Informacja

Drogi użytkowniku, aplikacja do prawidłowego działania wymaga obsługi JavaScript. Proszę włącz obsługę JavaScript w Twojej przeglądarce.

English (EN)·Polski (PL)·Yкраїнський (UK)
Przejdź do strony domowej biblioteki Centralna Biblioteka Wojskowa Link otwiera się w nowym oknie Logo biblioteki Prolib Integro - strona głównaCentralna Biblioteka Wojskowa

Wyszukujesz frazę "titanium dioxide," wg kryterium: Temat

  Lista filtrów
Wyrównaj
Wyświetlanie 1-15 z 16
Tytuł:
The optical parameters of TiO2 antireflection coating prepared by atomic layer deposition method for photovoltaic application
Autorzy:
Szindler, Marek
Szindler, Magdalena M.
Powiązania:
https://bibliotekanauki.pl/articles/1835965.pdf
Data publikacji:
2020
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
thin film
atomic layer deposition
titanium dioxide
Opis:
Titanium dioxide thin films have been deposited on silicon wafers substrates by an atomic layer deposition (ALD) method. There optical parameters were investigated by spectroscopic ellipsometry and UV/VIS spectroscopy. A material with a refractive index of 2.41 was obtained. Additionally, in a wide spectral range it was possible to reduce the reflection from the silicon surface below 5%. The Raman spectroscopy method was used for structural characterization of anatase TiO2 thin films. Their uniformity and chemical composition are confirmed by a scanning electron microscope (SEM) energy dispersive spectrometer (EDS).
Źródło:
Optica Applicata; 2020, 50, 4; 663-670
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural and photocatalytic properties of Ni-TiO2 photocatalysts prepared by mechanochemical synthesis assisted with calcination
Autorzy:
Kucio, Karolina
Charmas, Barbara
Zięzio, Magdalena
Pasieczna-Patkowska, Sylwia
Powiązania:
https://bibliotekanauki.pl/articles/2146911.pdf
Data publikacji:
2022
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
mechanochemical synthesis
titanium dioxide
photocatalysis
photocatalysts
safranin T
Opis:
In the study the mechanochemical synthesis in the planetary ball mill was used to prepare photocatalytic materials obtained on the basis of TiO2 and nickel(II) acetylacetonate as a Ni2+ source. Three materials with different contents of Ni2+: 5, 10 and 20% wt. were prepared. The obtained materials were calcinated at 800°C for 1 h. Their physicochemical properties were investigated using the N2 adsorption/desorption, FT-IR/PAS, XRD, UV-Vis/DRS and SEM methods. Additionally, thermal stability of the obtained materials was examined (TGA/DTG/DTA). Photocatalytic activity of the samples was tested in relation to the aqueous solution of Safranin T (initial concentration C0 = 1×10-5 mol L-1) at the visible light (Vis). The results indicate that the mechanochemical synthesis is an effective and simple method for preparing materials with photocatalytic properties. All obtained materials were characterized by greater photocatalytic activity compared to the initial TiO2.
Źródło:
Physicochemical Problems of Mineral Processing; 2022, 58, 4; art. no. 150348
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ammonia level sensor using tapered optical fiber coated with titanium dioxide-incorporated porphyrin
Autorzy:
Parasuti, Frazna
Hikmawati, Dyah
Trilaksana, Herri
Yasin, Moh.
Powiązania:
https://bibliotekanauki.pl/articles/27310105.pdf
Data publikacji:
2023
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
ammonia sensing
tapered optical fibre
titanium dioxide
porphyrin
Opis:
Since ammonia is water-soluble, environmental studies have shown that the industrial waste such as fertilizer manufacturing, food products, palm oil, urea fertilizer industry can cause very serious damage to water body ecosystems if not properly managed, resulting in a decrease in water quality. Devices based on optical technology, especially devices that combine optical fibers and nanomaterials, are identified as highly sensitive to the species of interest by detecting changes in physicochemical properties. A practical, easy-to-use, inexpensive instrument for detecting ammonia level was proposed using tapered optical fiber (TOF) coated with titanium dioxide-incorporated porphyrin. TOF was fabricated by simultaneously stretching and heating. The preparation of TiO2/porphyrin/gelatine was prepared to coat tapered optical fiber by dipping. SEM analysis shows an increase in length and a decrease in diameter, also the successful coating of titanium dioxide and porphyrin in the taper region. The EDX analysis also proves the presence of the Ti element in the TOF layer. The TOF produces significant sensing performances toward the ammonia liquid concentration level. The TOF coated with titanium dioxide-incorporated porphyrin can detect a one ppm difference in ammonia concentration with a certain range of output voltage for every concentration has.
