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Wyszukujesz frazę "Raman spectroscopy." wg kryterium: Temat

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    Wyświetlanie 1-13 z 13
    Tytuł:
    Detection of illicit chemicals by portable Raman spectrometer
    Autorzy:
    Smulko, J.
    Kwiatkowski, A.
    Gnyba, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/200103.pdf
    Data publikacji:
    2011
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Raman spectroscopy
    chemical detection
    lasers
    detection efficiency
    Opis:
    The Raman spectrometers can be built as the portable devices and can be used in various places to detect illicit chemicals. This method has become popular due to deficiency of other fast methods that could be applied against terrorist attacks or could help police at their work. The Conception of a portable Raman spectrometer has been presented. The Description enclosures the presentation of the prepared device and its possible applications by presenting exemplary detection results.
    Źródło:
    Bulletin of the Polish Academy of Sciences. Technical Sciences; 2011, 59, 4; 449-452
    0239-7528
    Pojawia się w:
    Bulletin of the Polish Academy of Sciences. Technical Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Portable Raman spectrometer - design rules and applications
    Autorzy:
    Gnyba, M.
    Smulko, J.
    Kwiatkowski, A.
    Wierzba, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/200133.pdf
    Data publikacji:
    2011
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Raman spectroscopy
    chemical detection
    lasers
    detection algorithms
    Opis:
    Raman spectroscopy has become more popular due to its new prospective field applications in forensic sciences, war against terrorism, environment protection and other field chemical analysis. Raman spectrometers can be miniaturised to portable devices and their price is decreasing due to development of optoelectronics components. Unfortunately, this technology has still numerous limitations that influence their design and limit the scope of possible applications. The conception and design of the portable Raman spectrometer is described, including discussion of performance and limitations of representative components of such device available on the market. An enhanced portable Raman spectrometer using two lasers, one emitting at 355 nm and the other at 785 nm, and employing advanced signal acquisition and data processing methods is presenented. Advantages of such system are outlined and example measurement results acquired using equivalent hardware are presented. Data processing flow for identification of chemicals is also described.
    Źródło:
    Bulletin of the Polish Academy of Sciences. Technical Sciences; 2011, 59, 3; 325-329
    0239-7528
    Pojawia się w:
    Bulletin of the Polish Academy of Sciences. Technical Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Examination of the Properties of Samples from Glass-Epoxy Core Rods for Composite Insulators Subjected to DC High Voltage
    Autorzy:
    Wieczorek, K.
    Jaroszewski, M.
    Ranachowski, P.
    Ranachowski, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/351254.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    DC high voltage
    composite insulator
    glass-epoxy core
    dielectric spectroscopy
    Raman spectroscopy
    Opis:
    This article presents the results of an examination performed on a set of samples of glass-epoxy core rods used in composite insulators with silicone rubber housings. The goal of the examination was to test the aging resistance of the core material when exposed to Direct Current (DC) high voltage. Long term exposure of a glass-epoxy core rod to DC high voltage may lead to the gradual degradation of its mechanical properties due to the ion migrations. Electrolysis of the core material (glass fiber) may cause electrical breakdown of the insulators and consequently lead to a major failure. After being aged for 6000 hours under DC high voltage, the samples were subjected to microscopic analysis. Their chemical composition was also examined using Raman spectroscopy and their dielectric losses and conductance in the broad range of frequencies were tested using dielectric spectroscopy.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1281-1286
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Raman Spectroscopy Studies of Carbon-Based Cathode Materials during Aluminum Electrolysis
    Autorzy:
    Wang, Wei
    Chen, Weijie
    Powiązania:
    https://bibliotekanauki.pl/articles/352779.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    aluminium electrolysis
    carbon cathodes
    Raman spectroscopy
    creep deformation
    sodium expansion
    Opis:
    The sodium expansion and creep strain of semi-graphitic cathodes are investigated using a modified Rapoport apparatus. To further understanding of the sodium and bath penetration damage processes, the impact of external stress fluence on the carbon cathode microstructure has been defined with XRD analysis, Raman spectroscopy and scanning electron microscope (SEM). Graphite atoms fracture into smaller fragments that are less directional than the pristine platelets, which allows for a possible filling of the cracks that thus develop by the sodium and bath during aluminum electrolysis. The average microcrystalline size (calculated by Raman spectroscopy) is reduced by the deformation. The decreased intensity and widened 'G' and 'D' peaks in the analysis indicate the poor order of the sheets along the stacking direction while the consistent layered graphite structure is sustained.
