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Wyszukujesz frazę "Crystallite size" wg kryterium: Wszystkie pola


Wyświetlanie 1-3 z 3
Tytuł:
Carbon Monolith Surface Chemistry Influence on the Silver Deposit Amount and Crystallite Size
Autorzy:
Vukčević, M.
Kalijadis, A.
Jovanović, Z.
Laušević, Z.
Laušević, M.
Powiązania:
https://bibliotekanauki.pl/articles/1503488.pdf
Data publikacji:
2011-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.U-
81.65.-b
68.35.Dv
81.15.-z
Opis:
The surface of carbon monolith (CM) was chemically treated in order to obtain antibacterial filters with silver deposit for water treatment. The chemical treatment involved submerging the as-received CM in $HNO_{3},$ $KOH$ and $H_{2}O_{2}$ solution. The specific surface area was examined by $N_{2}$ adsorption. Silver deposition at the surface of CM samples was performed using cheap and simple procedure of immersing CM samples in aqueous solution of $AgNO_{3}$. Temperature programmed desorption method has been used in order to investigate the nature and thermal stability of surface oxygen groups before and after silver deposition. The composition and crystalinity of silver deposits have been examined by X-ray diffraction. Chemical treatment does not cause any drastic changes of CM specific surface area, but increases a total amount of surface oxides. Amount of deposited silver is several times higher for all chemically treated samples. The results show that increasing the amount of CO yielding groups on CM surface leads to increased amount of Ag deposit and decreases its crystallite sizes
Źródło:
Acta Physica Polonica A; 2011, 120, 2; 284-288
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of crystallite size changes in an oxide layer formed on steel used in the power industry
Autorzy:
Gwoździk, M.
Powiązania:
https://bibliotekanauki.pl/articles/1075650.pdf
Data publikacji:
2016-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Bx
81.16.Pr
81.65.Mq
Opis:
The paper presents results of studies on the crystallite sizes of oxide layer formed during a long-term operation on steel at an elevated temperature. This value was determined by a method based on analysis of the diffraction line profile, according to a Scherrer formula. The oxide layer was studied on a surface and a cross-section at the inner site on the pipe inlet, at the fire and counter-fire wall of the tube. X-ray studies were carried out on the inner surface of a tube (in a flowing medium environment), then the layer's surface was polished and the diffraction measurements repeated to reveal differences in the originated oxides layer. X-ray phase analysis was performed by the use of a SEIFERT 3003 T/T X-ray diffractometer, with a cobalt source of λ_{Co}=0.17902 nm wavelength. X-ray diffraction measurements were performed in the 20÷120° range of angles with an angular step of 0.1°. To interpret the results the diffractograms were described by a pseudo Voigt curve using the Analyze software. A computer software and the DHN PDS, PDF4+2009 crystallographic database were used for the phase identification. The results showed that the crystallite sizes have an effect on the properties of the oxide. It has been shown that the outer oxide layer having larger crystallites, is more porous and thus more brittle.
Źródło:
Acta Physica Polonica A; 2016, 130, 4; 935-938
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Estimate of the Crystallite Size for Nanocrystalline AISI 316L Stainless Steel and Armco Iron Processed by Hydrostatic Extrusion Using Variable Energy Positron Beam
Autorzy:
Sarnek, M.
Dryzek, E.
Horodek, P.
Pachla, W.
Powiązania:
https://bibliotekanauki.pl/articles/1033950.pdf
Data publikacji:
2017-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
stainless steel
Armco iron
plastic deformation
hydrostatic extrusion
variable energy positron beam
X-ray diffraction
Opis:
The paper presents the results of research of nanocrystalline AISI 316L type stainless steel and nanocrystalline Armco pure iron processed by severe plastic deformation using hydrostatic extrusion method. Surface and subsurface of the steel samples extruded at different pressure were investigated using variable energy positron beam. It enabled us to determine the positron diffusion length and compare its values with those for annealed AISI 304 stainless steel. Furthermore positron lifetime and microhardness were measured for all the samples and X-ray diffraction was used to estimate the crystallite size.
Źródło:
Acta Physica Polonica A; 2017, 132, 5; 1598-1601
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-3 z 3

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