Źródło:
Optica Applicata; 2023, 53, 3; 353--361
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of chitosan, hyaluronic acid and/or titanium dioxide on the physicochemical characteristic of phospholipid film/glass surface
Autorzy:
Ładniak, Agata
Jurak, Małgorzata
Wiącek, Agnieszka Ewa
Powiązania:
https://bibliotekanauki.pl/articles/109601.pdf
Data publikacji:
2019
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
chitosan
titanium dioxide
hyaluronic acid
phospholipid
adhesion
topography
Opis:
The production of preparations, whose destination action takes place in close proximity to living cells, increases the necessity to carry out studies concerning the determination of the biomaterial surface effect on the cellular response. In achieving this goal, physicochemical characteristic of the surface can be helpful. This can be established based on topography, chemical composition, wettability, and surface energy analysis. In addition, determining the changes of these properties which can occur as a result of surface modification will allow prediction of cell behaviour when contacting with biomaterial. In the study, the Langmuir-Blodgett technique was used. It enabled the transfer of the Langmuir monolayer formed from 1,2-dipalmitoyl-sn-glycero-3-phosphocholine (DPPC) to a solid support. The DPPC film imitated a natural biological membrane capable of interacting with the components of the liquid subphase: chitosan (Ch), hyaluronic acid (HA) and/or titanium dioxide (TiO2). Depending on the type and strength of interactions of phospholipid molecules with the components of the subphase, the films obtained on the solid support were characterized by specific surface properties. Their characteristics based mainly on values of the work of adhesion in connection with films topography, allowed for statement that it is possible to form semi-interpenetrating Ch network in which HA is entrapped, contributing to the enhanced adhesion of the DPPC film, additionally intensified by TiO2 inclusion. This type of research permit for better understanding of the interactions at the interface, cell membrane-Ch/HA/TiO2 and can be important in the creation of a new generation of skin or tissue substitutes.
Źródło:
Physicochemical Problems of Mineral Processing; 2019, 55, 6; 1535-1548
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Kinetics of sulphuric acid leaching of titanium from refractory anatase under atmospheric pressure
Autorzy:
Gao, Likun
Rao, Bing
Dai, Huixin
Xie, Haiyun
Wang, Peng
Ma, Fangtong
Powiązania:
https://bibliotekanauki.pl/articles/109701.pdf
Data publikacji:
2019
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
anatase ore
kinetics
sulphuric acid
leaching
titanium dioxide
Opis:
Anatase, as an important titanium resource, is attracting more and more attention in research and application. In this study, an efficient process of comprehensively extracting the titanium and other valuable elements from the anatase mineral was proposed. The effect of particle size, stirring speed, initial sulphuric acid concentration, solid-to-liquid ratio, and reaction temperature on the leaching rate of titanium from anatase was investigated. Under appropriate two-stage countercurrent leaching conditions, with the first stage of the liquid-to-solid ratio of 1/3 g/cm3, reaction temperature of 120 °C, initial acid concentration of 11 mol/dm3, residence time of 30 min, stirring speed of 200 rpm, and the second stage of the liquid-to-solid ratio of 1/3 g/cm3, reaction temperature of 200 °C, initial acid concentration of 13 mol/dm3, residence time of 30 min, and stirring speed of 200 rpm, over 99% TiO2, 99% Al2O3, and 97% Sc2O3 were extracted respectively with quartz still remained in the residue. X-ray diffraction, X-ray fluorescence spectrometer, and scanning electron microscopy/energy-dispersive spectroscopy were used to characterize the anatase samples before and after the leaching. Additionally, the leaching kinetics analysis indicated that both acid concentration and temperature were the most significant parameters for the leaching process. And, the titanium leaching reaction rate was controlled by the diffusion of reactants through the residual layer.
