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    Wyświetlanie 1-15 z 15
    Tytuł:
    A novel method to extract vanadium from vanadium-bearing steel slag using sodium carbonate solution
    Autorzy:
    Gao, M.
    Xue, X.
    Li, L.
    Yang, H.
    Bai, R.
    Wang, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/109859.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    leaching
    kinetics
    vanadium
    vanadium-bearing steel slag
    Opis:
    A new method using sodium carbonate solution to treat a vanadium-bearing steel slag is proposed. The effects of the particle size, solid-to-liquid ratio, initial concentration of sodium carbonate solution, leaching temperature and stirring speed on the leaching rate of vanadium were investigated. The leaching kinetics of vanadium from the vanadium-bearing steel slag was studied, which indicated that the leaching rate was controlled by the step of diffusion through the solid layer around the unreacted core. The apparent activation energy for the process was 13.75 kJ/mol. By using this process, vanadium could be extracted effectively with the leaching rate of more than 80%.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 3; 911-921
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Application of Pyrolox sorbent for vanadium(V) ions removal
    Autorzy:
    Wójcik, Grzegorz
    Hubicki, Zbigniew
    Powiązania:
    https://bibliotekanauki.pl/articles/2146947.pdf
    Data publikacji:
    2022
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    vanadium(V)
    kinetics
    removal
    sorption
    Pyrolox
    Opis:
    The sorption of vanadium(V) ions from acidic solutions using the Pyrolox sorbent was studied at varying ions concentrations, pH, contact time and temperature. The investigated ions were determined by means of graphite-furnace atomic absorption spectrometry (GF-AAS). The sorption capacity of vanadium(V) ions was examined in the pH range 2-10. The adsorption capacities of vanadium(V) ions depend on the pH values. Therefore, the initial pH 2 of vanadium(V) results in the highest adsorption capacities. The sorption vanadium(V) kinetics was investigated. The experimental data were analyzed using the pseudo-first-order, pseudo-second-order forms, Elovich, and intra-particle diffusion models. The kinetics of vanadium(V) sorption is described by the pseudo-first-order in the best way. The results indicate the endothermic process of V(V) ions sorption. The presented results of vanadium ions recovery from the solutions obtained as a result of spent catalysts leaching indicate the possibility of vanadium recovery.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2022, 58, 2; art. no. 147974
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Pre-concentration of vanadium-bearing mica from stone coal by roasting-flotation
    Autorzy:
    Tang, J.
    Zhang, Y.
    Bao, S.
    Liu, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/109373.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    roasting
    flotation
    vanadium bearing mica
    stone coal
    Opis:
    In China, stone coal is an important source of vanadium. The use of roasting–floatation for the pre-concentration of vanadium bearing mica from vanadium bearing stone coal was investigated based on its mineralogical characteristics. The results showed that the vanadium occurred in mica minerals and the main gangue minerals were coal, calcite, and quartz. The pre-concentration process comprises three key steps: roasting, desliming, and flotation. The coal was completely removed by roasting at 700 °C for an hour. Slime was concentrated and the subsequent flotation pulp was improved by desliming. Calcite was removed by reverse flotation and mica was concentrated by positive floatation. During the process, the grade of V2O5 was increased from 0.71% to 1.14%, and 46.18% of the tailings were rejected. The leaching rate of vanadium was increased from 30.49% of raw ore to 69.15% of the concentrate which was an increase of about 40% at the same leaching process. This technique may promote the efficient utilization of stone coal resources.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2017, 53, 1; 402-412
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Feasibility study on preparation of magnesium titanate in carbonthermic reduction of vanadium titanomagnetite concentrates
    Autorzy:
    Chen, Chao
    Sun, Ti-Chang
    Kou, Jue
    Wang, Xiao-Ping
    Zhao, Yong-Qiang
    Powiązania:
    https://bibliotekanauki.pl/articles/110181.pdf
    Data publikacji:
    2019
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    vanadium titanomagnetite
    carbonthermic reduction
    magnesium titanate
    formation mechanism
    Opis:
    Effect of temperature and Mg:Ti ratio on phase composition and microstructure of reduced pellets was investigated to verify the feasibility of preparation of magnesium titanate by adding MgO in carbonthermic reduction of the vanadium titanomagnetite concentrates (VTC). Thermodynamic analysis results showed that magnesium titanate is more easily generated than FeTi2O5 or TiO2 by the reaction of FeTiO3 and MgO under the reductive atmosphere, which was confirmed by the discovery of magnesium titanate at roast experiment. It was found that the optimum conditions for reduction of VTC pellets were temperature of 1250 ºC and Mg:Ti ratio of 2, and the main phases of reduction product were metallic Fe and magnesium titanate (Mg2TiO4). However, trace iron impurities in Mg2TiO4 particles were found by energy-dispersive spectroscopy (EDS), so further purification is required.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2019, 55, 2; 417-425
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Simultaneous extraction of vanadium and chromium from vanadium slag using low-pressure liquid phase oxidation method
    Autorzy:
    Xia, J.-P.
