- Tytuł:
- Investigation of Electrocatalytic Properties of Pt/Mo - Expanded Graphite Composite Derived from Graphite Intercalation Compound
- Autorzy:
-
Urbaniak, J.
Skowroński, J. - Powiązania:
- https://bibliotekanauki.pl/articles/1535895.pdf
- Data publikacji:
- 2010-09
- Wydawca:
- Polska Akademia Nauk. Instytut Fizyki PAN
- Tematy:
-
82.47.Gh
82.80.Fk - Opis:
- In the present work, electrocatalytic properties of Pt-EG and Pt/Mo-EG composite electrodes are studied. These composites were prepared by a three-step synthesis. First, stage-1 $HClO_4$-GIC was synthesized using the chronopotentiometric method. Then, $HClO_4$-GIC was heat treated to obtain expanded graphite. Finally, expanded graphite was coated with platinum catalyst from a water-alcohol solution of $H_2PtCl_6$. $MoCl_5$-GIC synthesized in parallel was subjected to thermal exfoliation to get Mo-EG composite onto which platinum catalyst was dispersed. The X-ray diffraction and energy dispersive X-ray analyses coupled with scanning electron microscopy were applied for characterizing the obtained GICs and EG-based composites, whereas cyclic voltammetry was used to study electrocatalytic properties of Pt/EG and Pt/Mo-EG composite electrodes in sulfuric acid and sulfuric acid admixed with methanol.
- Źródło:
-
Acta Physica Polonica A; 2010, 118, 3; 442-446
0587-4246
1898-794X - Pojawia się w:
- Acta Physica Polonica A
- Dostawca treści:
- Biblioteka Nauki