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Wyświetlanie 1-6 z 6
Tytuł:
Microstructure and Mechanical Characteristics of the Ternary SnZnAl Lead-Free Alloy
Autorzy:
Pietrzak, K.
Klasik, A.
Maj, M.
Sobczak, N.
Powiązania:
https://bibliotekanauki.pl/articles/380398.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lead free alloy
microstructure
mechanical properties
scanning electron microscopy
stop bezołowiowy
mikrostruktura
właściwości mechaniczne
mikroskop skaningowy
Opis:
The paper describes the studies of ternary SnZn9Al1.5 lead-free alloy from the viewpoint of its mechanical behavior as well as microstructure examined by the light and scanning electron microscopy. The authors focused their attention specifically on the fatigue parameters determined by the original modified low-cycle fatigue method (MLCF), which in a quick and economically justified way allows determination of a number of mechanical parameters based on the measurement data coming from one test sample only. The effect of the addition of 1.5% Al to the binary eutectic SnZn9 alloy on its microstructure and the obtained level of mechanical parameters was analyzed. The phases and intermetallic compounds occurring in the alloy were identified based on the chemical analysis carried out in micro-areas by the SEM/EDS technique. It was shown that the addition of 1.5% Al to the binary eutectic SnZn9 alloy resulted in a more favorable microstructure and consequently had a positive effect on the mechanical parameters of the alloy. Based on the conducted research, it was recommended to use a combinatorial method based on the phase quanta theory to quickly evaluate the microstructure and the original MLCF method to determine a number of mechanical parameters.
Źródło:
Archives of Foundry Engineering; 2018, 18, 3; 31-36
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Fatigue Life of the Binary Lead-free Alloys with High Zn Content
Autorzy:
Pietrzak, K.
Klasik, A.
Maj, M.
Sobczak, N.
Powiązania:
https://bibliotekanauki.pl/articles/382479.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lead free alloy
alloy microstructure
mechanical properties
stop bezołowiowy
mikrostruktura stopu
właściwości mechaniczne
Opis:
The results of studies presented in this article are an example of the research activity of the authors related to lead-free alloys. The studies covered binary SnZn90 and SnZn95 lead-free alloys, including their microstructure and complex mechanical characteristics. The microstructure was examined by both light microscopy (LM) and scanning electron microscopy (SEM). The identification of alloy chemical composition in micro-areas was performed by SEM/EDS method. As regards light microscopy, the assessment was of both qualitative and quantitative character. The determination of the geometrical parameters of microstructure was based on an original combinatorial method using phase quantum theory. Comprehensive characterization of mechanical behavior with a focus on fatigue life of alloys was performed by means of the original modified low cycle fatigue method (MLCF) adapted to the actually available test machine. The article discusses the fatigue life of binary SnZn90 and SnZn95 alloys in terms of their microstructure. Additionally, the benefits resulting from the use of the combinatorial method in microstructure examinations and MLCF test in the quick estimation of several mechanical parameters have been underlined.
Źródło:
Archives of Foundry Engineering; 2018, 18, 4; 65-70
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Comparative Studies of Microstructure and Fatigue Life of Selected Lead-free Alloys
Autorzy:
Pietrzak, K.
Klasik, A.
Maj, M.
Sobczak, N.
Wojciechowski, A.
Powiązania:
https://bibliotekanauki.pl/articles/379514.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lead free alloys
microstructure
mechanical properties
stopy bezołowiowe
mikrostruktura
właściwości mechaniczne
Opis:
Lead-free alloys containing various amounts of zinc (4.5%, 9%, 13%) and constant copper addition (1%) were discussed. The results of microstructure examinations carried out by light microscopy (qualitative and quantitative) and by SEM were presented. In the light microscopy, a combinatorial method was used for the quantitative evaluation of microstructure. In general, this method is based on the phase quanta theory according to which every microstructure can be treated as an arrangement of phases/structural components in the matrix material. Based on this method, selected geometrical parameters of the alloy microstructure were determined. SEM examinations were based on chemical analyses carried out in microregions by EDS technique. The aim of the analyses was to identify the intermetallic phases/compounds occurring in the examined alloys. In fatigue testing, a modified low cycle fatigue test method (MLCF) was used. Its undeniable advantage is the fact that each time, using one sample only, several mechanical parameters can be estimated. As a result of structure examinations, the effect of alloying elements on the formation of intermetallic phases and compounds identified in the examined lead-free alloys was determined. In turn, the results of mechanical tests showed the effect of intermetallic phases identified in the examined alloys on their fatigue life. Some concepts and advantages of the use of the combinatorial and MLCF methods in materials research were also presented.
Źródło:
Archives of Foundry Engineering; 2017, 17, 3; 111-116
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructural Aspects of Fatigue Parameters of Lead-Free Sn-Zn Solders with Various Zn Content
Autorzy:
Pietrzak, K.