    Źródło:
    Archives of Metallurgy and Materials; 2019, 64, 4; 1257-1261
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Examination of Sol-Gel Derived Hydroxyapatite Enhanced with Silver Nanoparticles using OCT and Raman Spectroscopy
    Autorzy:
    Głowacki, M. J.
    Gnyba, M.
    Strąkowska, P.
    Gardas, M.
    Kraszewski, M.
    Trojanowski, M.
    Strąkowski, M. R.
    Powiązania:
    https://bibliotekanauki.pl/articles/221475.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    hydroxyapatite
    sol-gel
    nanoparticles
    Raman spectroscopy
    optical coherence tomography (OCT)
    Opis:
    Hydroxyapatite (HAp) has been attracting widespread interest in medical applications. In a form of coating, it enables to create a durable bond between an implant and surrounding bone tissues. With addition of silver nanoparticles HAp should also provide antibacterial activity. The aim of this research was to evaluate the composition of hydroxyapatite with silver nanoparticles in a non-destructive and non-contact way. For control measurements of HAp molecular composition and solvent evaporation efficiency the Raman spectroscopy has been chosen. In order to evaluate dispersion and concentration of the silver nanoparticles inside the hydroxyapatite matrix, the optical coherence tomography (OCT) has been used. Five samples were developed and examined ‒ a reference sample of pure HAp sol and four samples of HAp colloids with different silver nanoparticle solution volume ratios. The Raman spectra for each solution have been obtained and analyzed. Furthermore, a transverse-sectional visualization of every sample has been created and examined by means of OCT.
    Źródło:
    Metrology and Measurement Systems; 2017, 24, 1; 153-160
    0860-8229
    Pojawia się w:
    Metrology and Measurement Systems
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Mass spectrometry approaches in proteomic and metabolomic studies
    Autorzy:
    Rodziewicz, P.
    Swarcewicz, B.
    Chmielewska, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/80650.pdf
    Data publikacji:
    2014
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    proteomics
    metabolomics
    genomic DNA
    nuclear magnetic resonance
    mass spectrometry
    Fourier transform infrared spectroscopy
    Raman spectroscopy
    Źródło:
    BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology; 2014, 95, 3
    0860-7796
    Pojawia się w:
    BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructural characterization of cast magnesium matrix composites by Raman microscopy
    Autorzy:
    Malik, M. A.
    Braszczyńska-Malik, K. N.
    Majchrzak, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/380033.pdf
    Data publikacji:
    2013
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    magnesium matrix composites
    SiC
    Mg2Si
    Raman spectroscopy
    kompozyt magnezowy
    spektroskopia Ramana
    Opis:
    Cast magnesium matrix composites reinforced with silicon carbide particles were investigated by using Raman microscopy. 3C, 4H and 6H polytypes of SiC particles were identified in the investigated composites. Additionally, Mg2Si compound was detected by Raman microscopy in the composites microstructure.
    Źródło:
    Archives of Foundry Engineering; 2013, 13, 1; 95-98
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization and experimental investigation of TiN micro tubular coil heater using raman spectroscopy
    Charakterystyka i badania doświadczalne mikro-grzałek z TiN metodą spektroskopii ramanowskiej
    Autorzy:
    Sureshkannan, G
    Mohan Kumar, G
    Saravanan, M. P.
    Powiązania:
    https://bibliotekanauki.pl/articles/354813.pdf
    Data publikacji:
    2013
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    micro tubular coil heaters
    Raman spectroscopy
    thermal profile
    mikro cewki
    spektroskopia ramanowska
    profil termiczny
    Opis:
    Raman spectroscopy is a commonly used tool in bio-diagnostics and micro sensor technology. Surface-enhanced Raman scattering provides high signal enhancements especially at micro and nanostructured metallic surfaces. Micro tubular coil heaters have been widely investigated because of their extensive applications in PET Preformed Moulds, Hot Runner Nozzles & Bushings and Thin Walled Container Moulds and other Microsystems. This paper describes the characterization, experimental investigation and analysis of Titanium Nitride (TiN) micro tubular coil heater using Raman spectroscopy and Comsol multiphysics. The material characterization was performed using Raman spectrometer and the geometric optimization for the micro tubular coil heater was performed by simulating a wide range of possible geometries using COMSOLTM, a commercial Finite Element Analysis (FEA) package. The characteristic dimensions of the microstructures are varied and the results are discussed and compared to each other. The simulated results of micro tubular heaters having an improved temperature distribution over the sensing area and a higher density of integration is presented in this paper.
