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Wyświetlanie 1-15 z 223
Tytuł:
Application of laser and electrochemical interaction in sequential and hybrid micromachining processes
Autorzy:
Skoczypiec, S.
Powiązania:
https://bibliotekanauki.pl/articles/201232.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
laser beam
electrochemical machining
hybrid machining processes
promień lasera
obróbka elektrochemiczna
obróbka hybrydowa
Opis:
One of the research and development trends in nowadays manufacturing technology is integration of different manufacturing techniques into single machine tool. In the first part of the paper possibilities, goals, reasons and advantages of thermal and electrochemical interaction have been characterized. As literature review indicates such a connection can be realized as sequential or hybrid machining. The second part of the paper focuses on detailed analysis of laser assisted electrochemical process. For this purpose, the mathematical model of workpiece heating has been developed. Based on obtained results and literature review possibilities of technical realization and potential application have been discussed.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2015, 63, 1; 305-314
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preliminary evaluation of the applicability of F, V and AEsignals in diagnosis of ADI machining process
Autorzy:
Myszka, D.
Bombiński, S.
Powiązania:
https://bibliotekanauki.pl/articles/381921.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
austempered ductile iron
machining
diagnosis
ADI machining process
żeliwo sferoidalne
obróbka
diagnostyka
obróbka ADI
Opis:
In this study, a preliminary evaluation was made of the applicability of the signals of the cutting forces, vibration and acoustic emission in diagnosis of the hardness and microstructure of ausferritic ductile iron and tool edge wear rate during its machining. Tests were performed on pearlitic-ferritic ductile iron and on three types of ausferritic ductile iron obtained by austempering at 400, 370 and 320°C for 180 minutes. Signals of the cutting forces (F), vibration (V) and acoustic emission (AE) were registered while milling each type of the cast iron with a milling cutter at different degrees of wear. Based on individual signals from all the sensors, numerous measures were determined such as e.g. the average or maximum signal value. It was found that different measures from all the sensors tested depended on the microstructure and hardness of the examined material, and on the tool condition. Knowing hardness of the material and the cutting tool edge condition, it is possible to determine the structure of the material .Simultaneous diagnosis of microstructure, hardness, and the tool condition is probably feasible, but it would require the application of a diagnostic strategy based on the integration of numerous measures, e.g. using neural networks.
Źródło:
Archives of Foundry Engineering; 2014, 14, 1; 91-96
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of heating rate on sorbitic transformation temperature of tempering C45 steel
Autorzy:
Kulawik, A.
Winczek, J.
Powiązania:
https://bibliotekanauki.pl/articles/383135.pdf
Data publikacji:
2011
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
heat treatment
laser treatment
tempering
phase transformation
obróbka cieplna
obróbka laserowa
odpuszczanie stali
przemiana fazowa
Opis:
In this paper the analysis of speed heating influence on sorbitic transormation temperature of tempering C45 steel is presented. On the basis of dilatometric research, functions associating heating time with initial and final temperature of sorbitic transformation have been determined as well as the size structural (γ) and thermal (α) expansion coefficients of quenching and tempering structures have been estimated.
Źródło:
Archives of Foundry Engineering; 2011, 11, 2 spec.; 131-134
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Visual Testing of Castings Defects after Vibratory Machining
Autorzy:
Bańkowski, D.
Młynarczyk, P.
Powiązania:
https://bibliotekanauki.pl/articles/1840920.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
non-destructive testing
visual testing
vibratory machining
surface treatment
castings
badania nieniszczące
testy wizualne
obróbka wibracyjna
obróbka powierzchniowa
odlewy
Opis:
The paper presents an example of the application of vibratory machining for castings based on the results of visual testing. The purpose of the work is to popularize non-destructive testing and vibratory machining as finishing process, especially in the case of cast objects. Visual testing is one of the obligatory non-destructive tests used for castings and welded joints. The basic requirements concerning the dimensional accuracy and surface texture of cast components are not met if visible surface flaws are detected. The tested castings, which had characteristic traces of the casting process, were subjected to vibratory machining. The machining with loose abrasive media in vibrating containers is aimed at smoothing the surface and reducing or completely removing flashes. To complement the visual testing were also conducted research on the contact profilometer Taylor Hobson PGI 1200. Particular attention was focused on measuring the height of flashes and changes in the surface of smoothed details based on BNIF No. 359 touch-visual patterns. Based on the work, it can be concluded that vibratory machining allows for removal flashes and smoothing of the surface of aluminum alloy cast objects.