Klasik, A.
Maj, M.
Wojciechowski, A.
Sobczak, N.
Powiązania:
https://bibliotekanauki.pl/articles/379846.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lutowanie bezołowiowe
mikrostruktura
właściwości mechaniczne
lead-free solders
microstructure
mechanical properties
Opis:
The study includes the results of research conducted on selected lead-free binary solder alloys designed for operation at high temperatures. The results of qualitative and quantitative metallographic examinations of SnZn alloys with various Zn content are presented. The quantitative microstructure analysis was carried out using a combinatorial method based on phase quanta theory, according to which any microstructure can be treated as an array of elements disposed in the matrix material. Fatigue tests were also performed using the capabilities of a modified version of the LCF method hereinafter referred to in short as MLCF, which is particularly useful in the estimation of mechanical parameters when there are difficulties in obtaining a large number of samples normally required for the LCF test. The fatigue life of alloys was analyzed in the context of their microstructure. It has been shown that the mechanical properties are improved with the Zn content increasing in the alloy. However, the best properties were obtained in the alloy with a chemical composition close to the eutectic system, when the Zn-rich precipitates showed the most preferred morphological characteristics. At higher content of Zn, a strong structural notch was formed in the alloy as a consequence of the formation in the microstructure of a large amount of the needle-like Zn-rich precipitates deteriorating the mechanical characteristics. Thus, the results obtained during previous own studies, which in the field of mechanical testing were based on static tensile test only, have been confirmed. It is interesting to note that during fatigue testing, both significant strengthening and weakening of the examined material can be expected. The results of fatigue tests performed on SnZn alloys have proved that in this particular case the material was softened.
Źródło:
Archives of Foundry Engineering; 2017, 17, 1; 131-136
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructural Aspects of Fatigue Life of Sn-Zn Lead-free Solders with 1% of Ag Addition
Autorzy:
Pietrzak, K.
Klasik, A.
Maj, M.
Sobczak, N.
Wojciechowski, A.
Powiązania:
https://bibliotekanauki.pl/articles/382245.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lead-free solders
microstructure
mechanical properties
lutowanie bezołowiowe
mikrostruktura
właściwości mechaniczne
Opis:
The article presents the study results of Sn-Zn lead-free solders with the various Zn content. The results concern the hypoeutectic, eutectic and hypereutectic alloys containing respectively 4.5% Zn, 9% Zn and 13.5% Zn. Moreover, these alloys contain the constant Ag (1%) addition. The aim of the study was to determine the microstructural conditionings of their fatigue life. In particular it was focused on answer the question what meaning can be assigned to the Ag addition in the chemical composition of binary Sn-Zn alloys. The research includes a qualitative and quantitative assessments of the alloy microstructures, that have been carried out in the field of light microscopy (LM). In order to determine some geometrical parameters of the microstructure of alloys the combinatorial method based on the phase quanta theory was applied. Moreover, for the identification necessities the chemical analyses in the micro-areas by SEM/EDS technics were also performed. Based on the SEM/EDS results the phases and intermetallic compounds existing in the examined lead-free solders were identified. The mechanical characteristics were determined by means of the modified low cycle test (MLCF). Based on this method and on the results obtained every time from only one sample the dozen of essential mechanical parameters were evaluated. The research results were the basis of analyzes concerning the effects of microstructural geometrical parameters of lead-free alloys studied on their fatigue life at ambient temperature.
Źródło:
Archives of Foundry Engineering; 2018, 18, 1; 87-92
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Diacryloyl Derivative of Mannitol - Synthesis and Application in Gelcasting of Al2O3-ZrO2 Composites
Autorzy:
Wiecinska, P.
Kubica, D.
Pietrzak, E.
Sakowicz, A.
Prokurat, N.
Antosik, A.
Powiązania:
https://bibliotekanauki.pl/articles/356943.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gelcasting
ZTA
composites
zirconia
mannitol
Opis:
The aim of research was the elaboration of the synthesis of new organic monomer applicable in gelcasting. The substance named 3,4-di-acryloyl-D-mannitol which contains two acryloyl groups and four hydroxyl groups in its molecule has been synthesized. The monomer has been then applied in the preparation of Al2O3-ZrO2 composites by gelcasting and subsequent sintering. Rheological properties of ceramic suspensions have been examined, as well as the properties of green and sintered bodies. SEM observations allowed to determine the distribution of zirconia grains in alumina matrix. Density, Vickers hardness and fracture toughness of ZTA composites have been measured. The new monomer, that is diacryloyl derivative of mannitol, is less sensitive to the oxygen inhibition than commonly used in gelcasting and commercially available 2-hydroxyethyl acrylate.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 859-865
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-6 z 6

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