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Wyświetlanie 1-15 z 91
Tytuł:
ARMScope – the versatile platform for scanning probe microscopy systems
Autorzy:
Świadkowski, Bartosz
Piasecki, Tomasz
Rudek, Maciej
Świątkowski, Michał
Gajewski, Krzysztof
Majstrzyk, Wojciech
Babij, Michał
Dzierka, Andrzej
Gotszalk, Teodor
Powiązania:
https://bibliotekanauki.pl/articles/221551.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Scanning probe microscopy
AFM
Kelvin Probe force microscopy
scanning tunnelling microscopy
Opis:
Scanning probe microscopy (SPM) since its invention in the 80’s became very popular in examination of many different sample parameters, both in university and industry. This was the effect of bringing this technology closer to the operator. Although the ease of use opened a possibility for measurements without high labour requirement, a quantitative analysis is still a limitation in Scanning Probe Microscopes available on the market. Based on experience of Nano-metrology Group, SPM still can be considered as a tool for quantitative examination of thermal, electrical and mechanical surface parameters. In this work we present an ARMScope platform as a versatile SPM controller that is proved to be useful in a variety of applications: from atomic-resolution STM (Scanning Tunnelling Microscopy) to Multi-resonance KPFM (Kelvin Probe force microscopy) to commercial SEMs (Scanning electron microscopes).
Źródło:
Metrology and Measurement Systems; 2020, 27, 1; 119-130
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Deformation Mechanisms and Fracture of Ni-Based Metallic Glasses
Autorzy:
Lesz, S.
Griner, S.
Nowosielski, R.
Powiązania:
https://bibliotekanauki.pl/articles/353790.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metals
transmission electron microscopy
scanning electron microscopy
fracture
shear bands
Opis:
The cracking of materials and fracture surface is of great practical and academic importance. Over the last few years the development of the fractography of crystalline alloys resulted in a useful tool for the prediction or failure analysis. Many attempts have been made to observe cracks using optical microscopy, X-ray topography and transmission electron microscopy (TEM). Of these techniques, the resolution of optical microscopy and X-ray topography is too poor. By contrast, the resolution of TEM is high enough for detailed information to be obtained. However, in order to apply TEM observations, a thin foil specimen must be prepared, and it is usually extremely difficult to prepare such a specimen from a pre-selected region containing a crack. In the present work, deformation mechanisms fracture surfaces of Ni-based metallic glass samples have been studied by specially designed experiments. In order to study the deformation mechanisms and fracture the Ni-based metallic glasses have been investigated in the tensile test. The structure and fracture surfaces after the decohesion process in tensile tests were observed using transmission electron microscope (TEM) and scanning electron microscope (SEM), respectively. The studies of structure were performed on thin foils. Moreover the investigated tape was subjected to a banding test. Then, the tape was straightened and the thin foil from the area of maximum strain was prepared. This thin foil sample was deformed before the TEM investigation to obtain local tears.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 791-796
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Milling Time on Amorphization of Mg-Zn-Ca Powders Synthesized by Mechanical Alloying Technique
Autorzy:
Lesz, S.
Kremzer, M.
Gołombek, K.
Nowosielski, R.
Powiązania:
https://bibliotekanauki.pl/articles/354717.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Mg-based powders
transmission electron microscopy
scanning electron microscopy
mechanical alloying
Opis:
Mg60 Zn35 Ca5 amorphous powder alloys were synthesized by mechanical alloying (MA) technique. The results of the influence of high-energy ball-milling time on amorphization of the Mg60 Zn35 Ca5 elemental blend (intended for biomedical application) were presented in the study. The amorphization process was investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM). Initial elemental powders were mechanically alloyed in a Spex 8000 high-energy ball mill at different milling times (from 3 to 24 h). Observation of the powder morphology after various stages of milling leads to the conclusion that with the increase of the milling time the size of the powder particles as well as the degree of aggregation change. The partially amorphous powders were obtained in the Mg60 Zn35 Ca5 alloy after milling for 13-18h. The results indicate that this technique is a powerful process for preparing Mg60 Zn35 Ca5 alloys with amorphous and nanocrystalline structure.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 845-851
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of the Quenching Rate on the Structure and Magnetic Properties of the Fe-Based Amorphous Alloy
Autorzy:
Nabiałek, M.
