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Tytuł:
Deformation Mechanisms and Fracture of Ni-Based Metallic Glasses
Autorzy:
Lesz, S.
Griner, S.
Nowosielski, R.
Powiązania:
https://bibliotekanauki.pl/articles/353790.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metals
transmission electron microscopy
scanning electron microscopy
fracture
shear bands
Opis:
The cracking of materials and fracture surface is of great practical and academic importance. Over the last few years the development of the fractography of crystalline alloys resulted in a useful tool for the prediction or failure analysis. Many attempts have been made to observe cracks using optical microscopy, X-ray topography and transmission electron microscopy (TEM). Of these techniques, the resolution of optical microscopy and X-ray topography is too poor. By contrast, the resolution of TEM is high enough for detailed information to be obtained. However, in order to apply TEM observations, a thin foil specimen must be prepared, and it is usually extremely difficult to prepare such a specimen from a pre-selected region containing a crack. In the present work, deformation mechanisms fracture surfaces of Ni-based metallic glass samples have been studied by specially designed experiments. In order to study the deformation mechanisms and fracture the Ni-based metallic glasses have been investigated in the tensile test. The structure and fracture surfaces after the decohesion process in tensile tests were observed using transmission electron microscope (TEM) and scanning electron microscope (SEM), respectively. The studies of structure were performed on thin foils. Moreover the investigated tape was subjected to a banding test. Then, the tape was straightened and the thin foil from the area of maximum strain was prepared. This thin foil sample was deformed before the TEM investigation to obtain local tears.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 791-796
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Milling Time on Amorphization of Mg-Zn-Ca Powders Synthesized by Mechanical Alloying Technique
Autorzy:
Lesz, S.
Kremzer, M.
Gołombek, K.
Nowosielski, R.
Powiązania:
https://bibliotekanauki.pl/articles/354717.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Mg-based powders
transmission electron microscopy
scanning electron microscopy
mechanical alloying
Opis:
Mg60 Zn35 Ca5 amorphous powder alloys were synthesized by mechanical alloying (MA) technique. The results of the influence of high-energy ball-milling time on amorphization of the Mg60 Zn35 Ca5 elemental blend (intended for biomedical application) were presented in the study. The amorphization process was investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM). Initial elemental powders were mechanically alloyed in a Spex 8000 high-energy ball mill at different milling times (from 3 to 24 h). Observation of the powder morphology after various stages of milling leads to the conclusion that with the increase of the milling time the size of the powder particles as well as the degree of aggregation change. The partially amorphous powders were obtained in the Mg60 Zn35 Ca5 alloy after milling for 13-18h. The results indicate that this technique is a powerful process for preparing Mg60 Zn35 Ca5 alloys with amorphous and nanocrystalline structure.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 845-851
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of the Quenching Rate on the Structure and Magnetic Properties of the Fe-Based Amorphous Alloy
Autorzy:
Nabiałek, M.
Powiązania:
https://bibliotekanauki.pl/articles/350944.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
transmissions electron microscopy
scanning electron microscopy
amorphous matrials
free volumes
quasidislocation
Opis:
This paper presents the results of investigations into the structure, microstructure and magnetic properties of Fe61Co10Y8W1B20 amorphous alloy. The alloy samples were in two physical forms: (1) plates of approximate thickness 0.5 mm (so-called bulk amorphous alloys) and (2) a ribbon of approximate thickness 35 μm (so-called classic amorphous alloy). The investigations comprised: X-ray diffractometry, Mössbauer spectrometry, transmission electron microscopy, and selected magnetic measurements; all of the investigations were carried out on samples in the as-quenched state. Analysis of the obtained SEM and TEM images, X-ray diffraction patterns, Mössbauer spectrometry results and measurements of the magnetisation in a high magnetic field facilitated collectively the detailed description of the structure of the investigated alloy, which was found to depend on the quenching speed.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 439-444
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Aging and Degradation of Human Fingernail Plates Upon Cosmetic Agents
Autorzy:
Kulesza, S.
Bramowicz, M.
Gwoździk, M.
Wilczyński, S.