    Zheng, S.-L.
    Wang, S.-N.
    Liu, B.
    Zou, X.
    Powiązania:
    https://bibliotekanauki.pl/articles/110818.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    vanadium slag
    low pressure leaching
    liquid phase oxidation
    kinetics
    Opis:
    A low-pressure liquid oxidation method was proposed and proven to be effective to extract vanadium and chromium simultaneously from the vanadium slag in concentrated NaOH aqueous solutions. The effect of temperature, NaOH mass concentration, liquid-to-solid mass ratio, stirring speed and pressure on the extraction of vanadium and chromium in NaOH aqueous solutions were systematically investigated. Under the optimal reaction conditions (temperature of 473 K, liquid-to-solid mass ratio of 6:1, stirring speed of 700 rpm, NaOH mass concentration of 50%, pressure of 1 MPa and reaction time of 180 min), the vanadium and chromium recovery reached 95% and 90%, respectively. It was found that the reaction temperature and NaOH concentration were important factors for the extraction of vanadium and chromium. The kinetics of the decomposition of vanadium slag in concentrated NaOH aqueous under low pressure was analyzed using the shrinking core model, and the results indicated that the extraction of vanadium and chromium were both governed by the internal diffusion step, with apparent activation energies calculated to be 26.22 and 32.79 kJ/mol, respectively.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 2; 609-619
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Selective extraction of vanadium from vanadium-titanium magnetite concentrates by non-salt roasting of pellets-H2SO4 leaching process
    Autorzy:
    Luo, Yi
    Che, Xiaokui
    Wang, Haixia
    Zheng, Qi
    Wang, Lei
    Powiązania:
    https://bibliotekanauki.pl/articles/1445902.pdf
    Data publikacji:
    2021
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    vanadium-titanium magnetite
    pellets
    selective extraction
    sulfuric acid leaching
    Opis:
    In this work, a novel process of pellet non-salt roasting and H2SO4 leaching was proposed for the selective extraction of vanadium from vanadium–titanium magnetite concentrate. Vanadium can be leached but the iron impurity was maintained in the pellets. Moreover, the leached pellets can meet the quality requirements of the iron-making process after secondary roasting, realizing comprehensive utilization. The maximal vanadium leaching efficiency was up to 60.3%, whereas 0.17% of the iron impurity was leached. The optimum conditions of pellet roasting and leaching were obtained by single-factor experiments. The X-ray diffraction and scanning electron microscopy–energy disperse X-ray spectrometry analyses showed that the vanadium iron spinel can be oxidized and decomposed into Fe2O3 and vanadate during the roasting process. Given that dilute sulfuric acid can react with vanadate without reacting with Fe2O3 in the leaching process, selective vanadium extraction was realized. This work provides new insights into the industrial production of vanadium–titanium magnetite concentrate involving the direct extraction of vanadium.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2021, 57, 4; 36-47
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of sodium sulfide waste water recycling on the separation of chalcopyrite and molybdenite
    Autorzy:
    Wu, D.
    Peng, H.