    Spektroskopia ramanowska jest powszechnie stosowanym narzędziem w bio-diagnostyce i technologii mikroczujnika. Powierzchniowo wzmocniona spektroskopia ramanowska zapewnia wysokie wzmocnienie sygnału zwłaszcza na mikro i nanostrukturalnych powierzchniach metalowych. Mikro-grzałki (mikro cewki) były szeroko badane ze względu na ich szerokie zastosowanie w formowaniu wtryskowym, podgrzewaczach dysz i tulej, i cienkościennych formach i innych mikrosystemach. Artykuł opisuje charakterystykę, badania eksperymentalne i analizę mikro-grzałki rurowej z azotku tytanu (TiN) za pomocą spektroskopii ramanowskiej i oprogramowania COMSOL Multiphysics. Charakterystykę materiału przeprowadzono za pomocą spektrometru Ramana a geometryczna optymalizacje dla mikro-grzałki prowadzono symulując szeroki zakres możliwych geometrii, za pomocą COMSOLTU, komercyjnego pakietu do analizy metodą elementów skończonych. Charakterystyczne wymiary mikrostruktur są zróżnicowane, a wyniki zostały omówione i porównane ze sobą. Symulowane wyniki mikro-cylindrycznych grzejników o ulepszonym rozkładzie temperatur w obszarze wykrywania i większej gęstości integracji zostały przedstawione w niniejszym artykule.
    Źródło:
    Archives of Metallurgy and Materials; 2013, 58, 2; 641-645
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Surface Treatment And Modification Of Graphene Using Organosilane And Its Thermal Stability
    Obróbka powierzchniowa i modyfikacja grafenu przy użyciu organosilanu i jego stabilność termiczna
    Autorzy:
    Kim, D.-S.
    Dhand, V.
    Rhee, K.-Y.
    Park, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/354056.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    graphite
    thermal properties
    Raman spectroscopy
    surface treatment
    3-APTES
    grafit
    właściwości termiczne
    spektroskopia Ramana
    obróbka powierzchniowa
    Opis:
    In this study, graphene was functionalized via acid oxidation in the presence of a mixture of concentrated sulfuric acid and nitric acid. The oxidized graphene was silanized using the coupling agent, 3-aminopropyltriethoxsilane, resulting in functionalized graphene. The oxidized graphene and functionalized graphene were characterized by X-Ray diffraction, Fourier transform infrared spectroscopy, High-resolution micro Raman spectroscopy, thermogravimetric analysis, and atomic force microscopy to confirm the presence of functional moieties on the graphene surface. Thermal studies also demonstrate that the functionalized material is thermally stable up to higher temperatures.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1387-1391
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A multi-analytical approach for the analysis of cation distribution in a aluminoceladonite structure
    Autorzy:
    Kądziołka-Gaweł, Mariola
    Dulski, Mateusz
    Czaja, Maria
    Krzykawski, Tomasz
    Szubka, Magdalena
    Powiązania:
    https://bibliotekanauki.pl/articles/2172615.pdf
    Data publikacji:
    2022
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    aluminoceladonite
    ions position characterization isomorphic substitutions
    Fe bearing phyllosilicates
    X-ray photoelectron spectroscopy
    Mössbauer spectroscopy
    Raman spectroscopy
    glinokrzemiany
    krzemiany warstwowe
    rentgenowska spektrometria fotoelektronów
    XPS
    spektroskopia mössabuerowska
    spektroskopia Ramana
    Opis:
    In this paper cation arrangement in two samples of aluminoceladonite, emerald green and dark-green were studied by Mössbauer, Raman and X-ray photoelectron spectroscopies. The X-ray photoelectron spectroscopy (XPS) spectra obtained in the region of the Si2p, Al2p, Fe2p, K2p, and O1s core levels provided information, for the first time highlighting a route to identify the position of Si, Al, K, and Fe cations in a structure of layered silicates. The XPS analysis showed the presence of Al in tetrahedral and octahedral coordination while the K2p line indicated the possibility of K+ substitution by other cations in interlayer sites. Mössbauer spectroscopy provided information about crystal chemistry with respect to the local electronic and geometric environment around the Fe atom and to distortions of the polyhedra. It turned out that iron was located mostly in the cis-octahedra position wherein about 75% of iron appeared in the form of Fe3+. The most preferred cation combinations around Fe corresponded to 3Fe3+ ions and MgFe2+Fe3+/2MgFe3+. Raman spectroscopy illustrated aluminium substitution in silicon and iron positions wherein the concentration of the aluminium determined the degree of structural distortion within the layered system. These isomorphic substitutions implied a typical band arrangement in the hydroxyl region, which has not been observed in celadonites so far.
