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Tytuł:
Valorization of Cobalt from Waste LIB Cathode through Cobalt Oxalate and Cobalt Oxide Synthesis by Leaching-Solvent Extract-Precipitation Stripping
Autorzy:
Swain, B.
Lee, J.-C.
Lee, C.-G.
Powiązania:
https://bibliotekanauki.pl/articles/352333.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
valorization of cobalt
cobalt oxide powder
rod-shaped cobalt oxalate
precipitation stripping
Opis:
An ecoefficient, economical and sustainable valorization process for the synthesis of Co3O4 from waste lithium-ion battery (LIB) by leaching-solvent extract-scrubbing-precipitation stripping route has been developed. Through an optimization, the waste LIB cathode was leached using 2000 mole/m3 of H2SO4 and 5 Vol. % of the H2O2 at a pulp density of 100 kg/m3 under leaching time 60 minutes and temperature 75°C. From the separated leach liquor, cobalt was purified by saponified Cyanex 272. From cobalt, loaded Cyanex 272 impurities were scrubbed and the CoC2O4·2H2O was recovered through precipitation stripping. Finally, the precipitate was calcined to synthesize Co3O4, which is a precursor for LIB cathode materials manufacturing. From TGA-DTA, followed by XRD analysis it was confirmed that at 200°C the CoC2O4·2H2O can be converted to anhydrous CoC2O4 and at 350°C the anhydrous can be converted to Co3O4 and at 1100°C the Co3O4 can be converted to CoO. Through reported route waste LIB can back to LIB manufacturing process through a versatile and flexible industrial approach.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1037-1042
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Rapid Synthesis of Gold Nano-Particles Using Pulse Waved Potential in a Non-Aqueous Electrolyte
Autorzy:
Jang, J. G.
Lee, J.-O.
Lee, C. K.
Powiązania:
https://bibliotekanauki.pl/articles/352529.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gold
nanoparticle
nonaqueous electrolyte
pulse wave
catalyst
Opis:
Rapid synthesis of gold nanoparticles (AuNPs) by pulsed electrodeposition was investigated in the non-aqueous electrolyte, 1-ethyl-3-methyl-imidazoliumbis(trifluoro- methanesulfonyl)imide ([EMIM]TFSI) with gold trichloride (AuCl3). To aid the dissolution of AuCl3, 1-ethyl-3-methyl-imidazolium chloride ([EMIM]Cl) was used as a supporting electrolyte in [EMIM]TFSI. Cyclicvoltammetry experiments revealed a cathodic reaction corresponding to the reduction of gold at −0.4 V vs. Pt-QRE. To confirmthe electrodeposition process, potentiostatic electrodeposition of gold in the non-aqueous electrolyte was conducted at −0.4 V for 1 h at room temperature. To synthesize AuNPs, pulsed electrodeposition was conducted with controlled duty factor, pulse duration, and overpotential. The composition, particle-size distribution, and morphology of the AuNPs were confirmed by field-emission scanning electron microscopy (FE-SEM), energy-dispersive spectroscopy (EDS), and transmission electron microscopy (TEM). The electrodeposited AuNPs were uniformly distributed on the platinum electrode surface without any impurities arising from the non-aqueous electrolyte. The size distribution of AuNPs could be also controlled by the electrodeposition conditions.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1389-1392
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Allometric scaling of marbofloxacin pharmacokinetics: a retrospective analysis
Autorzy:
Yohannes, S.
Hossain, M.A.
Kim, J.Y.
Lee, S.J.
Kwak, D.M.
Suh, J.W.
Park, S.C.
Powiązania:
https://bibliotekanauki.pl/articles/31939.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Opis:
The association between physiologically dependent pharmacokinetic parameters (CLB, T1/2β, Vdss) of marbofloxacin and body weight was studied in eight animal species based on allometric equation Y = aWb, where ‘Y’ is the pharmacokinetic parameter, ‘W’ is body weight, ‘a’ is allometric coefficient (intercept) and ‘b’ is the exponent that describes relation between pharmacokinetic parameter and body weight. The body clearance of marbofloxacin has shown significant (P<0.0001) relation with size (Bwt) in various animal species. However, half-life and volume of distribution were not in association with body weight. Although half-life and volume of distribution were not in a good correlation with body weight, statistically significant association between the body clearance and body weight suggests validity of allometric scaling for predicting pharmacokinetic parameters of marbofloxacin in animal species that have not been studied yet. However further study considering large sample size and other parameters influencing pharmacokinetics of marbofloxacin is recommended.
Źródło:
Polish Journal of Veterinary Sciences; 2014, 17, 1
1505-1773
Pojawia się w:
Polish Journal of Veterinary Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
Autorzy:
Jo, Y. J.
