikacji:
2021
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
halloysite
DTA/TG
XRD
high-temperature microscope
linear changes
haloizyt
mikroskop wysokotemperaturowy
zmiany liniowe
Opis:
Purpose: The aim of the study was to investigate the possibility of sintering raw (natural) halloysite and pure halloysite to produce porous ceramic preforms, and determination of sintering temperature based on the results of investigations into thermal effects, linear changes and phase transitions. Design/methodology/approach: Due to mullitisation ability of halloysite at high temperature, alternative applications based on the sintering technology (including the production of reinforcement of metal matrix composites) are being searched for. Pure halloysite and Dunino halloysite were selected for the study. Findings: Pure halloysite, characterized by low impurities, dimensional stability during sintering, softening temperature above 1500ºC and ability to transform into mullite at temperatures above 950ºC could be used as a base for the production of sintered, porous mullite preforms. Research limitations/implications: Presence of impurities in Dunino halloysite, contribute to the shift of the sintering temperature towards lower temperatures and caused a rapid and uncontrolled shrinkage of the sample and the appearance of the softening temperature at 1300ºC. Practical implications: Based on the research of thermal (DTA/TG, linear changes in high-temperature microscopy) and XRD studies it is possible to determine the sintering temperature of pure halloysite to manufacture the porous mullite preforms with open porosity. Originality/value: The received results show the possibility of obtaining the new mullite preforms based on pure halloysite.
Źródło:
Archives of Materials Science and Engineering; 2021, 107, 1; 5--15
1897-2764
Pojawia się w:
Archives of Materials Science and Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The modern approach to manufacturing of carbon-rhenium nanocomposites
Autorzy:
Dobrzańska-Danikiewicz, A. D.
Wolany, W.
Powiązania:
https://bibliotekanauki.pl/articles/2201076.pdf
Data publikacji:
2022
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
rhenium
MWCNTs
multiwall carbon nanotubes
nanocomposites
high-temperature method
SEM
scanning electron microscope
TEM
transmission electron microscopy
ren
wielościenne nanorurki węglowe
nanokompozyt
skaningowa mikroskopia elektronowa
transmisyjna mikroskopia elektronowa
Opis:
Purpose The aim of the paper is to present the high-temperature method of producing MWCNTs-Re nanocomposites, the selection of satisfactory production conditions and the presentation of the results of microscopic and spectroscopic studies of nanocomposites produced by this method. Design/methodology/approach Two methods of manufacturing carbon-rhenium nanocomposites were tested: ineffective chemical synthesis and high-temperature reduction using H2, which was proven successful and allowed the production of nanocomposites with the expected properties. The received nanocomposites were investigated using Transmission Electron Microscope (TEM), and Scanning Electron Microscope (SEM), as well as were subjected to spectroscopic examination. Findings The article presents three steps of MWCNTs-Re nanocomposites fabrication using the high-temperature method, functionalization, impregnation and reduction. As part of own work, satisfactory conditions for producing those nanocomposites using a materials science and heuristic analysis were selected. Research limitations/implications The proposed high-temperature method allows to join rhenium nanoparticles with MWCNTs permanently. It is reasonable to test in the future whether the method is also effective for other carbon nanomaterials and/or nanoparticles of other metals. Practical implications MWCNTs-Re nanocomposites can be used as sensors of gases that are harmful to the environment. It was also confirmed that the MWCNTs-Re_4 nanocomposite has catalytic properties. Originality/value The paper presents a modern approach to the manufacturing of MWCNTs-Re nanocomposites, which assumes the use of a high-temperature furnace to heat the material in a hydrogen atmosphere.
Źródło:
Journal of Achievements in Materials and Manufacturing Engineering; 2022, 115, 2; 57--63
1734-8412
Pojawia się w:
Journal of Achievements in Materials and Manufacturing Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-2 z 2

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