Źródło:
Archives of Foundry Engineering; 2020, 20, 4; 72-76
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Research on the Influence of Vibratory Machining on Titanium Alloys Properties
Autorzy:
Bańkowski, D.
Spadło, S.
Powiązania:
https://bibliotekanauki.pl/articles/947596.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium alloy
vibratory machining
finishing treatment
surface roughness
micro-hardness
stop tytanu
obróbka wibracyjna
obróbka wykańczająca
chropowatość powierzchni
mikrotwardość
Opis:
This article proposes these of vibratory machining to Ti-6Al-4V titanium alloy as finishing treatment. Titanium alloy was used in the aerospace industry, military, metallurgical, automotive and medical processes, extreme sports and other. The three-level three-factor Box-Behnken experiment examined the influence of machining time of vibratory machining, the type of mass finishing media used and the initial state of the surface layer on the mass loss, geometric structure of the surface, micro hardness and the optimal process parameters were determined. Considerations were given the surfaces after milling, after cutting with a band saw and after the sanding process. The experiment used three types of mass finishing media: polyester, porcelain and metal. Duration of vibratory machining treatment was assumed to be 20, 40, 60 minutes. The form profiles before and after vibratory machining were determined with the Talysurf CCI Lite - Taylor Hobson optical profiler. Future tests should concern research to carry out tests using abrasive pastes with a larger granulation of abrasive grains, to carry out tests for longer processing times and to determine the time after which the parameters of geometrical structure of the surface change is unnoticeable.
Źródło:
Archives of Foundry Engineering; 2020, 20, 3; 47-52
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
New possibilities of shaping the surface properties in austempered ductile iron castings
Autorzy:
Myszka, D.
Powiązania:
https://bibliotekanauki.pl/articles/379832.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
austempered ductile iron
surface treatments
surface properties
casting
heat treatment
żeliwo sferoidalne austenityczne
obróbka powierzchni
właściwości powierzchniowe
odlew
obróbka cieplna
Opis:
The paper presents recent developments concerning the formation of surface layer in austempered ductile iron castings. It was found that the traditional methods used to change the properties of the surface layer, i.e. the effect of protective atmosphere during austenitising or shot peening, are not fully satisfactory to meet the demands of commercial applications. Therefore, new ways to shape the surface layer and the surface properties of austempered ductile iron castings are searched for, to mention only detonation spraying, carbonitriding, CVD methods, etc.
Źródło:
Archives of Foundry Engineering; 2013, 13, 1; 103-106
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Influence of Abrasive Paste on the Effects of Vibratory Machining of Brass
Autorzy:
Bańkowski, D.
Spadło, S.
Powiązania:
https://bibliotekanauki.pl/articles/382264.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
surface treatment
product development
vibratory machining
surface roughness
brass
finishing
obróbka powierzchniowa
rozwój produktu
obróbka wibracyjna
chropowatość powierzchni
wykończenie
mosiądz
Opis:
The article presents the results of research on the finishing of M63 Z4 brass by vibratory machining. Brass alloy was used for the research due to the common use of ammunition elements, cartridge case and good cold forming properties on the construction. Until now, the authors have not met with the results of research to determine the impact of abrasive pastes in container processing. It was found that the additive for container abrasive treatment of abrasive paste causes larger mass losses and faster surface smoothing effects. The treatment was carried out in two stages: in the first stage, the workpieces were deburred and then polished. Considerations were given to the impact of mass of workpieces, machining time and its type on mass loss and changes in the geometric structure of the surface. The surface roughness of machining samples was measured with the Talysurf CCI Lite optical profiler. The suggestions for future research may be to carry out tests using abrasive pastes with a larger granulation of abrasive grains, and to carry out tests for longer processing times and to determine the time after which the parameters of SGP change is unnoticeable.
Źródło:
Archives of Foundry Engineering; 2019, 4; 5-10
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Heat Treatment on Machining Properties of the AlSi9Cu3(Fe) Alloy
Autorzy:
Wieroński, W.
Pezda, J.
Ponikwia, Ł.