Yoon, Y. H.
Kim, Y. H.
Chang, S. Y.
Kim, J. Y.
Lee, Y. K.
Van Tyne, C. J.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/356790.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
implant
porous
sintering
X-ray photoelectron spectroscopy (XPS)
Opis:
A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
High-temperature Oxidation Behavior and Kinetics of Forged 12Cr-MoVW Steel
Autorzy:
Kim, Y. H.
Oak, J.-J.
Bae, K.-C.
Lee, W-J.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/351450.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ferritic/martensitic stainless steels
forging
oxidation kinetics
oxide layer
Opis:
The oxidation kinetics of forged 12Cr-MoVW steel was investigated in an air (N2+O2) atmosphere at 873-1073 K (Δ50 K) using thermogravimetric analysis. The oxidized samples were characterized using X-ray diffraction, and the surface and cross-sectional morphologies were examined using scanning electron microscopy coupled with energy-dispersive X-ray spectroscopy. The forged 12Cr-MoVW steel samples exhibited parabolic behavior and a low oxidation rate compared with their as-cast counterparts. A protective oxide layer was uniformly formed at relatively low temperature (≤973 K) for the forged samples, which thus exhibited better oxidation resistance than the as-cast ones. These oxides are considered solid-solution compounds such as (Fe, Cr)2O3.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1099-1104
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A stepwise ISO-based TQM implementation approach using ISO 9001:2015
Autorzy:
Chen, C.-K.
Anchecta, K.
Lee, J. -D.
Dahlgaard, J. J.
Powiązania:
https://bibliotekanauki.pl/articles/407353.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Total Quality Management
TQM
ISO QMS
ISO 9000
ISO 9001:2015
international standard
Opis:
The lack of an implementation roadmap always deters enterprises from choosing Total Quality Management (TQM) as its major management approach. This paper proposes a stepwise ISO-based TQM implementation approach which is based on the notion of the new threedimensional overall business excellence framework developed by Dahlgaard et al. [1]. The proposed approach consists of nine steps comprising three categories: “TQM faith building”, “TQM tools and techniques learning”, and “system development”. The steps in each of the three categories are arranged to span across the proposed nine-step approach. The ISO 9001:2015 standard is used as a case study to demonstrate the proposed approach. The ideas and benefits of the proposed approach are further discussed in relation to this illustration.
Źródło:
Management and Production Engineering Review; 2016, 7, 4; 65-75
2080-8208
2082-1344
Pojawia się w:
Management and Production Engineering Review
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphology Change Of Si Deposit In Molten Salt Electrorefining
Zmiana morfologii osadu Si podczas elektrorafinacji w stopionych solach
Autorzy:
Ryu, H. Y.
Kwon, S. C.
Han, M. H.
An, Y. S.
Lee, J. S.
Lee, J. H.
Powiązania:
https://bibliotekanauki.pl/articles/354346.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
molten salt
silicon
morphology
electrorefining
current density
sól stopiona
krzem
morfologia
elektrorafinacja
gęstość prądu
Opis:
The effects of processing parameters on the morphology change in a Si deposit recovered by means of molten salt electrorefining are evaluated using electrochemical techniques such as cyclic voltammetry and chronopotentiometry at 800°C. It was found that concentration of K2SiF6 and current density were important parameters in determining deposit size. Higher concentrations of K2SiF6 were effective in coarsening the silicon deposit and decreasing the cell potential. Silicon nanofiber was recovered at 5 wt% of K2SiF6 whereas dense particles were prepared at 30 and 50 wt% of K2SiF6. The morphology of the Si deposit was determined by the concentration of Si in the electrolyte which is related to the formation of crystal and growth of Si. The formation mechanism of the Si deposit was interpreted by using high resolution TEM as well as electrochemical properties.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1491-1497
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Study On Dispersion Stability Of Nickel Nanoparticles Synthesized By Wire Explosion In Liquid Media
Badanie stabilności dyspersji nanocząstek niklu wytworzonych metodą WEP w ciekłym medium
Autorzy:
Kim, C. K.
Lee, G.-J.
Lee, M. K.
Rhee, C. K.