    Źródło:
    Acta Geologica Polonica; 2022, 72, 3; 353--368
    0001-5709
    Pojawia się w:
    Acta Geologica Polonica
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization of carbon nanofibers/ ZrO2 ceramic matrix composite
    Charakterystyka kompozytu o osnowie ceramicznej modyfikowanej włóknami węglowymi
    Autorzy:
    Duszová, A
    Morgiel, J.
    Bastl, Z.
    Mihály, J
    Dusza, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/356257.pdf
    Data publikacji:
    2013
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    carbon nanofibers
    nanocomposites
    transmission electron microscopy
    high resolution transmission electron microscopy
    Raman spectroscopy
    włókna węglowe
    nanokompozyty
    transmisyjny mikroskop elektronowy
    mikroskopia skaningowa elektronowa
    spektroskopia Ramana
    Opis:
    Carbon micro/nanofibers prepared by catalytic chemical vapor deposition have been characterized in the form of powders and in the form of filaments, intercorporated in the matrix of ZrO2. Scanning electron microscopy, transmission electron microscopy, high resolution electron microscopy, electron spectroscopy for chemical analysis and Raman spectroscopy have been used. The outer diameter of the fibers varied from 50 nm to 600 nm with an average diameter of 120 nm, length from several micrometers to several tens of micrometers and inner diameters from 20 nm to 230 nm. Two types of fibers have been identified; cylindrical which consists of a distinct graphite layers parallel to the fiber axes and bamboo - shaped fibers with walls which are built from domains with different orientations of graphite layers. The fibers contain 99.05 at.% carbon and 0.95 at.% oxygen with a binding energy of O (1s) electrons of 532.7 e V which corresponds to carbon in C-O bonds. In the first-order Raman spectra, the position of the band G was found at 1600 cm-1 and D at 1282 cm-1. The CNFs in ZrO2+ CNFs composite have been relatively well dispersed, however clusters of CNFs together with porosity are present as a result of the difficulty of dispersing, too. TEM and HREM revealed that the CNFs are usually located at the grain boundaries of ZrO2 in the form of undamaged nanofibers or disordered graphite.
    Włókna węglowe przygotowane metodą osadzania z par (tzw. Chemical Vapour Deposition), były badane bezpośrednio po wytworzeniu oraz po wprowadzeniu do osnowy ceramicznej metodami elektronowej mikroskopii skaningowej, transmisyjnej oraz spektroskopii ramanowskiej. Średnica włókien wahała się pomiędzy 50 nm, a 600 nm przy sredniej wartości ok.120 nm, podczas gdy ich długość wynosiła od kilku do kilkudziesięciu mikrometrów. Identyfikowano dwa rodzaje budowy włókien, tj. cylindryczne oraz z wewnętrznymi przekładkami typu „łodygi bambusa“. Włókna węglowe zawierały do 0.95 at. % tlenu o energi wiazania O (1s) ok.532.7 e V, co odpowiada wiązaniu C-O. Na pierwszym widmie Ramana pasmo G identyfikowano dla 1600 cm-1, a pasmo D dla 1282 cm-1. Badania kompozytu wykazałay równomierny rozkład włókien w ceramicznej osnowie. W sąsiedztwie większych aglomeratów stwierdzono tendencje do występowania pustek. W czasie spiekania przeważająca część włókien zachowała swoją rurkową strukturę, natomiast pozostały materiał węglowy uległ przemianie do słabo uprządkowanych struktur grafitu lub nawet uległ amorfizacji.