Goździejewska, A. M.
Powiązania:
https://bibliotekanauki.pl/articles/354662.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Atomic Force Microscopy
Scanning Electron Microscopy
fractal characterization
nanoscale property mapping
Opis:
The knowledge whether and how chemical species react with tissues is important because of protection against harmful factors, diagnose of dermatological diseases, validation of dermatological procedures as well as effectiveness of topical therapies. In presented work the effects of chemical agents on plates of human fingernails were studied using Atomic Force Microscopy and Scanning Electron Microscopy. Apart from that, mapping of the elastic properties of the nails was also carried out. To obtain reliable measures of spatial evolution of the surface variations, recorded images were analyzed in terms of scaling invariance brought by fractal geometry, instead of common though not unique statistical measures.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 1; 181-184
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanical properties of Ni-Fe-Cu-P-B alloy produced by two component melt spinning (TCMS)
Autorzy:
Wojciechowska, M.
Ziewiec, K.
Kąc, S.
Prusik, K.
Powiązania:
https://bibliotekanauki.pl/articles/351728.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metallic glasses
scanning electron microscopy (SEM)
nanoindentation
transmission electron microscopy TEM
mechanical properties
Opis:
The aim of this work was to investigate the microstructure and mechanical properties of the two-component melt-spun (TCMS) alloy produced from Ni40Fe40B20 and Ni70Cu10P20 melts. The Ni40Fe40B20, Ni70Cu10P20, Ni55 Fe20 Cu5 P10 B10 alloys were arc-melted. Then the alloys were melt-spun in the two different ways i.e.: by casting from a single-chamber crucible and from the two-chamber crucible. All of the above mentioned alloys were processed in the first way and the Ni40Fe40B20 and Ni70Cu10P20 were simultaneously cast on the copper roller from the two-chamber crucible. The microstructure of the alloy was studied using transmission electron microscopy (TEM), scanning electron microscopy (SEM) with energy dispersive spectrometry (EDS) and light microscopy. The mechanical properties were investigated using tensile testing and nanoindentation. The two-component melt-spun (TCMS) amorphous Ni55 Fe20 Cu5 P10 B10 alloy present hardness, tensile strength and Young modulus on the significantly higher level than for a single phase amorphous Ni55 Fe20 Cu5 P10 B10 alloy and slightly below the corresponding values for the Ni40Fe40B20.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 137-140
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of the Powder Consolidation Method Type on the Microstructure and Selected Properties of Al2O3-Cu-Ni Composite
Autorzy:
Zygmuntowicz, J.
Wachowski, M.
Piotrkiewicz, P.
Kaszuwara, W.
Powiązania:
https://bibliotekanauki.pl/articles/351724.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
composites
Pulse Plasma Sintering
Uniaxial Powder Pressing
Scanning Electron Microscopy
Opis:
The present research is focused on the characterization of the composites from Al2O3-Cu-Ni system. Two methods of ceramic-metal composite forming were applied: uniaxial powder pressing and Pulse Plasma Sintering (PPS). To obtain the samples the powder mixtures containing 85 vol.% of Al2O3 and 15 vol.% of metal powders were used. Influence of the sintering process on microstructure and mechanical properties of the two series of the composites was analyzed in detail. The selected physical properties of samples were characterized by Archimedes immersion method. Vickers hardness and the fracture toughness of the composites was determined as well. The microstructure of the composites was characterized by XRD, SEM, EDX. Fractography investigation was carried out as well. Independently on composite production method Al2O3, Cu, Ni, and CuNi phases were revealed. Fractography investigation results revealed different character of fracture in dependence of fabrication method. Pulse Plasma Sintered samples were characterized by higher crack resistance and higher Vickers hardness in comparison to the specimens manufactured by uniaxial pressing.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 967-974
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Quartz grain features in modern glacial and proglacial environments: A microscopicstudy from the Russell Glacier, southwest Greenland
Autorzy:
Kalińska-Nartiša, Edyta
Lamsters, Kristaps
Karušs, Jānis
Krievāns, Māris
Rečs, Agnis
Meija, Raimonds
Powiązania:
https://bibliotekanauki.pl/articles/2042159.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Arctic
Greenland
modern glacial environment
Quartz grains
Scanning electron microscopy
Źródło:
Polish Polar Research; 2017, 38, 3; 265-289
0138-0338
2081-8262
Pojawia się w:
Polish Polar Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study of Nonmetallic Inclusions in Aluminum–Silicon Alloys
Autorzy:
Galek, Tomasz
Łączek, Andrzej
Łysiak, Karol
Powiązania:
https://bibliotekanauki.pl/articles/176066.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminum–silicon alloy
nonmetallic inclusions
scanning electron microscopy
X-ray tomography
Opis:
In this article, a study of nonmetallic inclusions introduced during the casting process of the aluminum–silicon alloy is presented. The samples were investigated using a scanning electron microscope to find the chemical composition and X-ray tomography to check the volumetric content of the non-metallic inclusions. The samples were made from AlSi7Mg alloy, used for car wheels, with 7% weight content of Si, 89% of Al, and 0.3% of Mg. The main goal of our investigations was to find out the chemical composition of the impurities and to identify the stage of the casting process at which the impurities are introduced.
