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Wyświetlanie 1-15 z 74
Tytuł:
Structure and properties of the tool ceramics with hard wear resistant coatings
Autorzy:
Pakuła, D.
Staszuk, M.
Gołombek, K.
Śliwa, A.
Mikuła, J.
Powiązania:
https://bibliotekanauki.pl/articles/351856.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
PVD coatings
Nitride Tool Ceramics
Sialon Tool Ceramics
Opis:
This work presents studies of the structure and functional properties of coatings deposited onto indexable inserts made of nitride and sialon tool ceramics with the required properties, i.e. high adhesion, niicrohardness. high resistance to abrasive and diffusion wear in working conditions of high-performance cuttings tools. In the present paper the results of the investigations of the structure, texture, mechanical and functional properties of the Ti(C,N), (Ti.Al)N, Ti(C.N)+(Ti,Al)N coatings were presented. The 80% increase in the hardness of the coatings in comparison to the substrate material was reported. Test coatings are characterized by good adhesion to the substrate. The maximum Lc load of (Ti A1)N coat applied to the substrate from the nitride ceramics is equal to 42 N. In the studied coatings compressive stresses were found. The results of mechanical properties investigations, especially tribological ones correlate with the results of exploitation tests carried out during the cutting test.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 3; 1265-1270
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Technology and Electrophysical Properties of the (K0.44Na0.52Li0.04)NbO3 Ceramics Doped by Cr3+, Zn2+, Sb3+ or Fe3+
Autorzy:
Bochenek, D.
Osińska, K.
Niemiec, P.
Adamczyk, M.
Goryczka, T.
Szych, R.
Powiązania:
https://bibliotekanauki.pl/articles/356149.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lead free ceramics
KNLN ceramics
SEM microstructure
dielectric tests
Opis:
In the work five ceramic compounds based on the (K0.44Na0.52Li0.04)NbO3 (KNLN) material modified with oxides: Cr2O3, ZnO, Sb2O3 or Fe2O3 (in an amount of 0.5 mol.%) were obtained. The KNLN-type composition powder was prepared by solid phase synthesis from a mixture of simple oxides and carbonates, while compacted of the ceramic samples was conducted by free sintering methods. In the work the effect of the used admixture on the electrophysical properties of the KNLN ceramics was presented. The XRD, EDS tests, the SEM measurements of the morphology ceramic samples, dielectric properties and DC electric conductivity were conducted. The research showed that the used admixtures introduced into the base of KNLN-type composition improve the microstructure of the ceramic samples and improve their sinterability. In the case of the dielectric measurements, it was observed a decrease in the maximum dielectric permittivity at the TC for dopred KNLN-type samples. The addition of an admixture of chromium, zinc, antimony or iron in an amount of 0.5 mol.% to the base composition (K0.44Na0.52Li0.04)NbO3 practically does not change the phase transition temperature. The diminution in the density value of doped KNLN ceramics was attributed to the alkali elements volatilization.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1401-1409
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of the sol-gel method at the fabrication of PLZT:Yb3+ ceramics
Autorzy:
Osińska, K.
Płońska, M.
Marzec, A.
Powiązania:
https://bibliotekanauki.pl/articles/353490.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
PLZT:Yb3+ ceramics
sol-gel method
perovskite structure ceramics
Opis:
The aim of presented study was to obtain the PLZT:Yb ceramics. Nanopowders of itterbiuni doped PLZT materials were synthesized by the sol-gel method from high quality metaloorganic precursors, as lead (II) acetate, lanthanum acetate, ytterbium acetate, zirconium (IV) propoxide and titanium (IV) propoxide. Anhydrous acetic acid and n-propyl alcohol were used as solvents, while acetyloacetone was added as stabilizer of hydrolysis reactions. Thermal evolution of the dried gels, before and after calcination, was studied by the simultaneous thermal analysis. The amorphous PLZT:Yb3+ gels were first calcined in the furnace at T = 850°C, and then mixed in the planetary ball mill. Additionally, the mean particle sizes were calculated by means of powder specific surface area measurements, based on the BET physical adsorption isotherm. Such obtained powders were subsequently pressed into pellets, and sintered by the free sintering method at temperature T= 1250°C / 6h. The morphology of fabricated PLZT:Yb:3+ ceramic powders and samples was studied using Scanning Electron Microscopy. Chemical characterization of samples was carried on using the Energy-dispersive X-ray spectroscopy – EDS system. Studies provided detailed data concerning die relationships between doping and preparing conditions on the basic physical and chemical properties of obtained ceramic materials.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 3; 1441-1446
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cast Iron Reinforced with Foaming Ceramic Insert
Autorzy:
Dulska, A.
Studnicki, A.
Cholewa, M.
Szajnar, J.