    Źródło:
    Archives of Metallurgy and Materials; 2013, 58, 2; 459-463
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermal history of the Carboniferous strata in the northern part of the Intra-Sudetic Basin (SW Poland): A combined Raman spectroscopy and organic petrography study
    Autorzy:
    Botor, Dariusz
    Toboła, Tomasz
    Waliczek, Marta
    Powiązania:
    https://bibliotekanauki.pl/articles/1835585.pdf
    Data publikacji:
    2020
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Raman spectroscopy
    vitrinite reflectance
    dispersed organic matter
    coalification
    Lower Silesia Coal District
    Bohemian Massif
    spektroskopia Ramana
    refleksyjność witrynitu
    rozproszona materia organiczna
    uwęglenie
    Dolnośląskie Zagłębie Węglowe
    Masyw Czeski
    Opis:
    Raman spectroscopy and vitrinite reflectance measurements of dispersed organic matter from Carboniferous shales in boreholes in the northern part of the Intra-Sudetic Basin were used for thermal history reconstruction. Microscopic investigations have shown that the organic matter is dominated by the vitrinite maceral group. In analysed samples, organic matter shows a varied degree of thermal alteration determined by the mean random vitrinite reflectance (VRo) ranging from 0.72% to 3.80%. Mean apparent maximum vitrinite reflectance (R’max) values reached 4.98%. The full width at half maximum of D1 and G bands in Raman spectra are well-correlated with mean VRo and R’max. Thermal maturity in the boreholes shows a regular increase with depth. Geological data combined with Raman spectroscopy and mean vitrinite reflectance results indicate that the analysed Carboniferous strata reached maximum paleotemperatures from c. 110 to c. 265°C. The regional paleogeothermal gradient in the late Paleozoic was c. 80°C/km. The Variscan heating event presumably caused a major coalification process of organic matter. The Carboniferous–Permian magmatic activity must have contributed to high heat flow, adding to the effect of sedimentary burial on the thermal maturity.
    Źródło:
    Acta Geologica Polonica; 2020, 70, 3; 363--396
    0001-5709
    Pojawia się w:
    Acta Geologica Polonica
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermal history of the Carboniferous strata in the northern part of the Intra-Sudetic Basin (SW Poland): A combined Raman spectroscopy and organic petrography study
    Autorzy:
    Botor, Dariusz
    Toboła, Tomasz
    Waliczek, Marta
    Powiązania:
    https://bibliotekanauki.pl/articles/139342.pdf
    Data publikacji:
    2020
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Raman spectroscopy
    vitrinite reflectance
    dispersed organic matter
    coalification
    Lower Silesia Coal District
    Bohemian Massif
    spektroskopia Ramana
    refleksyjność witrynitu
    rozproszona materia organiczna
    uwęglenie
    Dolnośląskie Zagłębie Węglowe
    Masyw Czeski
    Opis:
    Raman spectroscopy and vitrinite reflectance measurements of dispersed organic matter from Carboniferous shales in boreholes in the northern part of the Intra-Sudetic Basin were used for thermal history reconstruction. Microscopic investigations have shown that the organic matter is dominated by the vitrinite maceral group. In analysed samples, organic matter shows a varied degree of thermal alteration determined by the mean random vitrinite reflectance (VRo) ranging from 0.72% to 3.80%. Mean apparent maximum vitrinite reflectance (R’max) values reached 4.98%. The full width at half maximum of D1 and G bands in Raman spectra are well-correlated with mean VRo and R’max. Thermal maturity in the boreholes shows a regular increase with depth. Geological data combined with Raman spectroscopy and mean vitrinite reflectance results indicate that the analysed Carboniferous strata reached maximum paleotemperatures from c. 110 to c. 265°C. The regional paleogeothermal gradient in the late Paleozoic was c. 80°C/km. The Variscan heating event presumably caused a major coalification process of organic matter. The Carboniferous–Permian magmatic activity must have contributed to high heat flow, adding to the effect of sedimentary burial on the thermal maturity.
    Źródło:
    Acta Geologica Polonica; 2020, 70, 3; 363-396
    0001-5709
    Pojawia się w:
    Acta Geologica Polonica
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
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