Źródło:
Advances in Manufacturing Science and Technology; 2020, 44, 1; 28-31
0137-4478
Pojawia się w:
Advances in Manufacturing Science and Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cooling Characteristic and Microstructure of Ni-Si-B-Ag Alloy
Autorzy:
Wojciechowska, M.
Ziewiec, K.
Mucha, D.
Powiązania:
https://bibliotekanauki.pl/articles/356071.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
amorphous/crystalline composite
scanning electron microscopy
X-ray diffraction
thermography
melt spinning
Opis:
The aim of this work was to investigate the possibility of obtaining an amorphous/crystalline composite starting from Ni-SiB-based powder grade 1559-40 and silver powder. The alloy was produced using arc melting of 95% wt. Ni-Si-B-based powder (1559-40) and 5% wt. Ag powder. Ingot was re-melted on a copper plate and observed while cooling using a mid-wave infra-red camera. The alloy was then melt-spun in a helium atmosphere. The microstructure of the ingot as well as the melt-spun ribbon was studied using light microscopy and scanning electron microscopy with energy dispersive spectrometry. Phase identification was performed by means of X-ray diffraction. The observations confirmed an amorphous/crystalline microstructure of the ribbon where the predominant constituent of the microstructure was an amorphous phase enriched with Ni, Si, and B, while the minor constituent was an Ag-rich crystalline phase distributed in a film along the melt-spinning direction.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1357-1360
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Transition in SrZnO Laser Pulse Deposited Alloy
Autorzy:
Albrithen, H. A.
Elnaggar, M.
Ozga, K.
Szota, M.
Alahmed, Z. A.
Alanazi, A. Q.
Alshahrani, H.
Alfaifi, E.
Djouadi, M. A.
Labis, J. P.
Powiązania:
https://bibliotekanauki.pl/articles/355190.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
oxide materials
solid state alloys
structural phase transition
X-ray diffraction
scanning electron microscopy
Opis:
We have discovered a structural transition for the SrZnO alloy films from a wurtzite to a rock-salt structure, leading to a reduction in the (112̲0)/(0001) surface energy ratio. The films were grown by pulsed laser deposition using different SrO ratios, x. We have revealed that growth at a higher temperature, 750°C, resulted in a sharp 0002 peak at a low SrO content (5%), whereas growth at a higher SrO content (10%) resulted in a non-crystalline film with minute crystallites with a (112̲0) orientation. Generally the crystallinity decreased as the SrO content increased. No results obtained for the crystalline films showed any orientation of significant peaks besides the peak attributed to the (0001) plane, suggesting epitaxial growth. Optical measurements showed difference in transmission widows of alloys with different SrO percentage, and this was correlated to SrO influence on growth mode as indicated by scanning electron imaging. The studied SrZnO films, with SrO/(SrO + ZnO) ≤ 0.25, were grown by pulsed laser deposition using different SrO ratios, x. The effects of temperature and oxygen pressure during growth on the films’ structural properties were investigated. XRD results indicate that the film crystallinity was improved as the temperature and O2 pressure increased up to 650°C and 0.5 Torr, respectively.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 211-216
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cast iron component failure: A metallurgical investigation
Autorzy:
Sudhakar, K. V.