Powiązania:
https://bibliotekanauki.pl/articles/379474.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
silumin
heat treatment
machinability
refining
mechanical properties
cutting power
aluminum alloys
obróbka cieplna
obróbka mechaniczna
rafinacja
właściwości mechaniczne
cięcie
stopy aluminium
Opis:
Automation of machining operations, being result of mass volume production of components, imposes more restrictive requirements concerning mechanical properties of starting materials, inclusive of machinability mainly. In stage of preparation of material, the machinability is influenced by such factors as chemical composition, structure, mechanical properties, plastic working and heat treatment, as well as a factors present during machining operations, as machining type, cutting parameters, material and geometry of cutting tools, stiffness of the system: workpiece – machine tool – fixture and cutting tool. In the paper are presented investigations concerning machinability of the EN AC-AlSi9Cu3(Fe) silumin put to refining, modification and heat treatment. As the parameter to describe starting condition of the alloy was used its tensile strength Rm. Measurement of the machining properties of the investigated alloy was performed using a reboring method with measurement of cutting force, cutting torque and cutting power. It has been determined an effect of the starting condition of the alloy on its machining properties in terms of the cutting power, being indication of machinability of the investigated alloy. The best machining properties (minimal cutting power - Pc=48,3W) were obtained for the refined alloy, without heat treatment, for which the tensile strength Rm=250 MPa. The worst machinability (maximal cutting power Pc=89,0W) was obtained for the alloy after refining, solutioning at temperature 510 oC for 1,5 hour and aged for 5 hours at temperature 175 oC. A further investigations should be connected with selection of optimal parameters of solutioning and ageing treatments, and with their effect on the starting condition of the alloy in terms of improvement of both mechanical properties of the alloy and its machining properties, taking into consideration obtained surface roughness.
Źródło:
Archives of Foundry Engineering; 2016, 16, 3; 137-140
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electrochemical micromachining with ultra short voltage pulses
Mikroobróbka elektrochemiczna z wykorzystaniem ultrakrótkich impulsów napięciowych
Autorzy:
Zemann, R
Bleicher, F.
Zisser-Pfeifer, R
Powiązania:
https://bibliotekanauki.pl/articles/139555.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
electrochemical machining
pulsed electrochemical micromachining
PECM
finishing
micromachining
ultra short voltage pulses
obróbka elektrochemiczna
mikroobróbka elektrochemiczna impulsowa
obróbka wykańczająca
mikroobróbka
ultrakrótkie impulsy napięciowe
Opis:
The machining technology of electrochemical micromachining with ultra short voltage pulses (μPECM) is based on the already well-established fundamentals of common electrochemical manufacturing technologies. The enormous advantage of the highest manufacturing precision underlies the fact of the extremely small working gaps achievable through ultra short voltage pulses in nanosecond duration. This describes the main difference with common electrochemical technologies. With the theoretical resolution of 10 nm, this technology enables high precision manufacturing.
Technologia obróbki, polegająca na mikroobróbce elektrochemicznej z wykorzystaniem ultrakrótkich impulsów napięciowych (μPECM) opiera się na ugruntowanych podstawach powszechnie stosowanych elektrochemicznych technologii produkcyjnych. Ogromna zaleta metody, jaką jest najwyższa precyzja procesu obróbki, wynika ze skrajnie małych odstępów roboczych osiągalnych dzięki użyciu ultrakrótkich impulsów napięciowych o czasie trwania rzędu nanosekund. Ta cecha stanowi o głównej różnicy w stosunku do powszechnie stosowanych technologii elektrochemicznych. Przy teoretycznej rozdzielczości 10 nm, technologia μPECM zapewnia najwyższą precyzję obróbki.
Źródło:
Archive of Mechanical Engineering; 2012, LIX, 3; 313-327
0004-0738
Pojawia się w:
Archive of Mechanical Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Examination of coil pipe butt joint made of 7CrMoVTiB10 - 10(t24) steel after service
Badanie podczas remontu złączy doczołowych rur wykonanych ze stali 7CrMoVTiB10 - 10(t24)
Autorzy:
Golański, G.
Gawień, P.
Słania, J.
Powiązania:
https://bibliotekanauki.pl/articles/354991.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
spawanie
mikrostruktury
obróbka cieplna
T24 steel
welded joint
microstructure
Opis:
The paper presents the results of examination of coil pipe butt joint made of 7crmovtib10-10 steel (t24). tested joint was in service for approximately 12 000 hours at the temperature of 540 degree Celsjus and pressure of 5.48mpa. tests have revealed that the structure of all regions of the homogenous welded joint are correct and without any welding imperfections. operation of the weld contributed mainly to advantaged precipitation of carbides especially on grain boundaries - frequently in the contact area of three grains' boundaries as well as in the form of continuous network of precipitates. the measurement showed high hardness of the weld, what indicates high stability of the microstructure. It makes possible to find that post-weld heat treatment is indispensable.
