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Wyświetlanie 1-15 z 49
Tytuł:
Adsorption of Zn2+, Cd2+ and Cu2+ on zeolites coated by manganese and iron oxides
Autorzy:
Irannajad, M.
Hhaghighi, H. K.
Soleimanipour, M.
Powiązania:
https://bibliotekanauki.pl/articles/110138.pdf
Data publikacji:
2016
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
adsorption
wastewater
manganese oxide
iron oxide
zeolite
Opis:
Adsorption of copper, cadmium and zinc on manganese and iron oxide coated zeolite from aqueous solution was investigated in a batch mode. Experiments were conducted to investigate the effects of the initial concentration of metals, initial pH, contact time and temperature on the adsorption of ions. According to the results, adsorption of ions on manganese and iron oxide coated zeolite increased with the enhancement of initial Cu2+, Zn2+ and Cd2+ concentrations and contact time and also with increase of temperature. The results showed that at the beginning, the adsorption rate of Cu2+ and Cd2+ was more than 90 %. This rate continued to be slower for Zn2+ in both zeolites. Furthermore, the amount of Cu2+, Zn2+, and Cd2+ adsorption on the manganese oxide coated zeolite (qe) was equal to 14 mg/g, 9 mg/g and 16 mg/g and on the iron oxide coated zeolite it was 11 mg/g, 7 mg/g and 13mg/g, respectively. It was shown that at the concentrations below 100 mg/dm3 adsorption was rapid and almost all heavy metals were adsorbed. As a result, the significant factor affecting qe is the proportion of weight to liquid and pH in the solutions. Finally, the results showed that the adsorption of Zn2+, Cu2+ and Cd2+ onto the manganese oxide coated zeolite followed both the Langmuir and Freundlich isotherm models.
Źródło:
Physicochemical Problems of Mineral Processing; 2016, 52, 2; 894-908
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A successful operational initiative in copper oxide flotation: Sequential sulphidisation-flotation technique
Autorzy:
Asadi, Moharram
Soltani, Faraz
Mohammadi, Mohammad Reza Tavakoli
Khodadadi, Darban Ahmad
Abdollahy, Mahmoud
Powiązania:
https://bibliotekanauki.pl/articles/110770.pdf
Data publikacji:
2019
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
copper oxide
sulphidisation
flotation
Opis:
One of the main challenges in the copper oxide processing industry is implementation of a flotation method to reduce operating costs. Sulphidising flotation is the most common used technique in which a sulphidisation agent is used to sulphidise the surface of the oxide minerals. In this research, the mentioned technique was used sequentially for the concentration of silicate-carbonate ore containing 3.1% Cu (malachite). The presence of 39% Cu in -38 μm size fraction (fine particles) of feed led to poor grades and recoveries in the initial tests. The addition of sodium sulfide and subsequent flotation at three sequential stages was identified as a successful operational initiative to solve this problem in the following tests. The dosages of 1500, 1567 and 100 g/Mg of sodium silicate, sodium sulfide and potassium amyl xanthate, respectively, the conditioning time of 5 min for sulphidisation and pH=9.72 were chosen as optimum operational conditions using central composite design (CCD) method of experiments design. The rougher concentrate with 9.28% grade and 81.15% recovery was obtained under these conditions. The grade of obtained concentrate was reached to 24% in the cleaner step. The total recovery of both steps was over 74%.
Źródło:
Physicochemical Problems of Mineral Processing; 2019, 55, 2; 356-369
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Transparent yttrium oxide ceramics as potential optical isolator materials
Autorzy:
Kruk, A
Wajler, A
Mrozek, M
Zych, L
Gawlik, W
Brylewski, T
Powiązania:
https://bibliotekanauki.pl/articles/173500.pdf
Data publikacji:
2015
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
transparent ceramics
optical properties
yttrium oxide
Opis:
The objective of the presented study was to investigate the usefulness of transparent, sintered yttrium oxide for application as optical isolators, i.e., materials with high Verdet constant. The study utilizes the magneto-optical Faraday effect. To obtain yttrium oxide sinters, a commercial Y2O3 powder was applied, with LiF added to facilitate sintering. As a result of hot-press sintering and heating, transparent, dense sinters were obtained. The structure and morphology of the powders and bulk samples and the optical properties of the latter were investigated by means of X-ray diffraction, scanning electron microscopy, visible and near-infrared reflectance spectroscopy, and a study of magneto-optical (Faraday) effects. Measurements of the Faraday effect in the wavelength range of 500–1000 nm indicate high Verdet constants for the above-described materials, which means that they can be effectively applied in laser optics.