Powiązania:
https://bibliotekanauki.pl/articles/350944.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
transmissions electron microscopy
scanning electron microscopy
amorphous matrials
free volumes
quasidislocation
Opis:
This paper presents the results of investigations into the structure, microstructure and magnetic properties of Fe61Co10Y8W1B20 amorphous alloy. The alloy samples were in two physical forms: (1) plates of approximate thickness 0.5 mm (so-called bulk amorphous alloys) and (2) a ribbon of approximate thickness 35 μm (so-called classic amorphous alloy). The investigations comprised: X-ray diffractometry, Mössbauer spectrometry, transmission electron microscopy, and selected magnetic measurements; all of the investigations were carried out on samples in the as-quenched state. Analysis of the obtained SEM and TEM images, X-ray diffraction patterns, Mössbauer spectrometry results and measurements of the magnetisation in a high magnetic field facilitated collectively the detailed description of the structure of the investigated alloy, which was found to depend on the quenching speed.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 439-444
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Aging and Degradation of Human Fingernail Plates Upon Cosmetic Agents
Autorzy:
Kulesza, S.
Bramowicz, M.
Gwoździk, M.
Wilczyński, S.
Goździejewska, A. M.
Powiązania:
https://bibliotekanauki.pl/articles/354662.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Atomic Force Microscopy
Scanning Electron Microscopy
fractal characterization
nanoscale property mapping
Opis:
The knowledge whether and how chemical species react with tissues is important because of protection against harmful factors, diagnose of dermatological diseases, validation of dermatological procedures as well as effectiveness of topical therapies. In presented work the effects of chemical agents on plates of human fingernails were studied using Atomic Force Microscopy and Scanning Electron Microscopy. Apart from that, mapping of the elastic properties of the nails was also carried out. To obtain reliable measures of spatial evolution of the surface variations, recorded images were analyzed in terms of scaling invariance brought by fractal geometry, instead of common though not unique statistical measures.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 1; 181-184
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanical properties of Ni-Fe-Cu-P-B alloy produced by two component melt spinning (TCMS)
Autorzy:
Wojciechowska, M.
Ziewiec, K.
Kąc, S.
Prusik, K.
Powiązania:
https://bibliotekanauki.pl/articles/351728.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metallic glasses
scanning electron microscopy (SEM)
nanoindentation
transmission electron microscopy TEM
mechanical properties
Opis:
The aim of this work was to investigate the microstructure and mechanical properties of the two-component melt-spun (TCMS) alloy produced from Ni40Fe40B20 and Ni70Cu10P20 melts. The Ni40Fe40B20, Ni70Cu10P20, Ni55 Fe20 Cu5 P10 B10 alloys were arc-melted. Then the alloys were melt-spun in the two different ways i.e.: by casting from a single-chamber crucible and from the two-chamber crucible. All of the above mentioned alloys were processed in the first way and the Ni40Fe40B20 and Ni70Cu10P20 were simultaneously cast on the copper roller from the two-chamber crucible. The microstructure of the alloy was studied using transmission electron microscopy (TEM), scanning electron microscopy (SEM) with energy dispersive spectrometry (EDS) and light microscopy. The mechanical properties were investigated using tensile testing and nanoindentation. The two-component melt-spun (TCMS) amorphous Ni55 Fe20 Cu5 P10 B10 alloy present hardness, tensile strength and Young modulus on the significantly higher level than for a single phase amorphous Ni55 Fe20 Cu5 P10 B10 alloy and slightly below the corresponding values for the Ni40Fe40B20.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 137-140
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Phase Object Observation System Based on Diffraction Phase Microscopy
Autorzy:
Babicz, S.
Stawarz-Graczyk, B.
Wierzba, P.
Powiązania:
https://bibliotekanauki.pl/articles/221523.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
diffraction phase microscopy
DPM
phase objects
Opis:
In the paper authors present a special measurement system for observing phase objects. The diffraction phas microscopy makes it possible to measure the dimensions of a tested object with a nanometre resolution. To meet this requirement, it is proposed to apply a spatial transform. The proposed setup can be based either on a two lenses system (called 4f) or a Wollaston prism. Both solutions with all construction aspects are described in the paper. To make a full analysis of the object shape the authors developed an accurate image processing algorithm, also presented in the paper.