Źródło:
Physicochemical Problems of Mineral Processing; 2019, 55, 2; 467-478
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Novel (Ag,Y) doped TiO2 plasmonic photocatalyst with enhanced photocatalytic activity under visible light
Autorzy:
Kallel, Wannes
Chaabene, Sirine
Bouattour, Soraa
Powiązania:
https://bibliotekanauki.pl/articles/110853.pdf
Data publikacji:
2019
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
titanium dioxide
XRD
plasmonic photocatalyst
Methylene Blue
visible light
Opis:
Nano-sized Y- Ag doped and co-doped TiO2 particles were synthesized using the sol–gel method and Ti(OBu)4 as TiO2 precursor. Their structural and optical properties were examined by scanning electron microscopy (SEM), XRD, thermogravimetric-differential thermal analysis (TG-DTA), FT-IR and UV-vis absorption spectroscopies. The photocatalytic activity of these materials was investigated for the photodegradation of methylene blue (MB) as a model reaction under visible light irradiation. Ground state diffuse reflectance absorption studies reveal that both Y and Ag dopant cause deviations of the band gap to higher energies attesting that co-doping the TiO2 with Y and Ag could enhance the photocatalytic activity by delaying the electron–hole recombination by means of higher energy band gaps. Co-doping TiO2 at a level of 4% (Y, Ag) samples leads to a significant decrease in the crystallite size of photocatalyst and containing both anatase and Ag/AgCl components. However, the high photocatalytic performance is attributed to an efficient electron-hole pairs separation at the photocatalyst interfaces in addition to localized surface plasmon resonance of Ag particles. The development of these visible light- activated nanocatalysts has the potential of providing environmentally benign routes for water treatment.
Źródło:
Physicochemical Problems of Mineral Processing; 2019, 55, 3; 745-759
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The removal of Fe from the reduced ilmenite via aeration leaching assessing the effect of operating parameters
Autorzy:
Ibrahim, Siti Asmidar
Yunus, Farhana
Ariffin, Kamar Shah
Sheikh Abdul Hamid, Sheikh Abdul Rezan
Ismail, Suhaina
Jabit, Nurul Ain
Powiązania:
https://bibliotekanauki.pl/articles/2146865.pdf
Data publikacji:
2021
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
ilmenite
reduced ilmenite
aeration leaching
synthetic rutile
titanium dioxide
Opis:
An upgrade of Malaysian ilmenite (FeTiO3) concentrate to synthetic rutile (TiO2) using aeration leaching was investigated in this study. Carbothermal reduction using Sarawak MukahBalingan coal and compressed National Gas (CNG) as a reductant was used to produce reduced ilmenite (RI) as an intermediate phase consisting of titanium oxide matrix with metallic iron prior to aeration leaching. Metallic iron was dissolved in ammonium chloride solution after the reduction process, separating synthetic rutile in the leaching residue. This study aims to evaluate the leaching parameters, such as concentration, temperature, and leaching time. The optimum conditions established by the design of the experiment (DOE) and the analysis of variance (ANOVA) has indicated that leaching temperature was the most significant parameter for iron dissolution. It was found that iron dissolution at a maximum value of 97.0% was achieved at an optimum condition of 0.5 M NH4Cl at 90°C for 7 hours. With an initial weight of 46 wt.%TiO2 and 37 wt.% Fe2O3, ilmenite was successfully upgraded to 80 wt.% and 8 wt.%, respectively. In conclusion, Malaysian ilmenite has a high potential value to be upgraded to synthetic rutile by aeration leaching with ammonium chloride via Becher process.
Źródło:
Physicochemical Problems of Mineral Processing; 2021, 57, 6; 182--195
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of sunlight and ultraviolet radiation on the efficacy of Fe-doped titanium dioxide (Fe-TiO2) nanoparticles for the removal of furfural from aqueous solutions
Autorzy:
Veisi, F.
Zazouli, M. A.
Zadeh, M. A. E.
Charati, J. Y.
Dezfuli, A. S.