Źródło:
Optica Applicata; 2015, 45, 4; 585-594
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The impact of atomic layer deposition technological parameters on optical properties and morphology of Al2O3 thin films
Autorzy:
Dobrzanski, L. A.
Szindler, M.
Hajduk, B.
Kotowicz, S.
Powiązania:
https://bibliotekanauki.pl/articles/173801.pdf
Data publikacji:
2015
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
thin film
aluminum oxide
atomic layer deposition
Opis:
This paper presents some results of investigations on aluminum oxide Al2O3 thin films prepared by the atomic layer deposition method on polished monocrystalline silicon. It has been described how the technological parameters of the deposition process, like the number of cycles and substrate temperature, influenced the optical properties and morphology of prepared thin films. Their physical and optical properties like thickness, uniformity and refractive index have been investigated with spectroscopic ellipsometry, atomic force microscopy and UV/vis optical spectroscopy.
Źródło:
Optica Applicata; 2015, 45, 4; 573-583
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Temperature-dependence of cathodoluminescence of zinc oxide monolayers obtained by atomic layer deposition
Autorzy:
Witkowski, B S
Wachnicki, L
Nowakowski, P
Suchocki, A
Godlewski, M
Powiązania:
https://bibliotekanauki.pl/articles/173941.pdf
Data publikacji:
2013
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
zinc oxide
cathodoluminescence
profiling
temperature-dependence
localization
Opis:
We performed cathodoluminescence (CL) investigations of zinc oxide monolayers obtained by atomic layer deposition. Layers of different thickness were deposited on commercial GaN/sapphire templates. Scanning electron microscopy (SEM) system equipped with CL allows direct comparison of SEM images and CL maps, taken from exactly the same areas of samples. In addition to SEM and CL images, CL profiling was performed by collecting the CL spectra at different accelerating voltages. The CL profiling allows to distinguish the emissions from a surface and volume of samples. An inter-link between samples microstructure and emission properties is investigated. Shifts of emission bands, associated by us with the localization effects, are observed. CL investigations are supported by photoluminescence (PL) measurements, which are characterized by a higher spectral resolution. PL investigations allow determination of the origin of emission bands.
Źródło:
Optica Applicata; 2013, 43, 1; 187-194
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Leaching of zinc from low grade oxide ore using organic acid
Autorzy:
Irannajad, M.
Meshkini, M.
Azadmehr, A. R.
Powiązania:
https://bibliotekanauki.pl/articles/110892.pdf
Data publikacji:
2013
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
leaching
zinc oxide ore
citric acid
smithsonite
Opis:
The leaching of low grade zinc oxide mining tailings by organic acid as a leaching agent was investigated. Zinc was extracted successfully from sample by citric acid leaching. The effects of solid-to- liquid ratio, acid concentration, reaction time, temperature and ore particle size on the leaching efficiency were studied. The results obtained showed that particle sizes and reaction time had not any significant effect on the leaching recovery of zinc from smithsonite in the sizes range of 40-350 μm. Under conditions: temperature of 80ºC, reaction time of 60 min, citric acid concentration of 0.5 mol/L, and solid to liquid ratio of 1:10, 82% of zinc could be recovered.