Źródło:
Metrology and Measurement Systems; 2018, 25, 1; 213-221
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
New tool microscopy technique
Autorzy:
Rybka, S.
Powiązania:
https://bibliotekanauki.pl/articles/951236.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
VS120 system
high speed scanning system
differential interference contrast microscopy
virtual microscopy
virtual slide system
Źródło:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology; 2015, 96, 1
0860-7796
Pojawia się w:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cast iron component failure: A metallurgical investigation
Autorzy:
Sudhakar, K. V.
Powiązania:
https://bibliotekanauki.pl/articles/382757.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
cast iron
hardness test
optical microscopy
scanning electron microscopy
fractography
żeliwo
testy twardości
mikroskopia optyczna
mikroskop skaningowy
Opis:
A fractured nutcracker was examined for determining the root cause/s for premature fracture/failure. This is one of the common tools used typically for cracking hard nuts. In this study, metallurgical failure analysis techniques namely, visual inspection, optical microscopy, SEM, and hardness tests were used in investigating the broken product. From the metallurgical analysis, it was determined that the combined effect of low carbon equivalent and presence of inclusions contributed to the sudden fracture of the nut cracking tool.
Źródło:
Archives of Foundry Engineering; 2012, 12, 2s; 67-70
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of the Autocorrelation Function and Fractal Geometry Methods for Analysis of MFM Images
Zastosowanie funkcji autokorelacji oraz geometrii fraktalnej do analizy obrazów struktur domenowych rejestrowanych metodą MFM
Autorzy:
Bramowicz, M.
Kulesza, S.
Czaja, P.
Maziarz, W.
Powiązania:
https://bibliotekanauki.pl/articles/352007.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
atomic force microscopy (AFM)
magnetic force microscopy
magnetic domains
fractal analysis
mikroskopia sił magnetycznych
MFM
analiza fraktalna
Opis:
Presented work is focused on the use of correlation methods for numerical analysis of magnetic stray field over the surface of materials. Obtained results extend our previous findings about application of the autocorrelation function and the fractal analysis for characterization of magnetic surfaces. Several domain images are recorded at various tip-sample gaps (i.e. the lift heights), and then their average widths were extrapolated down to the zero distance in order to estimate the width seen right on the surface. Apart from that, fractal parameters were derived from autocorrelation function, which turned out to be sensitive to the lift height, and might constitute universal measure (the critical lift height), above which the MFM signal became dominated by thermal noises and non-magnetic residual interactions.
Niniejsza praca dotyczy zastosowania metod korelacyjnych do numerycznej analizy obrazów rozkładu pola magnetycznego emitowanego z obszarów spontanicznego namagnesowania. W pracy przedstawiono kontynuację badań nad zastosowaniem funkcji autokorelacji oraz metod analizy fraktalnej w badaniach struktury domenowej oraz charakterystyki emitowanego z nich pola magnetycznego. Wyniki badań wykazują zależność mierzonej metodami mikroskopii sił magnetycznych (MFM) szerokości domen od wysokości skanowania nad badaną powierzchnią, sugerując przeprowadzanie serii pomiarów na różnych wysokościach (h), ich aproksymację z następną ekstrapolacją do powierzchni (h=0). Przeprowadzona analiza fraktalna, wskazuje na możliwość jej aplikacji do charakterystyki zmian sygnału magnetycznego rejestrowanego przez MFM. Pozwala ona również na wyznaczenie wysokości krytycznej (hkr), na której sygnałem dominującym stają się nakładające się na sygnał magnetyczny pozostałości niemagnetycznych interakcji między igłą sondy i badaną powierzchnią, stanowiące rejestrowany przez MFM szum.
