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Wyszukujesz frazę "Sol-gel" wg kryterium: Temat


Wyświetlanie 1-8 z 8
Tytuł:
Soft Chemistry - Synthesis of Nano-Titanium-Doped-Tellerium-Cadmium for Solar Cell Applications
Autorzy:
Elsabawy, Khaled M.
Powiązania:
https://bibliotekanauki.pl/articles/1192983.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Sol-Gel
Hydrolysis
AFM
XRD
Microstructure
SEM
Opis:
Soft chemistry procedures through sol–gel technique has applied to synthesize nano- Ti-doped CdTe composite. Gels were synthesized by the hydrolysis of a complex solution of Si(OC2H5)4, Cd(CH3COO)2•2H2O, Ti(CH3COO)4 and Te were heated from 350 to 600 °C in a H2─N2 atmosphere to form fine cubic CdTe doped crystals. The size of CdTe crystals, determined from the line broadening of X-ray diffraction pattern, increases from 6 to 21 nm in diameter with increasing heat-treatment temperature. Micro-structural features of Ti-doped CdTe crystals were characterized by both of AFM and SEM investigations . The analysis of micro-structural micrographs of both of SEM and AFM indicated that titanium additions improved the crystal growth of grain towards more lower grain size which ranged in between 1.4-2.5 μm while 0.67 μm through Scherrer’s calculations.
Źródło:
World Scientific News; 2016, 36; 61-72
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Studying structural and optical properties of ZnO-CdO nanocomposites
Autorzy:
Abdul-Ameer, Zehraa N.
Agool, Ibrahim R.
Powiązania:
https://bibliotekanauki.pl/articles/1193878.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
CdO
ZnO
ZnO-CdO
nanocomposite
nanocomposites
sol gel
Opis:
Zinc oxide, cadimium oxide and their composites were synthesized in this research using sol-gel method and characterized by X-ray diffraction, to investigate their optical properties using UV-visible, photoluminenscence (PL) spectroscopy, which showed red shift behavior in the ZnO manner enhanced by addition of CdO which noticed through calculations of energy gap.
Źródło:
World Scientific News; 2015, 23; 35-45
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Factors Affecting of Porous Properties of Carbon Gel Microsphere
Autorzy:
Elsayed, M. A.
Powiązania:
https://bibliotekanauki.pl/articles/1194052.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
base catalysts
carbon microsphere
nitrogen adsorption
sol-gel polycondensation
Opis:
Carbon microsphere with high porosity and surface area were synthesized via the sol-gel polycondensation of resorcinol with formaldehyde in a slightly basic medium and followed by drying and pyrolysis. The effects of different parameters during synthesis were investigated. The porous properties of carbon microsphere were evaluated by nitrogen adsorption method and scanning electron microscopy (SEM). By changing both the catalyst species and resorcinol to catalyst ratio (R/C), it was possible to prepare ultramicroporous carbon sphere with pore size about 1.8 nm. The samples evolve from micro-mesoporous solid (RF-Na2CO3: combination of types I and IV isotherms) with 24.2% micropore to an exclusively microporous material (RF-NH4HCO3: type I isotherm) with 98.7% micropore. The results show that it is possible to tailor the morphology of these materials by varying the initial pH of the precursor’s solution in a narrow range and that the micropore surface area and micropore volume are independent from the initial pH, while the BET surface area vary from 582 m2/g (pH = 3.2) to 680 m2/g (pH = 6). However, as the pH increases over pH = 6 the surface area is decreases. These materials can be used as packing for separation columns or as catalysts supports.
Źródło:
World Scientific News; 2015, 13; 80-94
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural and Optical Properties of Sol-Gel Derived Dip-Coated CdO Thin Film
Autorzy:
Kumari, Renu
Kumar, Vipin
Powiązania:
https://bibliotekanauki.pl/articles/1159724.pdf
Data publikacji:
2018
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Band gap
CdO
Sol-gel dip coating
Thin film
Opis:
In this paper CdO thin film has been prepared by sol-gel dip-coating method on glass substrate. The film was characterized by X-Ray diffraction, UV-Visible spectroscopy and photoluminescence spectroscopy for structural and optical properties of CdO thin film. The XRD pattern shows that film is polycrystalline in nature and has a cubical structure with orientation along (111) plane. The diffuse reflectance spectra for the film is studied in wavelength range 400-800 nm. The direct energy band gap of 2.50 eV is found for the film using modified Kubelka-Munk function. Photoluminescence spectra shows one sharp peak at 540 nm due to oxygen vacancy of cadmium oxide.