Źródło:
Physicochemical Problems of Mineral Processing; 2013, 49, 2; 547-555
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of polysorbate 80 on the flotation of zinc oxide ores with amines
Autorzy:
Xie, Qiaoling
Wang, Dandan
Han, Zhichao
Tao, Huchun
Liu, Sitong
Powiązania:
https://bibliotekanauki.pl/articles/2146852.pdf
Data publikacji:
2022
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
polysorbate 80
pretreated amines
zinc oxide
flotation
Opis:
In this study, the influence of polysorbate 80 on zinc oxide flotation was investigated with an amine collector. The results indicated that the pretreatment of amines with polysorbate 80 enhanced the Zn grade and recovery obtained using zinc oxide flotation. Desliming prior to flotation is not suggested based on the results of this study. The appropriate temperature for flotation was as low as 8 °C, and this flotation method also could be applied to different types of zinc oxide ores. Under optimum flotation conditions, a concentrate with a Zn grade of 48.34% and a Zn recovery of 95.97% was obtained.
Źródło:
Physicochemical Problems of Mineral Processing; 2022, 58, 1; 149--158
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Zinc oxide as a functional admixture to cement composites
Autorzy:
Klapiszewska, Izabela
Ławniczak, Łukasz
Parus, Anna
Jesionowski, Teofil
Klapiszewski, Łukasz
Ślosarczyk, Agnieszka
Powiązania:
https://bibliotekanauki.pl/articles/2146946.pdf
Data publikacji:
2022
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
zinc oxide
admixtures
cement composites
antimicrobial tests
Opis:
There is an increasing trend in the modern construction industry to use nanomaterials, which allow to improve the performance of construction materials on the one hand, and to shape new properties on the other. This study presents the results of physicomechanical and antibacterial tests for cement composites modified with zinc nanooxide. The main aim of this study was to compare the structural and morphological properties of three selected commercial zinc nanooxides and to determine the influence of the above mentioned nanooxides on the physicomechanical properties of cement composites and the ability to inhibit the activity of gram-positive and gram-negative bacteria as well as fungi. It was shown that commercial nanooxides can significantly differ in terms of physicochemical properties, which depend on their production method. Two of them were characterized by high specific surface areas, which in turn translated into rheological properties of cement mortars. Nanooxides with higher specific surface areas tend to reduce the plasticity of the mortars. According to the literature data, all nanooxides caused a delay in cement binder setting by more than 100%. This resulted in a reduction of the early one-day flexural and compressive strength of the composite. In the later curing period, especially after 7 days of hardening, a significant acceleration of the hydration process was observed in composites with the addition of all nanooxides, which was confirmed by significant increases in mechanical parameters. Nevertheless, the tested nanooxides showed different sensitivity towards microorganisms, which was influenced by both the type of nanooxide and bacteria.
Źródło:
Physicochemical Problems of Mineral Processing; 2022, 58, 2; art. no. 145565
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Efficient sulfidization of lead oxide at high temperature using pyrite as vulcanizing reagent
Autorzy:
Zheng, Y.-X.
Lv, J.-F.
Wang, H.
Wen, S.-M.
Huang, L.
Powiązania:
https://bibliotekanauki.pl/articles/110351.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
lead oxide
sulfidization roasting
pyrite
reaction mechanism
TG
Opis:
A sulfidization roasting-flotation process was usually viewed to be effective in treating the refractory oxide ore. In this paper, pyrite was proposed to be applied as a potential vulcanizing reagent to transform PbO or its surface to PbS based on feasibilities of technology and economy. The evolution process, phase and characteristics of crystal growth were investigated by TG, XRD and SEM-EDS, respectively, to interpret the interaction mechanism of lead oxide and pyrite at high temperature. It was found that the decomposition process of pyrite under argon atmosphere was a slow process of sulfur released from FeS2 to FexS, which made the process easier to be controlled. When PbO was introduced into the system, the initial solid-solid (PbO-FeS2) reaction and prevailing solid-gas (PbO-S2(g)) reaction occurred at about 500 °C and 700 °C, respectively. Combined with the SEM-EDS analyses results, the optimal temperature for the sulfidization of PbO should be in the range of 700-750 °C.
Źródło:
Physicochemical Problems of Mineral Processing; 2018, 54, 2; 270-277
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Statistical approach to the production of cement composites doped with ZnO and ZnO-based materials
Autorzy:
Klapiszewska, Izabela
Balicki, Sebastian
Wilk, Kazimiera A.