Powiązania:
https://bibliotekanauki.pl/articles/382732.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ceramics
cast iron composite
ceramics insert
materiał ceramiczny
kompozyt żeliwny
wkład ceramiczny
Opis:
This paper presents matters related to production of ceramic and cast iron composite. The composite was made with the use of a foam structured ceramic insert. The tests included measuring of hardness, impact strength and resistance to abrasive wear of the composite produced. On the basis of obtaining results was stated that the use of foamed ceramic filters provides good conditions of filling a ceramic framework with molten grey or chromium cast iron. The growth of hardness of the ceramic-grey cast iron composite is ca. 60% as compared to the grey cast iron hardness. The growth of hardness of the ceramic-chromium cast iron composite is slight and does not exceed 5 % in comparison to the chromium cast iron. Introduction of the ceramic inserts deteriorates the cast iron impact strength by ca. 20 - 30 %. The use of ceramic inserts increases the resistance to abrasive wear in case of grey cast iron by ca. 13% and in case of the chromium cast iron by ca. 10 %.
Źródło:
Archives of Foundry Engineering; 2018, 18, 2; 137-140
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Lanthanum Dopant on the Structure and Electric Properties of BaBi2Nb2O9 Ceramics
Autorzy:
Adamczyk-Habrajska, M.
Goryczka, T.
Szalbot, D.
Dzik, J.
Rerak, M.
Bochenek, D.
Powiązania:
https://bibliotekanauki.pl/articles/353535.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ferroelectric relaxor
ceramics
impedance spectroscopy
Opis:
The paper reports the consequences of lanthanum modifications of barium bismuth niobiate (BaBi2 Nb2 O9) ceramics. The discussed materials were prepared by solid state synthesis and a one-step sintering process. The investigations are focused on dielectric aspects of the modification. The presented results reveal that the trivalent lanthanum ions incorporate twovalent barium ions, which is connected with the creation of A-site cationic vacancies as well as oxygen vacancies. Such a scenario results in significant decreasing in grain boundaries resistivity. The activation energy of grain boundaries conductivity is significantly reduced in the case of lanthanum admixture.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 1; 207-214
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Homogenization and Micro/Nano Source of Starting Powders on Format Ion of the Single YAP Phase
Autorzy:
Michalik, D.
Pawlik, T.
Plewa, J.
Sopicka-Lizer, M.
Powiązania:
https://bibliotekanauki.pl/articles/351720.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
YAP
scintillators
synthesis
polycrystalline ceramics
Opis:
Manufacturing high purity polycrystalline YAlO3 (YAP) ceramics could replace monocrystalline YAP thus recently it is an interesting task for low cost producers of scintillators. The paper presents influence of different source of initial oxide powders (micro/nano powders of Y2O3 and Al2O3) and the method of their homogenization on the formation of a YAP phase. The solid state reaction method was used to prepare YAP powder or ceramic pellets. After preheating, all samples in the form of powders and pellets were heat-treated in the temperature range of 1050-1650 °C. DTA method was applied for examination of the phase crystallization in the tested system. X-ray diffraction method (XRD) was used for characterization of the phase composition. X-ray microanalysis (EDS) was used to control homogeneity in the small areas. Morphology of the resultant samples are presented on SEM pictures. The results show a significant influence of the starting powders on the homogeneity, purity and temperature of formation of the main phase.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 4; 1753-1760
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis of SrTiO3 by the Calcination of SrCO3 and TiO2 Mixtures Intensively Ground by Means of High Energy Milling
Autorzy:
Rocha-Rangel, Enrique
Pech-Rodríguez, Wilian J.
López-Hernández, Juan
Calles-Arriaga, Carlos A.
Armendáriz-Mireles, Eddie N.
Castillo-Robles, José A.
Rodríguez-García, José A.
Powiązania:
https://bibliotekanauki.pl/articles/356247.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
SrTiO3
mechanochemistry
insulating ceramics
perovskite
Opis:
A SrTiO3 electroceramic with perovskite structure was produced by the calcination of a mixture of SrCO3 and TiO2 intensively grounded by high energy milling. For this purpose, raw materials were mixed in stoichiometric amounts in a planetary type mill; the obtained powder mixture was calcined for 2 h at temperatures between 800 and 1300°C. Samples resulting from the calcination were characterized by XRD, FTIR, SEM analysis and electrical measurements. From XRD, it was determined that the SrTiO3 formed presents the cubic structure of perovskite. The complete reaction for SrTiO3 compound formation occurs at 1200°C. Micrograph observations indicate the presence of a homogeneous microstructure with tiny grain size. The measured values of electrical resistivity were within the typical range of insulating materials.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 621-626
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigations on Wear Mechanisms of PVD Coatings on Carbides and Sialons
Autorzy:
Staszuk, M.
Pakuła, D.
Pancielejko, M.