Powiązania:
https://bibliotekanauki.pl/articles/356909.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nickel nanofluid
pulsed wire evaporation
surfactant
zeta potential
dispersion stability
nanocząstka niklu
środek powierzchniowo czynny
stabilność dyspersji
potencjał zeta
dyspersja
Opis:
In this study, nickel nanoparticles were synthesized in ethanol using portable pulsed wire evaporation, which is a one-step physical method. From transmission electron microscopy images, it was found that the Ni nanoparticles exhibited a spherical shape with an average diameter of 7.3 nm. To prevent aggregation of the nickel nanoparticles, a polymer surfactant was added into the ethanol before the synthesis of nickel nanoparticles, and adsorbed on the freshly synthesized nickel nanoparticles during the wire explosion. The dispersion stability of the prepared nickel nanofluids was investigated by zeta-potential analyzer and Turbiscan optical analyzer. As a result, the optimum concentration of polymer surfactant to be added was suggested for the maximized dispersion stability of the nickel nanofluids.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1379-1382
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization Of The Graded Microstructure In Powder Sintered Porous Titanium
Charakterystyka gradientowej mikrostruktury porowatego tytanu spiekanego z proszku
Autorzy:
Oak, J.-J.
Bang, J. I.
Bae, K.-C.
Kim, Y. H.
Lee, Y. C.
Chun, H. H.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/356239.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
powder metallurgy
porous structure
sintering
biomaterial
tytan
metalurgia proszków
struktura porowata
spiekanie
biomateriał
Opis:
The proposed sintering process produce porosity and functional graded microstructure in the sinterd titanium powders. Titanium powders with different micro sizes were sintered at the proposed temperature region at 1200 and 1300°C for 2h. The apatite-forming on the graded microstructure is observed by immersion test in Hanks balanced salt soluion at 37°C. Sintering condition of titanium powders is estimated by thermogravitmetry-differential thermal analysis (TG-DTA). The synthersied surface structures and apatite-forming ability were characterized by a field emission scanning electron microscopy (FE-SEM) observation and energy dispersive X-ray spectroscopy (EDS) analysis. As results, these graded microstructure of sintered porous titanium powders reveals apatite-forming ability as osseointegration by calcification in Hanks balanced salt soluion(HBSS) at 37°C.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1265-1269
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Properties and Mechanical Behavior of the 2 Step-Reinforced Al-Si/SiCp Metal Matrix Composite by Titanium-Fiber
Autorzy:
Oak, J.-J.
Lee, Y. C.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/356010.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metal matrix composite
sintering
Ti fiber
mechanical properties
diffusion
Opis:
In this study, the newly designed Al-9Si/SiC particles (SiCp) + Ti-fiber (2step-reinforced Al-9Si alloy matrix) metal matrix composites (MMCs) were fabricated by hot-pressing sintering at 560°C. 2step-reinforced Al-based MMCs were characterized by thermal shrinkage, phase transition, microstructure and tensile strength. The addition of Ti-fiber reduced thermal shrinkage was caused by temperature difference in sintering process as well as enhanced assistance for tensile strength and plastic deformation at room temperature. Experimental results reveal that the 2step-reinforcment sintering by ceramic and metal has a significant effect to increase interface bonding in boundary of each component material and the improved mechanical properties were due to the influence of interfacial product by diffusion. Tensile strength and elongation at room temperature by 2step-reinforcement were improved in 19.5% and 26.2% more than those of Al-9Si/SiCp, respectively. Especially, it reveals that diffusion direction may be varied by sintering methods at low temperature in this study.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1089-1097
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The effect of patterns on image-based modelling of texture-less objects
Autorzy:
Hafeez, J.
Jeon, H.-J.
Hamacher, A.
Kwon, S.-C.
Lee, S.-H.
Powiązania:
https://bibliotekanauki.pl/articles/221814.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
structure-from-motion
feature detection
patterns analysis
3D reconstruction
surface comparison
Opis:
The task of generating fast and accurate three-dimensional (3D) models of objects or scenes through a sequence of non-calibrated images is an active field of research. The recent development in algorithm optimization has resulted in many automatic solutions that can provide an accurate 3D model from texture-full objects. Structure-from-motion (SfM) is an image-based method that uses discriminative point-based feature identifier, such as SIFT, to locate feature points in the images. This method faces difficulties when presented with the objects made of homogenous or texture-less surfaces. To reconstruct such surfaces a well-known technique is to apply an artificial variety by covering the surface with a random texture pattern prior to the image capturing process. In this work, we designed three series of image patterns which are tested based on the contrast and density ratio which increases from the first to the last pattern within the same series. The performance of the patterns is evaluated by reconstructing the surface of a texture-less object and comparing it with the true data. Using the best-found patterns from the experiments, a 3D model of a Moai statue is reconstructed. The experimental results demonstrate that the density and structure of a pattern highly affects the quality of the reconstruction.
Źródło:
Metrology and Measurement Systems; 2018, 25, 4; 755-767
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Surfactant Addition on Bi2Te3 Nanostructures Synthesized by Hydrothermal Method
Autorzy:
Dharmaiah, P.
Lee, C. H.