Klapiszewski, Łukasz
Ślosarczyk, Agnieszka
Powiązania:
https://bibliotekanauki.pl/articles/24085675.pdf
Data publikacji:
2023
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
cement composite
zinc oxide
hybrid materials
design of experiments
Opis:
In this study, physical and functional properties of the cement composites containing ZnO, ZnO/lignin and lignin admixtures were investigated using Response Surface Methodology (RSM). The I-optimal design based on RSM was used to assess the influence of ZnO-based doping agent, of either commercial or synthetic origin, on cement composite production in the function of average compressive strength and cost. Polynomial mathematical models were developed by RSM confronting results from the experimental design. The accuracy and precision of the utilized models established by I-optimal design were tested using Analysis of Variance (ANOVA). The first stage of formulation optimization revealed that the use of commercially available ZnO-based admixture no. 4 (ZnO-SA, supplied by Sigma Aldrich) allowed to achieve the desired results, passing all the requirements, i.e., the best microbial purity combined with reasonable cost, followed by satisfactory physical properties. In the second stage of formulation optimization, the influence of implementing the hybrid materials, i.e., ZnO-SA mixed in different proportions with lignin was evaluated. RSM revealed that doping admixture no. 3, i.e., ZnO-SA/lignin (5:1), is the best candidate, which comprised augmented functional and physical properties of the fabricated cement composite. This component exhibited the best microbial purity as well as the lowest total pore volume, followed by satisfactory physical properties. Verification of the model findings indicated considerable agreement between the predicted and experimental values. From the findings, it was confirmed that a reasonable cost-performance balance for cement composites can be achieved using ZnO-SA and ZnO-SA/lignin (5:1).
Źródło:
Physicochemical Problems of Mineral Processing; 2023, 59, 4; art. no. 168352
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
TiO2 thin films grown on SiO2–Si(111) by the reactive evaporation method
Autorzy:
Grodzicki, M
Wasielewski, R
Mazur, P
Zuber, S
Ciszewski, A
Powiązania:
https://bibliotekanauki.pl/articles/173459.pdf
Data publikacji:
2013
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
titanium oxide
wettability
X-ray photoelectron spectroscopy
UV radiation
Opis:
TiO2 thin films were grown on silicon substrates using an electron-beam evaporator. Grainy TiO was used as the evaporation material. Temperature substrate during TiO2 growth was relatively low (about 150 °C), what is important for many optoelectronic devices and multilayers mirrors. High vacuum condition allows to maintain clean surfaces substrates before and during oxide growth. The morphology of titanium oxide thin films was ex situ investigated using atomic force microscopy operating in contact mode, X-ray photoelectron spectroscopy, X-ray powder diffractometry, and by means of a contact angle analyzer. The influence of annealing treatment and exposure to UV–VIS radiation on the morphology has been also discussed.
Źródło:
Optica Applicata; 2013, 43, 1; 99-107
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
On the possibility of using arc plasma melting technique in preparation of transparent yttria ceramics
Autorzy:
Kruk, Andrzej
Jany, Benedykt R.
Owczarczyk, Karolina
Madej, Dominika
Powiązania:
https://bibliotekanauki.pl/articles/173603.pdf
Data publikacji:
2019
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
plasma arc melting
transparent ceramic
yttrium oxide
optical properties
Opis:
A state-of-the-art fabrication of Y2O3 transparent ceramic by arc plasma synthesis using commercial micron-size powders is reported. The morphological observations of the surface by scanning electron microscope shows that a dense microstructure can be obtained. Arc melted samples are made of a white core and transparent layer. X-ray diffraction studies and also Raman spectroscopy confirm that only one phase occurred in the core and in the transparent layer, and that the physicochemical difference exists. The obtained Y2O3 shell ceramics have pores but also relative low absorbance in the VIS-NIR region after double side polishing. The optical band gap and the refractive index are reported. It is concluded that arc plasma melting allows obtaining quickly (10 minutes) dense and highly transparent polycrystalline samples, especially in the VIS-IR spectral region.