Źródło:
Archives of Metallurgy and Materials; 2014, 59, 2; 451-457
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Hot Pressing on the Microstructure of Multi-Layered Ti/Al Composites
Autorzy:
Kowalski, Wojciech
Paul, Henryk
Petrzak, Paweł
Maj, Łukasz
Mania, Izabela
Faryna, Marek
Powiązania:
https://bibliotekanauki.pl/articles/2049145.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ti/al multilayers
electron microscopy
impact test
Opis:
Metal-intermetallic layered (MIL) composites attract considerable attention due to their remarkable structural and ballistic performance. This study aimed to develop a Ti/Al-based multilayered MIL material by adding ceramic powders, since they can improve the composite’s impact resistance. To this end, an experiment was conducted which a stack of alternating Ti and al sheets bonded by hot pressing; Ti/Al multilayers containing additional layers of Al2O3 and SiC powders were also produced. The samples obtained were examined using electron microscopy techniques. The clads’ mechanical properties were investigated using a Charpy hammer. In the reaction zone, only one intermetallic phase occurred: the Al3Ti phase. The model with an additional Al2O3 layer showed the highest impact energy. none of the Ti/Al clads broke during the Charpy impact test, a result proving their high ductility.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 4; 1149-1156
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Texture and Microtexture of Pure (6N) and Commercially Pure Aluminum after Deformation by Extrusion with Forward-Backward Rotating Die (Kobo)
Autorzy:
Bieda, M.
Boczkal, S.
Koprowski, P.
Sztwiertnia, K.
Pieła, K.
Powiązania:
https://bibliotekanauki.pl/articles/958221.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
pure aluminium
KOBO
texture
EBSD
orientation microscopy
Opis:
Pure aluminium (6N) and commercially pure aluminium (99.7) was deformed by KOBO method. Microstructure and texture of both materials after deformation was analyzed by means of scanning and transmission electron microscopy. Advanced methods of crystallographic orientations measurements like Electron Backscatter Diffraction - EBSD (SEM) and microdiffraction (TEM) was used. Grain size distribution and misorientation between grains in cross and longitudinal sections of the samples were analyzed. Differences in size and homogeneity of the grains were observed in both materials. Pure aluminium was characterized by larger grain size in both sections of extruded material. Whereas commercially pure aluminium reveals smaller grain size and more homogeneous and stable microstructure.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 461-468
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of Using Acoustic Microscopy to Evaluate Defects in Spot Welding Joints
Autorzy:
Korzeniowski, M.
Białobrzeska, B.
Powiązania:
https://bibliotekanauki.pl/articles/352373.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
resistance spot welding
acoustic microscopy
aluminium
metallography
Opis:
The article presents the possibilities of using acoustic microscopy to evaluate defects in resistance spot welding joints. For this purpose, the welded joints were made from two grades of aluminium plates EN AW5754 H24 and EN AW6005 T606, which were then subjected to non-destructive testing using acoustic microscopy and conventional destructive testing using traditional light microscopy techniques. Additionally, the study examined the influence of the typical contaminants found in industrial conditions on the quality of the joint.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2B; 1009-1019
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
In Situ TEM Study of Precipitation in a Quasicrystal-Strengthened Al-Alloy
Autorzy:
Boncina, T.
Zupanič, F.
Powiązania:
https://bibliotekanauki.pl/articles/356245.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
precipitation
Al-alloy
transmission electron microscopy TEM
quasicrystal
Opis:
Precipitation kinetics and mechanisms within an Al-Mn-Be-Cu quasicrystal strengthened alloy at 300°C were studied using in-situ transmission electron microscopy. The alloy was cast into a copper mould. Quasicrystalline precipitates formed throughout the Al-rich solid solution, whilst heterogeneous formations of Al2Cu and T-phase occurred on icosahedral quasicrystalline particles formed during solidification. The formation of quasicrystalline particles and T-phase was limited by manganese diffusivity, whilst that of Al2Cu by copper diffusivity. The precipitation produced only a small hardening effect.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 5-9
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of Fractal Analysis Methods for Lift Height Optimization in Magnetic Force Microscopy Measurements
Autorzy:
Bramowicz, M.
Kulesza, S.
Chrostek, T.
Sendrowski, C.
Powiązania:
https://bibliotekanauki.pl/articles/354969.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lift height optimization
magnetic force microscopy
fractal analysis
Opis:
The paper presents results of a research on simulation of magnetic tip-surface interaction as a function of the lift height in the magnetic force microscopy. As expected, magnetic signal monotonically decays with increasing lift height, but the question aris es, whether or not optimal lift height eventually exists. To estimate such a lift height simple procedure is proposed in the paper based on the minimization of the fractal dimension of the averaged profile of the MFM signal. In this case, the fractal dimension ser ves as a measure of distortion of a pure tip-surface magnetic coupling by various side effects, e.g. thermal noise and contribution of topographic features. Obtained simulation results apparently agree with experimental data.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1109-1113
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 91

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