    Abdalla, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/110657.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    vanadium slag
    low pressure leaching
    liquid phase oxidation
    kinetics
    Opis:
    The effect of sodium sulfide waste water recycling on the separation of chalcopyrite and molybdenite was investigated in this work. The waste water, which was separated from the slurry after selective flotation, was recycled in the flotation system. This operation significantly improved the subsequent flotation of chalcopyrite and saved the reagent. The results showed that the depression efficiency of sodium sulfide gradually disappeared in the recycling tests due to the consumption. The consumption of sodium sulfide in the separation was not only caused by the adsorption on mineral surfaces but also resulted from the precipitation of metal ions which released from minerals. These effects decreased the solution reducibility and the adsorption of hydrosulfide ions, finally resulting in the less depression for chalcopyrite flotation. After adding a certain amount of sodium sulfide to the recycling, the depression of chalcopyrite performed well and the pulp potential maintained at a relatively lower level. Moreover, the pulp potential was an available parameter to control the flotation separation of chalcopyrite and molybdenite, which made the method easily applied to industry.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 3; 629-638
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Investigation of quartz flotation from decarburized vanadium bearing coal
    Autorzy:
    Ren, L.
    Zhang, Y.
    Bian, Y.
    Liu, X.
    Liu, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/110937.pdf
    Data publikacji:
    2015
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    mica
    vanadium-bearing coal
    flotation
    quartz
    ion dissolution
    calcium ion
    Opis:
    Ether diamine (Fm 2835-2L) was used as a collector for flotation of quartz. It allows flotation of quartz from mica and calcite. The adsorption mechanism of Fm 2835-2L on quartz was investigated by flotation tests, zeta-potential measurements and infra-red (FTIR) spectra measurements. Results show that Fm 2835-2L adsorbs on the quartz surface in physical adsorption with no new products, changing its zeta potentials, and increasing its hydrophobicity. The effect of calcium ions on flotation of quartz was investigated by flotation tests and zeta-potential measurements. Results show that under neutral or weakly acidic conditions calcium cation can adsorb onto the surfaces of quartz, increase the zeta potential of quartz particles, which in turn causes weaker aggregation of quartz particles and lower flotation recovery of quartz. Under the alkaline conditions the hydrolytic components of calcium are also adsorbed on the quartz surface and increase the zeta potential of quartz particles, which causes stronger aggregation of quartz particles and higher flotation recovery of quartz. However, the hydrolytic components such as CaOH+, Ca(OH)2(aq) and Ca(OH)2(s) were not formed in significant amounts in the best flotation tests.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2015, 51, 2; 755-767
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Photocatalytic properties of Ti–V oxides thin films
    Autorzy:
    Domaradzki, J
    Mazur, M
    Sieradzka, K
    Wojcieszak, D
    Adamiak, B
    Powiązania:
    https://bibliotekanauki.pl/articles/174210.pdf
    Data publikacji:
    2013
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    titanium dioxide (TiO2)
    thin films
    magnetron sputtering
    vanadium
    photocatalysis
    Opis:
    In this work, the photocatalytic properties of Ti–V oxides thin films with 19 and 23 at.% of vanadium addition have been outlined. The films were deposited by the high energy reactive magnetron sputtering method. X-ray photoelectron spectroscopy measurements were done in order to determine the chemical composition and binding energy of the elements on the samples surface. Additionally, based on wettability measurements, the water contact angles were evaluated and were equal to ca. 94° and 55° for thin films with 19 and 23 at.% of V, respectively. This testifies about hydrophilic and hydrophobic properties, respectively. Photoactivity of thin films was determined by percent decomposition of phenol for 5 hours during UV–vis radiation exposure. The highest photocatalytic activity of 6.2%/cm2 was obtained for thin films with 19 at.% of V. It has been found that an increase in V amount in Ti–V oxides thin films to 23 at.% results in lowered to 3%/cm2 photocatalytic activity.