W pracy przedstawiono wyniki badań doczołowego złącza spawanego rury wężownicy ze stali 7crmovtib10-10 (t24). badane złącze eksploatowane było przez około 12 000 godzin w temperaturze 540 stopni Celsjusza przy ciśnieniu 5.48 mpa. Przeprowadzone badania wykazały prawidłową budowę we wszystkich strefach jednorodnego złącza spawanego bez niezgodności spawalniczych. Eksploatacja badanego złącza przyczyniła się przede wszystkim do uprzywilejowanego wydzielania węglików po granicach ziaren, często na styku trzech granic ziaren oraz w postaci tzw. ciągłej siatki wydzieleń. Pomiar twardości wykazał wysoką twardość złącza, co wskazuje na dużą stabilność mikrostruktury. pozwala to na stwierdzenie o konieczności stosowania zabiegów obróbki cieplnej po spawaniu.
Źródło:
Archives of Metallurgy and Materials; 2012, 57, 2; 553-557
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effect of PVD and CVD Coating Structures on the Durability of Sintered Cutting Edges
Wpływ struktury powłok PVD i CVD na trwałość spiekanych ostrzy skrawających
Autorzy:
Staszuk, M.
Dobrzański, L.A.
Tański, T.
Kwaśny, W.
Musztyfaga-Staszuk, M.
Powiązania:
https://bibliotekanauki.pl/articles/353335.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
tool materials
PVD and CVD coatings
surface treatment
machining
artificial neural network
materiały narzędziowe
powłoki PVD i CVD
obróbka powierzchni
obróbka skrawaniem
sztuczne sieci neuronowe
Opis:
In the work it was demonstrated that the exploitative stability of edges from tool ceramics and sintered carbides coated with gradient and multilayer PVD and CVD coatings depends mainly on the adherence of the coatings to the substrate, while the change of coating microhardness from 2300 to 3500 HV0.05, the size of grains and their thickness affect the durability of the edges to a lesser extent. It was found that some coatings showed a fine-grained structure. The coatings which contained the AlN phase with hexagonal lattice showed a considerably higher adhesion to the substrate from sialon ceramics rather than the coatings containing the TiN phase. Better adherence of the coatings containing the AlN phase with hexagonal lattice is connected with the same kind of interatomic bonds (covalent) in material of both coating and ceramic substrate. In the paper the exploitative properties of the investigated coatings in the technological cutting trials were also determined. The models of artificial neural network, which demonstrate a relationships between the edge stability and coating properties such as: critical load, microhardness, thickness and size of grains were worked out.
W pracy wykazano, że trwałość eksploatacyjna ostrzy skrawających z ceramiki narzędziowej i węglików spiekanych pokrytych gradientowymi i wielowarstwowymi powłokami PVD oraz CVD zależy głównie od przyczepności powłok do podłoża, natomiast zmiana mikrotwardości w zakresie od 2300 do 3500 HV0.05. wielkości ziarn oraz ich grubości w mniejszym stopniu wpływają na trwałość ostrzy. Powłoki wykazują drobnoziarnistą strukturę. Powłoki zawierające fazę AlN o sieci heksagonalnej wykazują lepszą przyczepność do sialonowego podłoża niż powłoki zawierające fazę TiN. Lepsza przyczepność powłok zawierających fazę A1N o sieci heksagonalnej związana jest z takim samym rodzajem wiązań międzyatomowych (kowalencyjnych) w materiale powłoki i ceramicznego podłoża. W pracy określono także własności eksploatacyjne powłok w technologicznej próbie toczenia. Zależności pomiędzy trwałością ostrza a własnościami powłok takimi jak obciążenie krytyczne, mikrotwardość, grubość i wielkość ziarna określono z zastosowaniem sztucznych sieci neuronowych.
Źródło:
Archives of Metallurgy and Materials; 2014, 59, 1; 269-274
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ductile Cast Iron Microstructure Adjustment by Means of Heat Treatment
Autorzy:
Mróz, M.
Orłowicz, A. W.
Tupaj, M.
Kupiec, B.
Kawiński, M.