Tański, T.
Dobrzański, L. A.
Powiązania:
https://bibliotekanauki.pl/articles/350842.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
PVD coatings
Sialon Tool Ceramics
carbides
Opis:
The paper presents the results on the wear resistance of PVD coatings on cutting inserts made from sintered carbide and sialon ceramics. The exploitative properties of coatings in technological cutting trials were defined in the paper, which also examined the adhesion of coatings to the substrate, the thickness of the coating, and the microhardness. As a result, it was found that isomorphic coating with AlN-h phase of covalent interatomic bonds exhibits much better adhesion to the sialon substrate than isomorphic coating with titanium nitride TiN. These coatings assure the high wear resistance of the coated tools, and the high adhesion combined with the high microhardness and fine-grained structure assure an increase in the exploitative life of the coated tools. In the case of coatings on substrate made from sintered carbide, there was a significant influence on the properties of the tools coated with them as concerns the existence of the diffusion zone between the substrate and the coating.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 4; 2095-2100
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study of CuO and V2O5 Effect on IR Spectra of Polycrystalline Bismuth Niobate
Autorzy:
Kuźniarska-Biernacka, I.
Lisińska-Czekaj, A.
Czekaj, D.
Powiązania:
https://bibliotekanauki.pl/articles/352587.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
BiNbO4
ceramics
SEM
FTIR spectroscopy
Opis:
Bismuth niobate (BiNbO4) ceramics were fabricated by mixed oxide method and sintered by presureless sintering method. BiNbO4 ceramics doped with V2 O5 additive in amount 0.125 wt%, 0.250 wt% and 1 wt% of was sintered at T = 910°C whereas BiNbO4 ceramics doped with 2 wt% of CuO additive was sintered at T = 890°C and T = 910°C. It was found that V2 O5 additive improved morphology of the ceramic samples. However, the chemical composition of BiNbO4 ceramics in relation to bismuth oxide and niobium oxide manifested a tendency of lack of Bi2 O3 component. Absorption bands for the BiNbO4 compound were identified. FTIR band positions associated with NbO6 octahedra suggested that the crystal structure changes after V2 O5 incorporation.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 817-821
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The relationship between microstructure and mechanical properties of directly bonded copper-alumina ceramics joints
Autorzy:
Pietrzak, K.
Olesińska, W.
Kaliński, D.
Strojny-Nędza, A.
Powiązania:
https://bibliotekanauki.pl/articles/199776.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
directly bonded copper-alumina ceramics joints
Opis:
The effect of phase transformations induced in the surface layer of alumina ceramics during its direct joining with copper activated with oxygen or titanium on the mechanical strength of the ceramic/copper joints was examined. The materials used in the experiments were an alumina single crystal, alumina ceramics (97.5 wt% Al2O3), the cermet mixtures: Cu-Cu2O with 10-50 wt% of Cu2O, copper with 5 wt% of Ti, and copper with 5 wt% of Ti and 10 wt% of Ag. The microstructure of the transition layer was examined by the X-ray diffraction method (XRD), scanning electron microscopy method (SEM) and energy dispersive x-ray spectroscopy (EDX). The mechanical strength of the joints was measured using the three-point bending method. The amount of oxygen optimal for the joining process was determined. It has been demonstrated that the cohesion of the joints depends not only on the formation of the individual phases but also, or even primarily, on the microstructure of the transition layer formed between them.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2014, 62, 1; 23-32
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Multiscale Approach for Modeling Fracture in Piezoelectric Ceramics
Autorzy:
Biglar, M.
Stachowicz, F.
Trzepieciński, T.
Gromada, M.
Powiązania:
https://bibliotekanauki.pl/articles/355254.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
barium titanate
BEM
boundary element method
ceramics
Opis:
The barium titanate material is the most intensively studied perovskite material due to its wide use in the ceramic industry. Barium titanate is also technologically important material owing to its ferroelectric behaviour at and above room temperature. The paper presents an effective implementation of boundary element multiscale method in analyzing of fracture of piezoelectric ceramics. This method can be easily used to get a better understanding of damage mechanism in the ceramic materials in order to improve the constitutive models and to support the future design of those materials. In this method the relation of boundary element method for obtaining traction is presented. The main advantage of boundary element method is the reduction of the dimensionality of the problem. Boundary element method becomes very attractive in cases of numerically complex problems that are computationally expensive.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 22-28
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Calcium Ions on the Structure and Properties of LaMnO3
Autorzy:
Bara, M.
Dzik, J.
Feliksik, K.
Kozielski, L.
Wodecka-Duś, B.
Goryczka, T.
Zarycka, A.
Adamczyk-Habrajska, M.