Powiązania:
https://bibliotekanauki.pl/articles/207273.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
chromatography
titanium dioxide
ultraviolet radiation
chromatografia
dwutlenek tytanu
promieniowanie ultrafioletowe
Opis:
Furfural, chemical compound very harmful to human health and difficult to degrade, is used or generated in many industries, including petrochemical, paper, and oil refining industries. The study evaluates the performance of Fe-TiCh nanoparticles for the removal of furfural in the presence of sunlight and UV radiation. Fe-TiO2 nanoparticles were prepared by the sol-gel method, and the characteristics of the resultant nanoparticles were determined using scanning electron microscopy. Samples with known concentrations of furfural and nanoparticles were individually exposed to sunlight and UV radiation under varying conditions, and the residual furfural concentration was measured using high- performance liquid chromatography. The results showed that for both processes the efficiency of furfural removal increased with increased reaction time, nanoparticle loading, and pH, whereas the efficiency decreased with increased furfural concentratioa The highest removal efficiencies of the Fe-TiCh/UV and Fe-TiCh/sun processes were 95 and 76%, respectively. In general, the degradation and elimination rate of furfural using Fe-TiO2/UV process was higher than Fe-TiCVsun process because TiO2 nanoparticles can only be activated upon irradiation with photons of light in the UV domain.
Źródło:
Environment Protection Engineering; 2017, 43, 3; 207-224
0324-8828
Pojawia się w:
Environment Protection Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterisation of nano-thin film GO/TiO2 layers for Kretschmann-based surface plasmon resonance visible sensing using FDTD method
Autorzy:
Khairulazdan, N. B.
Mohamed, R.
Berhanuddin, D. D.
Menon, P. S.
Powiązania:
https://bibliotekanauki.pl/articles/2033878.pdf
Data publikacji:
2021
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
surface plasmon resonance
FDTD
titanium dioxide
graphene oxide
Kretschmann
biosensor
Opis:
Kretschmann-based surface plasmon resonance (K-SPR) is suitable for biomolecular sensing which provides label-free and quick detection results with real-time analysis. In this work, we have investigated the effect of graphene oxide (GO) with titanium dioxide (TiO2) thin films that are placed in hybrid above metal layers such as gold (Au), silver (Ag) and copper (Cu) with the presence of chromium (Cr) as an adhesive layer. The thickness of the Au, Ag and Cu metal thin films were optimized to 40, 30 and 30 nm, respectively, with a fixed thickness of GO of 2 nm and TiO2 of 1.9 nm. The sensing was evaluated for SPR excitation at three different visible wavelengths of 633, 670 and 785 nm. The performance of sensing was analyzed based on the reflectance intensity and full-width at half-maximum (FWHM) of the spectrum using the finite-difference time-domain (FDTD) method. The sensitivity was calculated for analyte sensing in dielectric mediums of air versus water. The sensitivity increment percentage (%∆S ) was determined when comparing analyte detection using Cr/metal and Cr/metal/GO/TiO2 sensor structures. The highest sensitivity of 94.51 deg/RIU was achieved for Cr/Cu/GO/TiO2 K-SPR sensor at 633 nm wavelength.
Źródło:
Optica Applicata; 2021, 51, 4; 579-587
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Photocatalytic properties of Ti–V oxides thin films
Autorzy:
Domaradzki, J
Mazur, M
Sieradzka, K
Wojcieszak, D
Adamiak, B
Powiązania:
https://bibliotekanauki.pl/articles/174210.pdf
Data publikacji:
2013
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
titanium dioxide (TiO2)
thin films
magnetron sputtering
vanadium
photocatalysis
Opis:
In this work, the photocatalytic properties of Ti–V oxides thin films with 19 and 23 at.% of vanadium addition have been outlined. The films were deposited by the high energy reactive magnetron sputtering method. X-ray photoelectron spectroscopy measurements were done in order to determine the chemical composition and binding energy of the elements on the samples surface. Additionally, based on wettability measurements, the water contact angles were evaluated and were equal to ca. 94° and 55° for thin films with 19 and 23 at.% of V, respectively. This testifies about hydrophilic and hydrophobic properties, respectively. Photoactivity of thin films was determined by percent decomposition of phenol for 5 hours during UV–vis radiation exposure. The highest photocatalytic activity of 6.2%/cm2 was obtained for thin films with 19 at.% of V. It has been found that an increase in V amount in Ti–V oxides thin films to 23 at.% results in lowered to 3%/cm2 photocatalytic activity.