Powiązania:
https://bibliotekanauki.pl/articles/382757.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
cast iron
hardness test
optical microscopy
scanning electron microscopy
fractography
żeliwo
testy twardości
mikroskopia optyczna
mikroskop skaningowy
Opis:
A fractured nutcracker was examined for determining the root cause/s for premature fracture/failure. This is one of the common tools used typically for cracking hard nuts. In this study, metallurgical failure analysis techniques namely, visual inspection, optical microscopy, SEM, and hardness tests were used in investigating the broken product. From the metallurgical analysis, it was determined that the combined effect of low carbon equivalent and presence of inclusions contributed to the sudden fracture of the nut cracking tool.
Źródło:
Archives of Foundry Engineering; 2012, 12, 2s; 67-70
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of structural relaxations within the amorphous structure on the magnetic properties of amorphous tapes from FeCoB family
Autorzy:
Szota, M.
Powiązania:
https://bibliotekanauki.pl/articles/354999.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
amorphous materials
free volumes
quasidislocation dipoles
scanning electron microscopy
approach to ferromagnetic saturation
magnetic moments
Opis:
The paper presents the research results for the Fe78Co2Si9B11 amorphous alloy, and after the process of annealing resulting only in the relaxation of the material. The structure relaxations occurring in the volume of test samples lead to the changes in their magnetic and mechanic properties. Therefore the studies on the effect of the structure defects on the properties of these type of materials are important. Understanding the processes occurring during the magnetizing of amorphous alloys can be helpful in the design of modern functional materials for special purposes. The main purpose of this elaboration was to determine the effect of the amorphous structure defects in the state after solidification and after heat treatment on the changes in the magnetizing process and in such parameters as the saturation magnetization and the coercivity field.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 217-222
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of some compounds on development of Sphaerotheca pannosa var. rosae
Autorzy:
Wojdyla, A T
Powiązania:
https://bibliotekanauki.pl/articles/66257.pdf
Data publikacji:
2000
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
plant disease
Sphaerotheca pannosa var.rosae
control
biopreparation
rose
development
scanning electron microscopy
oil
compound
Opis:
Influence of triforine (standard), garlic juice, Antifung 20 SL (20% vermicompost), Atpolan 80 EC (76% mineral oil), Biosept (grapefruit juice) and Atonik AL on development of Sphaerotheca pannosa var. rosae was evaluated. Garlic juice, Atpolan 80 EC and Biosept applied as rose spray gave similar effect in the control S. pannosa var. rosae as triforine. Observations under scanning electron microscop indicated that 24 hrs after rose spraying all tested compounds cause almost complete collapse of conidia and hyphe.
W przeprowadzonych badaniach polowych oraz w uprawie róż pod osłonami oceniano aktywność biologiczną biopreparatów (Antifung 20 SL), Biosept, sok z czosnku, oleju (Atpolan 80 EC) i stymulatora wzrostu roślin (Atonik AL) do zwalczania S. pannosa var. rosae. Krzewy róż opryskiwano co 7 lub 14 dni. W drugiej części badań przy użyciu mikroskopu skaningowego oceniano wpływ badanych związków na grzyba. W tym celu krzewy róż uprawiane pod osłonami opryskano jeden raz, a po 24 godzinach pobrano liście do obserwacji. Badane preparaty wykazywały wysoką skuteczność w zwalczaniu S. pannosa var. rosae. Niektóre z nich dorównywały (sok z czosnku) bądź nieznacznie ustępowały (Antifung 20 SL, Atpolan 80 EC, Biosept) skutecznością fungicydowi standardowemu Saprol 190 EC. Zdecydowanie niższą skuteczność wykazywał Atonik AL. Z kolei wzrost stężenia preparatów Biosept oraz soku z czosnku wiązał się ze wzrostem ich skuteczności. Natomiast Antifung 20 SL stosowany co 14 dni wykazywał niższą skuteczność aniżeli przy aplikowaniu co 7 dni. Już po 24 godzinach od wykonania opryskiwania w obserwacji przeprowadzonej przy użyciu mikroskopu skaningowego stwierdzono, że badane związki powodowały prawie całkowite spłaszczenie i deformację grzybni, trzonków oraz zarodników konidialnych. Jednak w przypadku preparatu Atonik AL tylko fragmenty grzybni były całkowicie zniszczone. Z kolei po zastosowaniu oleju Atpolan 80 EC stwierdzono rozpad fragmentów grzyba, a następnie ich łączenie się w płatowate, strzępiaste - dosyć duże struktury.
