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    Wyświetlanie 1-3 z 3
    Tytuł:
    Synthesis of vanadium-enriched oxide materials via modified sol-gel route with the use of waste solutions contaminated with vanadium ions
    Autorzy:
    Weidner, Ewelina
    Piasecki, Adam
    Siwińska-Ciesielczyk, Katarzyna
    Jesionowski, Teofil
    Ciesielczyk, Filip
    Powiązania:
    https://bibliotekanauki.pl/articles/1450632.pdf
    Data publikacji:
    2020
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    modified sol-gel method
    zirconia
    vanadium recovery
    hybrid oxide materials
    harmful metal ions
    Opis:
    In this study, the synthesis of zirconia as well as zirconia enriched with vanadium by modified sol-gel method was presented. The modification of the method was based on the replacement of the traditional basic promoter of hydrolysis, which is ammonia, with sodium hydroxide solution. The most favorable conditions for the synthesis of zirconium with a new hydrolysis promoter were selected. A comparative analysis of $ZrO_2$ obtained using various hydrolysis promoters was performed. Both materials exhibited almost the same physicochemical properties, which proves that in this case the nature of the hydrolysis promoter used in sol-gel route does not significantly affect the properties of the $ZrO_2$. Then, synthesis of $ZrO_2$/V systems was carried out using model and real solutions containing vanadium ions as hydrolysis promoters. The solutions formed after vanadium catalyst leaching were used as real solutions. The effect of vanadium concentration and the presence of impurities on the final physicochemical properties of the obtained hybrid materials were investigated via scanning electron microscopy (SEM), dynamic light scattering (DLS), energy-dispersive X-ray microanalysis (EDS), Fourier transform infrared spectroscopy (FT-IR), low-temperature nitrogen sorption (BET), thermogravimetric analysis (TGA). The analysis of the obtained results allows to state that the developed technique for the synthesis of $ZrO_2$ and $ZrO_2$/V systems, using a modified sol-gel method, enabled the production of attractive materials.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2020, 56, 6; 60-75
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Statistical approach to the production of cement composites doped with ZnO and ZnO-based materials
    Autorzy:
    Klapiszewska, Izabela
    Balicki, Sebastian
    Wilk, Kazimiera A.
    Klapiszewski, Łukasz
    Ślosarczyk, Agnieszka
    Powiązania:
    https://bibliotekanauki.pl/articles/24085675.pdf
    Data publikacji:
    2023
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    cement composite
    zinc oxide
    hybrid materials
    design of experiments
    Opis:
    In this study, physical and functional properties of the cement composites containing ZnO, ZnO/lignin and lignin admixtures were investigated using Response Surface Methodology (RSM). The I-optimal design based on RSM was used to assess the influence of ZnO-based doping agent, of either commercial or synthetic origin, on cement composite production in the function of average compressive strength and cost. Polynomial mathematical models were developed by RSM confronting results from the experimental design. The accuracy and precision of the utilized models established by I-optimal design were tested using Analysis of Variance (ANOVA). The first stage of formulation optimization revealed that the use of commercially available ZnO-based admixture no. 4 (ZnO-SA, supplied by Sigma Aldrich) allowed to achieve the desired results, passing all the requirements, i.e., the best microbial purity combined with reasonable cost, followed by satisfactory physical properties. In the second stage of formulation optimization, the influence of implementing the hybrid materials, i.e., ZnO-SA mixed in different proportions with lignin was evaluated. RSM revealed that doping admixture no. 3, i.e., ZnO-SA/lignin (5:1), is the best candidate, which comprised augmented functional and physical properties of the fabricated cement composite. This component exhibited the best microbial purity as well as the lowest total pore volume, followed by satisfactory physical properties. Verification of the model findings indicated considerable agreement between the predicted and experimental values. From the findings, it was confirmed that a reasonable cost-performance balance for cement composites can be achieved using ZnO-SA and ZnO-SA/lignin (5:1).
    Źródło:
    Physicochemical Problems of Mineral Processing; 2023, 59, 4; art. no. 168352
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Use of synthetic zeolite materials from fly ash to remove copper(II) ions from aqueous solutions
    Autorzy:
    Ulatowska, Justyna
    Stala, Łukasz
    Nowakowska, Alicja
    Polowczyk, Izabela
    Powiązania:
    https://bibliotekanauki.pl/articles/1450167.pdf
    Data publikacji:
    2020
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    fly ash
    copper oxide (II)
    Cu(II)
    modification of fly ashes
    zeolite materials
    adsorption
    Opis:
    Water quality and waste management are two chief problems that the modern world is struggling with. Intensified development of the industry not only leads to the production of large amounts of solid waste that must be stored in landfills but can also result in contaminant emissions into the environment. Enormous quantities of ash produced from coal combustion have been a long-term problem of the industry. Literature studies show that fly ash can be used as a material to produce cheap and efficient zeolite-type adsorbents due to abundance of alumina-silicates in their composition. Fly ashes which were processed into zeolites as a result of alkaline hydrothermal treatment were obtained from two power plants in Poland (in Turów and Zgierz). The obtained zeolite materials and raw fly ash samples were characterised in terms of specific surface area, particle size distribution and density. The structure was also investigated using Fourier transform infrared spectroscopy (FTIR) in the mid- infrared wavenumber range. Two raw fly ashes and two zeolite materials were examined for their ability to remove Cu(II) ions from aqueous solutions. The results showed that the amount of adsorbed copper ions by alkaline-modified fly ash was higher than for unmodified fly ash. The ion removal efficiency is high and exceeds 95%.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2020, 56, 6; 114-124
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-3 z 3

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