    Źródło:
    Optica Applicata; 2013, 43, 1; 153-162
    0078-5466
    1899-7015
    Pojawia się w:
    Optica Applicata
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of direct reduction time of vanadium titanomagnetite concentrate on the preparation and photocatalytic performance of calcium titanate
    Autorzy:
    Li, Xiaohui
    Kou, Jue
    Sun, Tichang
    Wu, Shichao
    Tian, Yuechao
    Powiązania:
    https://bibliotekanauki.pl/articles/1449028.pdf
    Data publikacji:
    2021
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    vanadium titanomagnetite concentrate
    calcium titanate
    direction reduction
    metallic iron
    photocatalytic performance
    Opis:
    Effects of direct reduction time of vanadium titanomagnetite concentrate (VTCE) on the preparation and photocatalytic performance of calcium titanate were investigated in this study. It was found that extending the reduction time could not only promote the formation of calcium titanate, but also facilitate the reduction of iron minerals in the reduction products. The optimum reduction time was 180min under the conditions of $CaCO_3$ dosage of 18wt%, reduction temperature of 1400℃ and lignite dosage of 70wt%. The reduced iron (Fe grade of 90.95wt%, Fe recovery of 92.21wt%) and calcium titanate were obtained via grinding-magnetic separation. Moreover, calcium titanate prepared via the direct reduction method could be used as a photocatalyst, where the degradation degree of methylene blue increased from 25.13% to 60.14% with the addition of calcium titanate. Furthermore, Langmuir Hinshelwood fitting results indicated that the degradation of methylene blue by the calcium titanate prepared under different reduction times conformed to first-order reaction kinetics, where the photocatalytic degradation rate of methylene blue was noted to be the highest for a reduction time of 180 min.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2021, 57, 1; 75-86
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Recovery of Fe and V via selective reduction–magnetic separation of vanadium-titanium magnetite concentrate
    Autorzy:
    Liu, Liwei
    Li, Guofeng
    Zhao, Libing
    Li, Jinpeng
    Li, Yanfeng
    Powiązania:
    https://bibliotekanauki.pl/articles/2146847.pdf
    Data publikacji:
    2022
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    vanadium-titanium magnetite concentrate
    selective reduction
    magnetic separation
    Fe separation
    V separation
    Opis:
    With the aim of separating Fe and V, a vanadium-titanium magnetite concentrate was selectively reduced, followed by magnetic separation. The processes accompanying reduction of the vanadium-titanium magnetite concentrate were investigated using thermodynamic simulation, experiments, scanning electron microscopy, and electron probe microanalysis. Appropriate reduction conditions and controlling the amount of CaCO3 promoted the reduction of Fe-containing minerals to metallic Fe. V was released from magnetite, ilmenite, and titanomagnetite, and was inhibited to reduce to metallic V, leading to V enrichment in the non-magnetic products in the form of oxides. Moreover, the Fe particles wrapped the slag phase when the amount of CaCO3 exceeded 8%, which is unfavourable for the magnetic separation of Fe and V. Magnetic products with an Fe content of 87.19%, Fe recovery of 82.62%, V content of 0.09% and non-magnetic products with a V content of 1.00% and a V recovery of 85.49% were obtained when the vanadium-titanium magnetite concentrate was reduced for 100 min at 1623 K with a C/O molar ratio of 2.5 and 8% CaCO3, followed by separating at a magnetic field strength of 85 mT.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2022, 58, 1; 50--62
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A novel method to extract vanadium from high-grade vanadium slag: non-salt roasting and alkaline leaching
    Autorzy:
    Liu, B.
    Meng, L.
    Zheng, S.
    Li, M.
    Wang, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/110480.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    high-grade vanadium slag
    cleaner production
    non-salt roasting
    alkaline leaching
    mechanisms
    Opis:
    A new method using non-salt roasting-alkaline leaching to treat vanadium slag was proposed in this study. The V(III) in vanadium slag is oxidized to V(V) by roasting and the latter can be effectively leached out as vanadate by alkaline leaching. This method possesses distinct advantage of being able to treat high-grade vanadium slag. For the South Africa high-grade vanadium slag, the maximum vanadium recovery of 98% was achieved when the reaction conditions were roasting temperature of 850 °C, roasting time of 2 h, alkali concentration of 30 wt.%, leaching temperature of 210 °C, and leaching time of 2 h. The roasting and leaching mechanisms have been well elucidated based on the XRD and SEM analysis results. The phases transitions of vanadium slag were clearly presented. This work has laid the foundation for the industrial application of non-salt roasting-alkaline leaching and provided new insights into effective extraction of high-grade vanadium slag.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 3; 657-667
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Theoretical investigation of vanadium oxide film with surface microstructure
    Autorzy:
    Hong, W.
    Wang, Z.
    Chen, Q.
    Sheng, C.
    Gu, G.
    Luo, P.
    Xie, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/174416.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    vanadium oxide
    VO2
    film
    surface microstructure
    photonic band edge
    dispersion material
    Opis:
    This paper presents a method to design a surface microstructure of vanadium oxide to enhance optical absorption. This method, using a density of eigenfrequency, can be calculated by a planar wave expand method, to indicate the absorption efficiency of a dispersion material, which can be used as an approach method for further design. Based on this, a nanostructure-based vanadium oxide film is designed and simulated to validate this method. The simulation results show that the tendency of density of eigenfrequency is corresponding to the tendency of optical absorption enhancement. Moreover, this structure can achieve high optical broadband absorption when the material dispersion is considered. High optical absorption enhancement can be achieved by adjusting the geometrical parameters; our maximum overall enhancement absorption ratio was 31.84% at the metal phase, which can be attributed to the enhancement effect of a photonic band edge.