Powiązania:
https://bibliotekanauki.pl/articles/947626.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ductile cast iron
heat treatment
microstructure
żeliwo sferoidalne
obróbka cieplna
mikrostruktura
Opis:
The study presented in this paper concerned the possibility to apply a heat treatment process to ductile cast-iron thin-walled castings in order to remove excessive quantities of pearlite and eutectic cementite precipitates and thus meet the customer’s requirements. After determining the rates of heating a casting up to and cooling down from 900°C feasible in the used production heat treatment furnace (vh = 300°C/h and vc = 200°C/h, respectively), dilatometric tests were carried out to evaluate temperatures Tgr, TAc1start, TAc1end, TAr1start, and TAr1end. The newly acquired knowledge was the base on which conditions for a single-step ferritizing heat treatment securing disintegration of pearlite were developed as well as those of a two-step ferritization process guaranteeing complete disintegration of cementite and arriving at the required ferrite and pearlite content. A purely ferritic matrix and hardness of 119 HB was secured by the treatment scheme: 920°C for 2 hours / vc = 60°C/h / 720°C for 4 hours. A matrix containing 20–45% of pearlite and hardness of 180–182 HB was obtained by applying: 920°C for 2 hours or 4 hours / vc = 200°C/h to 650°C / ambient air.
Źródło:
Archives of Foundry Engineering; 2020, 20, 3; 37-40
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Use of the Precipitation Hardening to Improve the Properties of Combustion Engine Pistons Made of Eutectic Silumins
Autorzy:
Trepczyńska-Łent, Małgorzata
Műller, K.
Powiązania:
https://bibliotekanauki.pl/articles/2079815.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
silumins
precipitation hardening
heat treatment
hardness
siluminy
utwardzanie
obróbka cieplna
twardość
Opis:
The study presents methods to be used for improving the performance parameters of car engine pistons made of EN AC-AlSi12CuNiMg alloy according to the PN-EN 1706: 2011. Pistons of slow sucking and turbocharged engines were researched. A solution heat and ageing treatments were applied according to four variants. Temperatures of the solution heat treatment were: 550 ±5°C; 510°C ±5°C; and alternate: 276 ±5°C/510 ±5°C. The solution time ranged from 6 min to 4 h. Temperatures of the ageing heat treatment were 20°C and 250°C, while the ageing time ranged from 1,5 to 3h. Natural ageing was performed in 5 days. Measurements of hardness HRB and the piston diameters were performed. An improvement in the performance parameters of combustion engines was observed. Three solution heat treatment and ageing variants, allowed to obtain the pistons with hardness equal/higher than pistons of the turbocharged engines. The test results confirmed the possibility of providing a piston with properties exceeding the high load parameters specified by the manufacturer. Further studies will make it possible to improve the effects of the proposed solutions.
Źródło:
Archives of Foundry Engineering; 2021, 21, 4; 77-81
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The effect of toughening combined with microjet cooling during quenching (solution heat treatment) of calcium carbide-modified CuAl10Fe4Ni4 alloy on its mechanical properties
Autorzy:
Górny, Z.
Kluska-Nawarecka, S.
Saja, K.
Powiązania:
https://bibliotekanauki.pl/articles/382512.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
cast aluminum bronzes
heat treatment
odlew aluminiowy
brąz aluminiowy
obróbka cieplna
Opis:
The work presents the results of the experimental research concerning the impact of a heat treatment (toughening) of aluminum bronze CuAl10Fe4Ni4 on its mechanical properties. The conditions of the experiments and selected results are described. A detailed description of the effects of individual heat treatment conditions namely low and high temperature aging is also presented in the work.
Źródło:
Archives of Foundry Engineering; 2013, 13, 1; 29-32
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Large-Area Sodium Titanate Nanorods Formed On Titanium Surface Via NaOH Alkali Treatment
Wielkopowierzchniowe nanopręty tlenku tytanu sodu wytworzone na powierzchni tytanu pod wpływem NaOH
Autorzy:
Lee, K.
Yoo, D.
Powiązania:
https://bibliotekanauki.pl/articles/354441.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sodium titanate
nanorods
alkali treatment
SEM
tytanian sodu
nanopręty
obróbka alkaliczna
Opis:
Ti surfaces covered with large sodium titanate nanorods act as efficient electrodes for energy conversion and environmental applications. In this study, sodium titanate nanorod films were prepared on a Ti substrate in a 5M NaOH aqueous solution followed by heat treatment. The morphological characterization and the crystal structures of the sodium titanate nanorods were investigated via scanning electron microscopy (SEM), X-ray diffraction (XRD), and energy dispersive spectroscopy (EDS). Thin amorphous sodium titanate layers formed during the alkali-treatment, and sodium titanate nanorods were obtained after heat treatment at a temperature of 700°C. The sodium titanate nanorods obtained at this temperature had a thickness of about 80 nm and a length of 1 μm. The crystal structure of the sodium titanate was identified with the use of Na2Ti5O11. The nanorods were agglomerated at a temperature above 900°C, and large-scale nanorods formed on the Ti surface, which may be used for electrodes for energy conversion applications.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1371-1374
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 223

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