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    Wyświetlanie 1-10 z 10
    Tytuł:
    Synthesis and characterization of some new Schiff bases of 2-oxonaphtho[2,1-b][1,4]oxazine
    Autorzy:
    Chovatiya, P.
    Mehta, C.
    Senjani, H.
    Shah, A.
    Joshi, H. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/411737.pdf
    Data publikacji:
    2014
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    2-Oxonaphtho[2,1-b][1,4]oxazine
    Schiff base
    Opis:
    The literature review reveal that [1,4]-oxazine derivatives represent one of the most active classes of compounds possessing wide spectrum of biodynamic activities and use as potent therapeutic agents. In the present work, a series of Schiff base of 2-(2,3-dihydro-2-oxonaphtho[2,1-b][1,4]oxazin-1-yl)acetohydrazide, 5a-5j has been synthesized using 1-aminonaphthalen-2-ol. Various aromatic aldehyde were react with carbohydrazide 4 in the presence of acid to produce the 2-oxonaphtho[2,1-b][1,4]oxazin Schiff base derivatives with good yields. All synthesized compounds were characterized by IR, NMR and Mass spectrometry analysis.
    Źródło:
    International Letters of Chemistry, Physics and Astronomy; 2014, 12; 26-30
    2299-3843
    Pojawia się w:
    International Letters of Chemistry, Physics and Astronomy
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A rapid, convient and diversified-multicomponent synthesis and characterization of pyrano[2,3-b]indoles
    Autorzy:
    Ghodasara, H. B.
    Singala, P. M.
    Shah, V. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/412134.pdf
    Data publikacji:
    2014
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    1,3-bifunctional synthon
    Pyrano[2,3-b]indoles
    multi component reaction
    non-chromatographic metod
    Opis:
    A series of pyrano[2,3-b]indoles, was efficiently synthesized via one-pot, multi component reaction (MCRs) of 1,3-bifunctional synthon(malononitrile/ethylcyano acetate), aromatic aldehydes and oxiindole in the presence of various basic catalyst. The key advantages of this process are high yields, shorter reaction times, easy work-up, and purification of products by non-chromatographic method.
    Źródło:
    International Letters of Chemistry, Physics and Astronomy; 2014, 7; 69-76
    2299-3843
    Pojawia się w:
    International Letters of Chemistry, Physics and Astronomy
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis and biological activity of 1,2,4-triazolo-[3,4-b]thiadiazole as antimicrobial agents
    Autorzy:
    Vekariya, P. B.
    Pandya, J. R.
    Goswami, V.
    Joshi, H. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/412334.pdf
    Data publikacji:
    2014
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    6-Fluoro chroman
    1,2,4-triazole
    triazolothiadiazole
    antimicrobial activity
    Opis:
    Some novel 6-fluoro chroman derivatives having 1,2,4-triazolo-[3,4-b]thiadiazole were synthesized and characterized by IR, NMR and mass spectral analysis. All synthesized compounds were screened for antimicrobial activity using broth dilution method. All the compounds showed good antimicrobial activity and compound 5e showed significant antibacterial activity.
    Źródło:
    International Letters of Chemistry, Physics and Astronomy; 2014, 7; 45-52
    2299-3843
    Pojawia się w:
    International Letters of Chemistry, Physics and Astronomy
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation and characterization of TiO2 and TiO2P25 nanomaterial and photocatalytic application
    Autorzy:
    Kamalakkannan, J.
    Karthikeyan, B.
    Senthilvelan, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1182809.pdf
    Data publikacji:
    2017
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    HR-SEM
    HR-TEM
    Photocatalytic properties
    Reusable
    Opis:
    TiO2 nanomaterial was prepared by precipitation method and sonication technique. The nanomaterial was characterized by HR-SEM with EDX, TEM, XRD, FT-IR and PL analysis. The photocatalytic activity of TiO2 was much better than that of TiO2–P25 under UV-light irradiation at 365 nm. The photocatalytic activity was evaluated from the photodegradation of malachite green (MAG). The influence of operational parameters such as the effect of catalyst loading dye concentration and chemical oxygen demand measurements had also been investigated. The Photodegradation was found to follow the pseudo-first-order kinetics. Hydroxyl radical formation in the mechanism was confirmed by fluorescence quenching technique. It was proposed that the catalyst is found to be stable and reusable.
    Źródło:
    World Scientific News; 2017, 65; 81-93
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis, spectral and thermal study of (2E, 6E) 2,6-bis(4-hydroxy benzylidene)-4-R-cyclohexanone
    Autorzy:
    Sankhavara, Dharmesh B.