    Źródło:
    Optica Applicata; 2017, 47, 4; 601-609
    0078-5466
    1899-7015
    Pojawia się w:
    Optica Applicata
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis of vanadium-enriched oxide materials via modified sol-gel route with the use of waste solutions contaminated with vanadium ions
    Autorzy:
    Weidner, Ewelina
    Piasecki, Adam
    Siwińska-Ciesielczyk, Katarzyna
    Jesionowski, Teofil
    Ciesielczyk, Filip
    Powiązania:
    https://bibliotekanauki.pl/articles/1450632.pdf
    Data publikacji:
    2020
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    modified sol-gel method
    zirconia
    vanadium recovery
    hybrid oxide materials
    harmful metal ions
    Opis:
    In this study, the synthesis of zirconia as well as zirconia enriched with vanadium by modified sol-gel method was presented. The modification of the method was based on the replacement of the traditional basic promoter of hydrolysis, which is ammonia, with sodium hydroxide solution. The most favorable conditions for the synthesis of zirconium with a new hydrolysis promoter were selected. A comparative analysis of $ZrO_2$ obtained using various hydrolysis promoters was performed. Both materials exhibited almost the same physicochemical properties, which proves that in this case the nature of the hydrolysis promoter used in sol-gel route does not significantly affect the properties of the $ZrO_2$. Then, synthesis of $ZrO_2$/V systems was carried out using model and real solutions containing vanadium ions as hydrolysis promoters. The solutions formed after vanadium catalyst leaching were used as real solutions. The effect of vanadium concentration and the presence of impurities on the final physicochemical properties of the obtained hybrid materials were investigated via scanning electron microscopy (SEM), dynamic light scattering (DLS), energy-dispersive X-ray microanalysis (EDS), Fourier transform infrared spectroscopy (FT-IR), low-temperature nitrogen sorption (BET), thermogravimetric analysis (TGA). The analysis of the obtained results allows to state that the developed technique for the synthesis of $ZrO_2$ and $ZrO_2$/V systems, using a modified sol-gel method, enabled the production of attractive materials.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2020, 56, 6; 60-75
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    On influence of anodic oxidation on thrombogenicity and bioactivity of the Ti-13Nb- 13Zr alloy
    Autorzy:
    Szymonowicz, M.
    Kazek-Kęsik, A.
    Sowa, M.
    Żywicka, B
    Rybak, Z.
    Simka, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/951810.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    stopy tytanu
    utlenianie anodowe
    modyfikacja powierzchni
    krew
    vanadium-free titanium alloys
    anodic oxidation
    surface modification
    blood compatibility
    Opis:
    Purpose: This paper reports the results of investigations of the blood response of the modified titanium alloys surfaces. Methods: To enhance biocompatibility of the Ti-13Nb-13Zr alloy, anodisation was performed at 80 and 150 V. The oxidation process was carried out in a solution containing 4 mol dm−3 H3PO4 and 0.59 mol dm−3 Ca(H2PO2)2. Results: The haemolytic activity of the titanium alloy surface was not altered much by the anodisation. The obtained values of the percentage of haemolysis were well below the levels required for the materials intended for blood contact. The clotting time of the blood was similar for the as-ground sample and the sample anodised at 80 V. For the sample anodised at 150 V the clotting time was shorter. The differences between these samples were observed in partial thromboplastin time after activation, prothrombin time and thrombin time, after 24 h. Extracts taken from the samples were not toxic towards the L-929 mouse fibroblast cells. Conclusions: The proposed treatment might be appropriate for the preparation of the modified Ti-13Nb-13Zr surfaces intended for bone reconstruction or cardiovascular implants depending on process parameters.
    Źródło:
    Acta of Bioengineering and Biomechanics; 2017, 19, 2; 41-50
    1509-409X
    2450-6303
    Pojawia się w:
    Acta of Bioengineering and Biomechanics
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-15 z 15

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