Źródło:
World Scientific News; 2018, 113; 210-217
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Cd Doping on Structural and Some Optical Studies of Nano CuO Films Prepared by Sol–Gel Technique
Autorzy:
Kadhim, Raheem G.
Ban, Raheem Saleh Kzar
Powiązania:
https://bibliotekanauki.pl/articles/1182823.pdf
Data publikacji:
2017
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Cd
CuO
Sol–Gel Spin Coating Technique
Thin Film
Opis:
This research deals with the study of the structural and optical properties of CuO and Cd doped CuO nano films in thickness 100nm were deposited on a glass substrate using sol-gel spin coating technique. XRD results indicated that the films are polycrystalline and have monoclinic structure with a preferred orientation along ((111).) ̅ and the grain size increase with increasing concentration Cd. Data of AFM indicate that the surface of films is smooth. From SEM image observed the particles are smallest an even particle distribution on a smooth surface. The optical transition in the CuO and (Cd– doped CuO) thin films are observed to be allowed direct transition. The value of the optical energy gap decreases with increasing of (Cd) for all samples.
Źródło:
World Scientific News; 2017, 64; 69-83
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural and Optical Properties of CuO Doped (Li) Thin Films Prepared by Sol-Gel Technique
Autorzy:
Kadhim, Raheem G.
Kzar, Kzar
Powiązania:
https://bibliotekanauki.pl/articles/1188084.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
CuO
Li
Sol-gel
spin coating
x-ray diffraction
UV- Visible
Opis:
CuO and (Li–doped CuO) thin films have been prepared on glass substrates by sol-gel method using spin coating technique. X-ray diffraction (XRD) results reveal that the deposited CuO and (Li– doped CuO) thin films monoclinic crystal structure and the grain size increase with increasing concentration Li. The optical transition in the CuO and (Li– doped CuO) thin films are observed to be allowed direct transition. The value of the optical energy gap decreases with increasing of (Li) for all samples.
Źródło:
World Scientific News; 2016, 56; 56-66
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Substrate Temperature on Structural and Optical Properties of CdO Thin Films
Autorzy:
Ali, H. R. A.
Powiązania:
https://bibliotekanauki.pl/articles/411893.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
cadmium oxide
spray pyrolysis technique
XRD
AFM
thin films
sol-gel
Opis:
Thin films of CdO have been prepared by spray pyrolysis technique. XRD analysis reveals that all the prepared samples were polycrystalline and have preferred orientation along [111] orientation. The surface topography was determined by AFM which indicate that surface roughness and rms roughness were increased by the increasing of substrate temperature. The optical energy gap were determined and its value lies between (2.4-2.5) eV.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 8; 47-55
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and investigation of optical, structural, and morphological characteristics of nanostructured TiO2-ZnO thin films
Autorzy:
Yasir, Nagham Abdulameer
Hlail, Alzubaidy Muneer
Mohsin, Ali Kamel
Powiązania:
https://bibliotekanauki.pl/articles/1070855.pdf
Data publikacji:
2019
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Crystallite size
Photocatalysis
Sol–gel process
Titanium dioxide
X-Ray Diffraction
Zinc oxide
drop casting
energy gap
thin films
Opis:
TiO2-ZnO thin films have been prepared by using drop casting technique. The optical, structural, and morphological properties of nanostructured TiO2-ZnO thin films deposited by drop casting technique was studied by using several experimental techniques were used to characterize optical, structural, and morphological properties; X-Ray Diffraction (XRD) was used to study the crystal structures, the crystallite size, the dislocation density, and the number of crystallites per unit area of TiO2-ZnO thin films. The surface topography, surface roughness parameters, and average grain size for all samples were done by Atomic Force Microscopy (AFM) micrograph which confirm the existence of Nano-structured thin films. The optical energy gap of the TiO2-ZnO thin films was determined by using UV spectroscopy. It was found that one type of basic electrons transitions, through which the values of the optical energy gap for all the prepared thin films which are allowed direct transition.
Źródło:
World Scientific News; 2019, 123; 87-101
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-8 z 8

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