    Chopda, Jalpa V.
    Patel, Jignesh P.
    Parsania, P. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/1070865.pdf
    Data publikacji:
    2019
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    Chalcone
    bisphenol
    heat of melting
    kinetic parameters
    thermal stability
    Opis:
    (2E,6E) 2,6-Bis(4-hydroxybenzalidene)-4-R-cyclohexanone (BHBC, R = H and MBHBC, R = CH3) was synthesized by condensing cyclohexanone/4-methylcyclohexanone with 4-hydroxy benzaldehyde using mixture of boric acid and hydrochloric acid as a catalyst at 60-70 ºC for 1 h. The structures of BHBC and MBHBC are supported by FTIR, 1HNMR, 13CNMR and MS techniques. DSC endothermic transition at 282.48 ºC (BHBC) and two endothermic transitions at 214.66 and 224.83 ºC and assigned as melting transitions. The compositions of the two isomers of MBHBC were determined from their corresponding peak areas and observed compositions are 81.5% and 18.5%, respectively for Isomer-I and Isomer-II. BHBC and MBHBC are thermally stable up to 305 ºC and 285 ºC, respectively and followed three step degradation kinetics. Both the compounds followed apparently first order degradation kinetics and were completely degraded into low molecular mass hydrocarbons.
    Źródło:
    World Scientific News; 2019, 123; 141-160
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Quantitative profile analysis of mulberry silkworm Bombyx mori L. (CSR2XCSR4)
    Autorzy:
    Reddy, B.V.
    Divya, P.
    Anitha, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/11923.pdf
    Data publikacji:
    2015
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    quantitative profile analysis
    mulberry silkworm
    Bombyx mori
    growth parameter
    crossbreed
    Opis:
    Bombyx mori. L. (CSR2XCSR4) is a bivolitne crossbreed that produces high quantity of silk. The weights of worms and glands are directly related to the yield of silk, higher larval weights leads to higher silk production. In the present study, quantitative parameters of 5th instar and pupal stages of silkworm larvae were observed. The analysis of quantitative estimation showed that the maximum weights and lengths of silk gland and silk worm were recorded on 7th day of 5th instar larval stage. The day dependent variation in protein concentration was observed in total silk gland 5th instar larval and pupal stages.
    Źródło:
    International Letters of Natural Sciences; 2015, 07
    2300-9675
    Pojawia się w:
    International Letters of Natural Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation and performance evaluation of jute and glass composites of epoxy resin of (2E,6E)-2,6-bis (4-hydroxy benzylidene)-4-methylcyclohexanone
    Autorzy:
    Chopda, Jalpa V.
    Sankhavara, Dharmesh B.
    Patel, Jignesh P.
    Parsania, P. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/1075481.pdf
    Data publikacji:
    2019
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    Composites
    Diffusivity
    Electric strength
    Flexural strength
    Photosensitive epoxy resin
    Tensile strength
    Volume resistivity
    Water uptake
    Opis:
    Jute and glass composites were prepared by compressing molding technique at 150C for 3h under 20 MPa pressure. J-EMBHBC-DDS, J-EMBHBC-THPA, G-EMBHBC-DDS and G-EMBHBC-THPA showed 15, 15.1, 58.3 and 18.7 MPa tensile strength, respectively. J-EMBHBC-DDS and J-EMBHBC-THPA showed 22.9 and 19.4 MPa flexural strength, respectively. J-EMBHBC-DDM and G-EMBHBC-DDM showed 1.6×109 and 1.2×1012 ohm cm volume resistivity, respectively. J-EMBHBC-DDM and G-EMBHBC-DDM showed 2.8 and 11.2 kVmm-1, respectively. Water uptake in the composites was carried out in pure water and 10% each of aqueous HCl, H2SO4, HNO3, NaOH, KOH and NaCl solutions at 35 C as well as in boiling water. Composites showed high water uptake tendency and longer equilibrium time in different environments. High water uptake in the composites is due to presence of hydroxyl groups in celluloses and resins and also due to formation of micro cracks. Nature of the electrolytes also played an important role on water uptake behavior and diffusivity in the composites. Drastic reduction in equilibrium water uptake time was observed in boiling water.
    Źródło:
    World Scientific News; 2019, 129; 23-39
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis, Characterization and Biological evaluation of 6-substituted-2-(substituted-phenyl)-quinoline derivatives bearing 4-amino-1,2,4-triazole-3-thiol ring at C-4 position
    Autorzy:
    Vaghasiya, R. G.
    Ghodasara, H. B.
    Vachharajani, P. R.