Źródło:
Journal of Plant Protection Research; 2000, 40, 2
1427-4345
Pojawia się w:
Journal of Plant Protection Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Mechanical Characteristics of the Ternary SnZnAl Lead-Free Alloy
Autorzy:
Pietrzak, K.
Klasik, A.
Maj, M.
Sobczak, N.
Powiązania:
https://bibliotekanauki.pl/articles/380398.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lead free alloy
microstructure
mechanical properties
scanning electron microscopy
stop bezołowiowy
mikrostruktura
właściwości mechaniczne
mikroskop skaningowy
Opis:
The paper describes the studies of ternary SnZn9Al1.5 lead-free alloy from the viewpoint of its mechanical behavior as well as microstructure examined by the light and scanning electron microscopy. The authors focused their attention specifically on the fatigue parameters determined by the original modified low-cycle fatigue method (MLCF), which in a quick and economically justified way allows determination of a number of mechanical parameters based on the measurement data coming from one test sample only. The effect of the addition of 1.5% Al to the binary eutectic SnZn9 alloy on its microstructure and the obtained level of mechanical parameters was analyzed. The phases and intermetallic compounds occurring in the alloy were identified based on the chemical analysis carried out in micro-areas by the SEM/EDS technique. It was shown that the addition of 1.5% Al to the binary eutectic SnZn9 alloy resulted in a more favorable microstructure and consequently had a positive effect on the mechanical parameters of the alloy. Based on the conducted research, it was recommended to use a combinatorial method based on the phase quanta theory to quickly evaluate the microstructure and the original MLCF method to determine a number of mechanical parameters.
Źródło:
Archives of Foundry Engineering; 2018, 18, 3; 31-36
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Crystallization of FeSiB Amorphous Ribbons Induced by Laser Interference Irradiation
Autorzy:
Kusinski, J.
Czyż, O.
Radziszewska, A.
Morgiel, J.
Ostrowski, R.
Strzelec, M.
Czyż, K.
Rycyk, A.
Powiązania:
https://bibliotekanauki.pl/articles/379811.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
laser interference heating
FeSiB alloy
amorphous alloy
scanning electron microscopy
transmission electron microscopy
stop FeSiB
stop amorficzny
skaningowa mikroskopia elektronowa
transmisyjna mikroskopia elektronowa
Opis:
Detailed studies on the effects of pulsed laser interference heating on surface characteristics and subsurface microstructure of amorphous Fe80Si11B9 alloy are reported. Laser interference heating, with relatively low pulsed laser energy (90 and 120 mJ), but with a variable number (from 50-500) of consecutive laser pulses permitted to get energy accumulation in heated areas. Such treatment allowed to form two- Dimensional micro-islands of laser-affected material periodically distributed in amorphous matrix. The crystallization process of amorphous FeSiB ribbons was studied by means of scanning and transmission electron microscopy. Detailed microstructural examination showed that the use of laser beam, resulted in development of nanostructure in the heated areas of the amorphous ribbon. The generation of nanocrystalline seed islands created by pulsed laser interference was observed. This key result may evidently give new knowledge concerning the differences in microstructure formed during the conventional and lased induced crystallization the amorphous alloys. Further experiments are needed to clarify the effect of pulsed laser interference crystallization on magnetic properties of these alloys.
Źródło:
Archives of Foundry Engineering; 2018, 18, 2; 27-30
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł

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