Źródło:
Optica Applicata; 2019, 49, 2; 355-364
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Buffering of pulp pH and its influence on process water chemistry during iron ore flotation
Autorzy:
Tang, Min
Xiao, Qingfei
Powiązania:
https://bibliotekanauki.pl/articles/1446441.pdf
Data publikacji:
2021
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
pulp pH
buffering
water chemistry
mineral dissolution
iron oxide
Opis:
It is inevitable for the occurrences of pulp pH buffering during pH control in flotation as the minerals with acidic/alkali properties tend to interact with pH modifiers and restore the pulp pH. This could result in some disturbing ions and alter the water/pulp chemistry. The purpose of this study was to identify the influences of pulp pH buffering on process water chemistry through a series of pH buffering tests, bench flotation experiments, ore dissolution tests, zeta potential measurement, and Xray diffraction (XRD) analysis. The built-up and distribution of the dominant cations in the process water from different locations in an industrial flotation system of the iron ore were analyzed and recorded by Inductively Coupled Plasma-Optical Emission (ICP-OES) at a period of about six months when the operations were stable. The data showed that a near five-minute buffer of pulp pH at a range from near 7.9 to 8.9 occurred before it reached a stable value. At this period, the dissolution of Ca/Mg from the iron ore was dominant. And, the pulp pH at a lower value tended to induce more dissolved $Ca^{2+}$ and $Mg^{2+}$ ions. These divalent cations seem to have different influences on the flotation properties of iron oxides at the same concentrations, indicating a positive effect on the recovery of iron oxides with the presence of $Mg^{2+}$ ions but an opposite effect if $Ca^{2+}$ ions occurred. The presence of sulfate, however, tended to restore the floatability of silicate depressed by $Ca^{2+}$ ions.
Źródło:
Physicochemical Problems of Mineral Processing; 2021, 57, 4; 157-167
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Evaluation of electrical resistivity, residual stress and surface roughness of sputtering indium tin oxide films with different thicknesses
Autorzy:
Tien, Chuen-Lin
Lin, Tsai-Wei
Su, Shu-Hui
Powiązania:
https://bibliotekanauki.pl/articles/2033888.pdf
Data publikacji:
2021
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
indium tin oxide
magnetron sputtering
residual stress
surface roughness
Opis:
This paper investigates the influence of film thickness on the electrical and mechanical properties of transparent indium tin oxide (ITO) thin films. Two groups of ITO thin films deposited on unheated substrates were prepared by the radio-frequency magnetron sputtering technique. The biaxial residual stress and surface roughness for two groups of ITO thin films were measured by a Twyman–Green interferometer and a Linnik microscopic interferometer, respectively. The electrical resistivity of the ITO films was measured by a four-point probe apparatus, the thickness was determined mechanically with a profilometer. The measurement results show that the average resistivity of ITO thin films decreases with increasing the deposited thickness. The compressive residual stress in the ITO thin films decreases with increasing the deposited thickness. We also find that an anisotropic stress in the two groups of ITO films is more compressive in a certain direction. The RMS surface roughness in the two groups of ITO films is less than 1 nm.
Źródło:
Optica Applicata; 2021, 51, 4; 499-512
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of ZnO:Al layers for applications in thin film solar cells
Autorzy:
Zdyb, A.
Krawczak, E.
Lichograj, P.
Powiązania:
https://bibliotekanauki.pl/articles/173619.pdf
Data publikacji:
2016
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
transparent conductive oxide
magnetron sputtering
thin film solar cell
Opis:
Thin films of zinc oxide doped with aluminium were obtained by using the magnetron sputtering technique on glass substrates. The changes in magnetron power influence the structural, optical and electrical properties of the ZnO:Al layers. The deposited films are characterized by very good homogeneity and high optical transmission. Thicker films with larger agglomerates on the surface exhibit lower resistivity with the remaining good transparency.
Źródło:
Optica Applicata; 2016, 46, 2; 181-185
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 49

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