Powiązania:
https://bibliotekanauki.pl/articles/353112.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
LCMO
ceramics
manganites
X-ray diffraction
SEM
Opis:
La0,7 Ca0,3 MnO3 polycrystalline were synthesized from La2 O3 , CaO and MnO2 powder mixture using a solid state reaction technique. The compound powders were obtained through the free sintering method at different temperatures and sintering times in order to study the influence of technological conditions on Ca doped La manganites. The most important physical features as structure, microstructure and morphology were described after X-ray diffraction investigation. Photographs of the specimen fractures were taken with SEM (scanning electron microscope) and they revealed high porosity of the tested material and great tendency for its grains to create agglomerates. Influence of doping and technological conditions on lattice parameters were studied by means of Rietvield analysis. The XRD measurements reveal that La0,7 Ca0,3 MnO3 has orthorhombic symmetry with Pnma space group.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 3; 1189-1195
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Biomechanical analysis of individual all-ceramic abutments used in dental implantology
Autorzy:
Ziębowicz, B.
Ziębowicz, A.
Bączkowski, B.
Kajzer, W.
Kajzer, A.
Powiązania:
https://bibliotekanauki.pl/articles/353180.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
dental implant
abutment
zirconia ceramics
cyclic fatigue
Opis:
Biomechanical analysis of individual all-ceramic abutments used in dental implantology The paper presents the results of finite element analysis and experimental testing under simulated physiological loading conditions on issues shaping the functional properties of individual all-ceramic abutments manufactured by CAD'CAM technology The conducted research have cognitive significance showing the all-ceramic abutment behavior, as a key element of the implantological system, under the action of cyclic load. The aim of this study was evaluation the fatigue behavior of yttria-stabilized zirconia abutment submitted to cyclic stresses, conducted in accordance with EN ISO 14801 applies to dynamic fatigue tests of endosseous dental implants.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 3; 1357-1362
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Acoustic Matching Characteristics of Annular Piezoelectric Ultrasonic Sensor
Autorzy:
Li, Haoran
Hu, Yan
Li, Laibo
Xu, Dongyu
Powiązania:
https://bibliotekanauki.pl/articles/2141675.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
piezoelectric ceramics
ultrasonic sensors
acoustic matching characteristics
Opis:
Using intelligent materials and sensors to monitor the safety of concrete structures is a hot topic in the field of civil engineering. In order to realize the omni-directional monitoring of concrete structural damage, the authors of this paper designed and fabricated an embedded annular piezoelectric ultrasonic sensor using the annular piezoelectric lead zirconate titanate (PZT) ceramic as a sensing element and epoxy resin as the matching and the backing layers. The influence of different matching and backing layers thickness on the acoustic characteristic parameters of the sensor were studied. The results show that the resonant frequency corresponding to the axial mode of annular piezoelectric ceramics moves toward the high frequency direction with the decrease of the height of piezoelectric ceramics, and the radial vibration mode increases as well as the impedance peak. With the thickness of the backing layer increases from 1 mm to 2 mm, the radial resolution of the annular piezoelectric ultrasonic sensor is enhanced, the pulse width is reduced by 39% comparing with the sensors which backing layer is 1 mm, and the head wave amplitude and −3 dB bandwidth are increased by 61% and 66%, respectively. When the matching layer thickness is 3 mm, the sensor has the highest amplitude response of 269 mV and higher sensitivity.
Źródło:
Archives of Acoustics; 2022, 47, 2; 275-284
0137-5075
Pojawia się w:
Archives of Acoustics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of La3+ Doping Effect on Piezoelectric Coefficients of BLT Ceramics
Autorzy:
Wodecka-Dus, B.
Kozielski, L.
Erhart, J.
Pawełczyk, M.
Radoszewska, D.
Adamczyk, M.
Bochenek, D.
Powiązania:
https://bibliotekanauki.pl/articles/352118.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
BLT
piezoelectric coefficients
Lead-free piezoelectric ceramics
Opis:
Effects of La3+ admixture in barium lanthanum titanate (BLT) ceramics system with colossal permittivity on performance of prospective piezoelectric cold plasma application were studied. Usage of cold atmospheric pressure plasma appears promising in terms of industrial and healthcare applications. Performed investigation provide consistent evaluation of doping lanthanum amount on piezoelectric coefficients values with simultaneous capability of charge accumulation for effective plasma generation. Modification of ferroelectric materials with heterovalent ions, however with the lower radii than the original atoms, significantly affects their domain mobility and consequently electromechanical properties. To determine the piezoelectric coefficients, the resonanceantiresonance method was implemented, and values of piezoelectric and dielectric parameters were recorded. Finally the results indicated that addition of 0.4 mol.% of La3+ ions to the ceramic structure maximally increased the values of piezoelectric coefficient to d33 = 20 pC/N and to huge dielectric constant to ε33 T = 29277.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2A; 691-696
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 74

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