Madavali, B.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/351609.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
bismuth telluride
hydrothermal synthesis
spark plasma sintering
thermoelectric materials
X-ray diffraction
Opis:
In the present work, we have prepared Bi2Te3 nanostructures with different morphologies such as nano-spherical, nanoplates and nanoflakes obtained using various surfactant additions (EG, PVP, and EDTA) by a hydrothermal method. The shape of the nanoparticles can be controlled by addition of surfactants. The samples were characterized by x-ray diffraction (XRD) and scanning electron microscopy (SEM). It is found that the minority BiOCl phase disappears after maintained pH at 10 with EG as surfactant. SEM bulk microstructure reveals that the sample consists of fine and coarse grains. Temperature dependence of thermoelectric properties of the nanostructured bulk sample was investigated in the range of 300-450K. The presence of nanograins in the bulk sample exhibits a reduction of thermal conductivity and less effect on electrical conductivity. As a result, a figure of merit of the sintered bulk sample reached 0.2 at 400 K. A maximum micro Vickers hardness of 102 Hv was obtained for the nanostructured sample, which was higher than the other reported results.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1005-1010
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Recovery Of Electrodic Powder From Spent Lithium Ion Batteries (LIBs)
Odzysk proszku elektrodowego z zużytych akumulatorów litowo-jonowych
Autorzy:
Shin, S. M.
Jung, G. J.
Lee, W-J.
Kang, C. Y.
Wang, J. P.
Powiązania:
https://bibliotekanauki.pl/articles/354084.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lithium ion battery
electrodic powder
cobalt
lithium
thermal treatment
bateria litowo-jonowa
proszek elektrodowy
kobalt
lit
obróbka termiczna
Opis:
This study was focused on recycling process newly proposed to recover electrodic powder enriched in cobalt (Co) and lithium (Li) from spent lithium ion battery. In addition, this new process was designed to prevent explosion of batteries during thermal treatment under inert atmosphere. Spent lithium ion batteries (LIBs) were heated over the range of 300°C to 600°C for 2 hours and each component was completely separated inside reactor after experiment. Electrodic powder was successfully recovered from bulk components containing several pieces of metals through sieving operation. The electrodic powder obtained was examined by X-ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDS), and atomic absorption spectroscopy (AA) and furthermore image of the powder was taken by scanning electron microscopy (SEM). It was finally found that cobalt and lithium were mainly recovered to about 49 wt.% and 4 wt.% in electrodic powder, respectively.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1145-1149
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Trace Elements (Co, Cr) on the Microstructure and Physical Properties of Al-Si-Cu-Mg-Fe Extruded Alloy
Autorzy:
Ahn, S. S.
Sharief, P.
Lee, C. H.
Son, H. T.
Kim, Y. H.
Kim, Y. C.
Hong, S.
Hong, S. J.
Powiązania:
https://bibliotekanauki.pl/articles/352787.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Al-Si alloy
microstructure
extrusion
coefficient of thermal expansion
trace elements
Opis:
Trace elements Co, Cr were added to investigate their influence on the microstructure and physical properties of Al-Si extruded alloy. The Co, Cr elements were randomly distributed in the matrix, forms intermetallic phase and their existence wereconfirmed by XRD, EDS and SEM analysis. With addition of trace elements, the microstructure was modified, Si particle size was reduced and the growth rate of β-(Al5 FeSi) phase limited. Compared to parent alloy, hardness and tensile strength were enhanced while the linear coefficient of thermal expansion (CTE) was significantly reduced by 42.4% and 16.05% with Co and Cr addition respectively. It is considered that the low CTE occurs with addition of Co was due to the formation of intermetallic compound having low coefficient of thermal expansion. The results suggested that Co acts as an effective element in improving the mechanical properties of Al-Si alloy.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 857-862
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Quantitative Analysis of Cryomilled Nanocrystalline Ti-6Al-4V Alloy Powder by X-Ray Diffraction
Autorzy:
Oh, M.
Yu, H. K.
Lee, J.-H.
Oh, M. C.
Jung, S.-H.
Ahn, B.
Powiązania:
https://bibliotekanauki.pl/articles/356265.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nanocrystalline
cryomilling
Ti alloy
X-ray diffraction
size-strain plot method
Opis:
A nanocrystalline Ti alloy powder was fabricated using cryomilling. The grain size and lattice strain evolution during cryomilling were quantitatively analyzed using X-ray diffraction (XRD) based on the Scherrer equation, Williamson-Hall (W-H) plotting method, and size-strain (S-S) method assuming uniform deformation. Other physical parameters including stress and strain have been calculated. The average crystallite size and the lattice strain evaluated from XRD analysis are in good agreement with the result of transmission electron microscopy (TEM).
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1439-1442
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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