Źródło:
Optica Applicata; 2013, 43, 1; 153-162
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of geometry and annealing temperature in argon atmosphere of TiO2 nanotubes on their electrochemical properties
Autorzy:
Nycz, Marta
Paradowska, Ewa
Arkusz, Katarzyna
Pijanowska, Dorota Genowefa
Powiązania:
https://bibliotekanauki.pl/articles/307103.pdf
Data publikacji:
2020
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
dwutlenek tytanu
TiO2
modyfikacja termiczna
wyżarzanie
titanium dioxide (TiO2)
titanium nanotubes
thermal modification
annealing
Opis:
In this paper, electrochemical properties of the as-formed and thermally treated titanium dioxide (TiO2) nanotubes with diameter in the range of 20–100 nm and height in the range of 100–1000 nm were presented. In addition, the effects of annealing temperature (450–550 °C) on the electrochemical characteristics of these structures, as well as the influence of diameter and height of TiO2 nanotubes on these properties were examined. The results were referred to a compact TiO2 layer (100 nm thick). Methods: The electrochemical test included open circuit potential, impedance spectroscopy and cyclic voltammetry measurements. The scanning electron microscope with energy dispersive spectroscopy analyser, x-ray photoelectron spectroscopy, and x-ray diffraction analysers were used for surface morphology characterisation as well as elemental, phase and chemical composition of TiO2 layers. Results: It was found that nanotubes with the diameter of 50 and 75 nm (height of 1000 nm) annealed at 550 °C exhibit the lowest impedance and phase angle values. However, the voltammetric detection of potassium ferricyanide indicated that the closest to 1 Ipc /Ipa ratio were shown by nanotubes with a diameter of 50 and 75 nm annealed at 450 °C. Conclusions: On the basis of performed analysis, it can be stated that the TiO2 layer with nanotubes of 50 nm in diameter and of 1000 nm in height, annealed in 450 °C may be indicated as the ones having the most favourable sensing and biosensing properties.
Źródło:
Acta of Bioengineering and Biomechanics; 2020, 22, 1; 165-177
1509-409X
2450-6303
Pojawia się w:
Acta of Bioengineering and Biomechanics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and physicochemical characteristics of titanium dioxide doped with selected metals
Autorzy:
Siwinska-Stefanska, K.
Paukszta, D.
Piasecki, A.
Jesionowski, T.
Powiązania:
https://bibliotekanauki.pl/articles/951839.pdf
Data publikacji:
2014
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
titanium dioxide
sol-gel method
doping
TiO2 surface modification
Fe and Co dopant
Opis:
The paper details with of the preparation and physicochemical characterisation of nano- and microstructured TiO2 doped with Fe and Co produced by the sol-gel method using titanium alkoxide as the precursor of titania as well as iron or cobalt nitrates as dopant sources. Fe and Co doped TiO2 materials were successfully prepared with two different methods. The effect of the dopant type on the synthesis of TiO2 powders was investigated. The physicochemical properties of the studied samples were determined. The characterisation included determination of the dispersion and morphology of the systems (particle size distribution, SEM images), characteristics of porous structure (BET isotherms), crystalline structure (XRD), surface composition (EDS), as well as thermal stability (TG/DTA).
Źródło:
Physicochemical Problems of Mineral Processing; 2014, 50, 1; 265-276
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects of ZnO, CuO, Au, and TiO2 nanoparticles on Daphnia magna and early life stages of zebrafish danio rerio
Autorzy:
Liu, J.
Fan, D.
Wang, L.
Shi, L.
Ding, J.
Chen, Y.
Shen, S.
Powiązania:
https://bibliotekanauki.pl/articles/207169.pdf
Data publikacji:
2014
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
metal oxides
titanium dioxide
nanoparticles
toxicity
zinc oxide
Daphnia magna
nanocząsteczki
tlenki metali
dwutlenek tytanu
toksyczność
tlenek cynku
rozwielitki
Opis:
The effects of four different kinds of nanoparticles (NPs), namely, CuO, ZnO, TiO2, and Au, of the sizes ranging from <20 nm to 50 nm on Daphnia magna, early life stage of zebrafish, and various enzymes have been investigated. The experimental results showed that the NPs inhibited both the body length and hatching rate of zebrafish larvae; the small nanoparticles exhibited more toxicity. In a 21 day chronic toxicity test, metal ions of higher concentrations significantly reduced the number of Daphnia magna offspring. Studies on enzyme activity showed that the NPs reduced the glutathione content and inhibited catalase and superoxide dismutase activities, resulting in shorter body length, lower hatching success, and lower reproduction of zebrafish larvae. Therefore, studies should focus more on the potential toxicity of smaller NPs.