    Shah, V. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/412211.pdf
    Data publikacji:
    2014
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    Quinoline, 4-amino-1,2,4-triazole-3-thiol
    therapeutic agents
    antimicrobial assai
    Opis:
    Quinoline derivatives represent one of the most active classes of compounds possesses wide spectrum biodynamic activities and use as potent therapeutic agents. In this research work, a synthesis, characterization and biological evaluation of 6-substituted-2-(substituted-phenyl)-quinoline derivatives bearing 4-amino-1,2,4-triazole-3-thiol ring at C-4 position is described. The synthesis of quinoline derivatives is carried out by the reaction of substituted quinoline-4-carbohydrazides with a mixture of carbon disulphide and potassium hydroxide which further react with hydrazine hydrate to give final compounds. All of these compounds were screened for their in vitro antimicrobial assay against gram (+ve), gram (-ve) bacteria and fungi activity compared with standard drugs viz., Ampicilin, Chloramphenicol, Ciprofloxacin, Norfloxacin, Griseofulvin and Nystatin at different concentrations.
    Źródło:
    International Letters of Chemistry, Physics and Astronomy; 2014, 8; 30-37
    2299-3843
    Pojawia się w:
    International Letters of Chemistry, Physics and Astronomy
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of temperature and solvents on ultrasonic speed and thermo-acoustic parameters of epoxy resin of (2E, 6E)-bis (4-hydroxy benzylidene)-4-methylcyclohexanone solutions at four different temperatures
    Autorzy:
    Chopda, Jalpa V.
    Sankhavara, Dharmesh B.
    Patel, Jignesh P.
    Parsania, P. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/1066232.pdf
    Data publikacji:
    2019
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    Density
    Epoxy resin
    Solvation number
    Thermo-acoustic parameters
    Ultrasonic speed
    Viscosity
    Opis:
    The density (), viscosity () and ultrasonic speed (U) of 1, 4-dioxane (DO), tetrahydrofuran (THF), chloroform (CF) and solutions (0.25-5 wt%) of epoxy resin of (2E, 6E)-bis(4-hydroxy benzylidene)-4-methylcyclohexanone have been investigated at 298, 303, 308 and 313 K to understand molecular interactions in solutions of different polarity. Various acoustical and thermodynamic activation parameters such as acoustical impedance (Z), adiabatic compressibility (a), internal pressure (), free volume (Vf), intermolecular free path length (Lf), van der Waals constant(b), viscous relaxation time (), classical absorption coefficient (f2)cl, Rao`s molar sound function (Rm) and solvation number (Sn) were determined using, and U data and correlated with concentration (C) at four different temperatures (T). Good to excellent correlation between a given parameter and concentration is observed at all T. Linear or non-linear increase or decrease of studied acoustical and thermodynamic parameters with concentration of epoxy resin at different temperatures indicated existence of strong molecular interactions (solvent-solute and solute-solute) in the solutions. The non-linear increase of Sn with concentration of epoxy resin further supported the existence of strong molecular interactions and structure forming tendency of EMBHBC. The competing solvent-solute and solute-solute interactions are also supported by thermodynamic activation parameters (G, H and S).
    Źródło:
    World Scientific News; 2019, 131; 222-241
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Novel synthesis of 3-(((E)-benzylidene)amino)-5-((Z)-3,4-dimethoxybenzylidene)-2-phenyl-3,5-dihydro-4H-imidazol-4-one derivatives as potent antimicrobial agents
    Autorzy:
    Manawar, Rohit B.
    Parmar, Mukesh B.
    Nayaka, Indresh J.
    Pandit, Brinda H.
    Shah, Manish K.
    Powiązania:
    https://bibliotekanauki.pl/articles/1066261.pdf
    Data publikacji:
    2019
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    4H-imidazol-4-one
    A. niger
    Anti-fungal
    Anti-microbial Agent
    Bioactivity
    C. albicans
    E. coli
    Elemental analysis
    IR spectroscopy
    Mass spectroscopy
    NMR spectroscopy
    P. aeruginosa
    S. aureus
    S. pyogenes
    Opis:
    Novel synthesis of 4H-imidazol-4-one derivative by reaction of (Z)-3-amino-5-(3,4 dimethoxybenzylidene)-2-phenyl-3,5-dihydro-4H-imidazol-4-one with derivative of different aromatic aldehydes and Salicyldehyde. New synthesized compound are thermally stable and neither air-nor moisture sensitive at RT. Successive library of synthesized compound characterized using IR, NMR, Elemental, Mass, and its antimicrobial activity study.
    Źródło:
    World Scientific News; 2019, 130; 42-70
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-10 z 10

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