Źródło:
Environment Protection Engineering; 2014, 40, 1; 139-149
0324-8828
Pojawia się w:
Environment Protection Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The influence of sintering conditions on microstructure and mechanical properties of titanium dioxide scaffolds for the treatment of bone tissue defects
Autorzy:
Rumian, Ł.
Reczyńska, K.
Wrona, M.
Tiainen, H.
Haugen, H. J.
Pamuła, E.
Powiązania:
https://bibliotekanauki.pl/articles/307325.pdf
Data publikacji:
2015
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
porowatość
inżynieria tkankowa
ditlenek tytanu
właściwości mechaniczne
porosity
titanium dioxide
bone tissue engineering
mechanical properties
polymer sponge replication
ceramic scaffolds
Opis:
In this study the attempts to improve mechanical properties of highly-porous titanium dioxide scaffolds produced by polymer sponge replication method were investigated. Particularly the effect of two-step sintering at different temperatures on microstructure and mechanical properties (compression test) of the scaffolds were analysed. To this end microcomputed tomography and scanning electron microscopy were used as analytical methods. Our experiments showed that the most appropriate conditions of manufacturing were when the scaffolds were heat-treated at 1500 °C for 1 h followed by sintering at 1200 °C for 20 h. Such scaffolds exhibited the highest compressive strength which was correlated with the highest linear density and the lowest size of grains. Moreover, grain size distribution was narrower with predominating fraction of fine grains 10–20 μm in size. Smaller grains and higher linear density suggested that in this case densification process prevailed over undesirable process of grain coarsening, which finally resulted in improved mechanical properties of the scaffolds.
Źródło:
Acta of Bioengineering and Biomechanics; 2015, 17, 1; 3-9
1509-409X
2450-6303
Pojawia się w:
Acta of Bioengineering and Biomechanics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of the effect of heat treatment process on characteristics and photocatalytic activity of TiO2-UV100 nanoparticles
Autorzy:
Behnajady, M. A.
Alamdari, M. E.
Modirshahla, N.
Powiązania:
https://bibliotekanauki.pl/articles/208146.pdf
Data publikacji:
2013
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
titanium dioxide
photocatalysis
X ray diffraction
Brunauer Emmett Tellers
heat treatment
photocatalytic activity
dwutlenek tytanu
ditlenek tytanu
fotokataliza
dyfrakcja promieniowania rentgenowskiego
izotermy Brunauer Tellers Emmett
obróbka cieplna
aktywność fotokatalityczna
Opis:
The effect of heat treatment process on crystallite size, phase content, surface area, band gap energy and photocatalytic activity of TiO 2-UV100 nanoparticles were investigated. Heat treated TiO2 nanoparticles were characterized by X-ray diffraction (XRD), Brunauer-Emmett-Teller (BET) isotherm and diffuse reflectance spectroscopy (DRS) techniques, and its photocatalytic activity was investigated in the removal of C.I. Acid Red 88 (AR88), an anionic monoazo dye of acid class, as a model contaminant. Heat treatment process at 600 °C causes an increase in crystallite size and band gap energy of TiO2-UV100 nanoparticles. The results indicate that the nanoparticles treated for 1 h at 600 °C show the highest photocatalytic activity which can effectively degrade AR88 under UV-irradiation. Increasing heat treatment temperature above 600 °C led to reduction in TiO2 photoactivity which may be related to the anatase-rutile phase transformation, increasing particle size and decreasing specific surface area. Removal efficiency of AR88 with heat treated TiO 2-UV100 nanoparticles was sensitive to the operational parameters such as catalyst dosage, pollutant concentration and light intensity.
Źródło:
Environment Protection Engineering; 2013, 39, 1; 33-46
0324-8828
Pojawia się w:
Environment Protection Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 16

Ta witryna wykorzystuje pliki cookies do przechowywania informacji na Twoim komputerze. Pliki cookies stosujemy w celu świadczenia usług na najwyższym poziomie, w tym w sposób dostosowany do indywidualnych potrzeb. Korzystanie z witryny bez zmiany ustawień dotyczących cookies oznacza, że będą one zamieszczane w Twoim komputerze. W każdym momencie możesz dokonać zmiany ustawień dotyczących cookies