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    Tytuł:
    The influence of electron and gamma irradiation on the properties of starch : PVA films : the effect of irradiation dose
    Autorzy:
    Cieśla, Krystyna A.
    Abramowska, Anna
    Powiązania:
    https://bibliotekanauki.pl/articles/1841645.pdf
    Data publikacji:
    2021
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    starch
    PVA film
    poly(vinyl alcohol)
    gamma irradiation
    electron irradiation
    UV-VIS
    mechanical properties
    swelling
    solubility
    Opis:
    The paper discusses the effect of ionizing radiation on the functional properties of the biodegradable starch:PVA films. The analysis is related to the possible use of the material for packing the products (particularly, food) that are predicted for radiation decontamination and to the potential modifi cation of the material by radiation treatment. Our previous results have shown that the infl uence of ionizing radiation on the films’ properties varied for the specific compositions (differing in starch:PVA ratio or the type of substrates) and depended on irradiation conditions. However, these studies considered only the irradiation performed in gamma chamber or in e-beam using a dose of 25 kGy. Therefore, the present study deals with the effect of the irradiations performed using various doses on the selected promising starch:PVA composition. The films characterized by starch:PVA weight ratio of 45:55 was obtained by solution casting and irradiated with fast electrons in air and with 60Co gamma rays in nitrogen applying the doses of 5, 10, 20, 25, 30, 50, and 75 kGy. No regular dependence has been noticed between the composition of films (differing in the starch and PVA content) and the intensities of the particular bands in the UV-VIS DRS spectra after irradiation. The results indicated strong interaction of the starch and PVA components in the films and the occurrence of specific reactions in each composition upon irradiation. No special differences were observed between tensile strength and Young’s modulus of the non-irradiated films characterized by the starch:PVA ratio equal to 45:55 and the samples irradiated using doses in the range of 5–75 kGy. Similarly, no differences were observed in both cases between the swelling capability of the non-irradiated and the irradiated films. However, it can be deduced that solubility in water increased when the radiation dose increased. The results show that using the doses till the range 25 kGy does not cause an essential change of all the examined properties of the starch:PVA (45:55) films. Accordingly, starch:PVA (45:55) films might be considered suitable for packing food predicted for radiation decontamination.
    Źródło:
    Nukleonika; 2021, 66, 1; 3-9
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preliminary studies of the influence of starch irradiation on physicochemical properties of films prepared using starch and starch-surfactant systems
    Autorzy:
    Cieśla, K. A.
    Nowicki, A.
    Buczkowski, M. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/148406.pdf
    Data publikacji:
    2010
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    starch films
    starch-surfactants films
    gamma irradiation
    mechanical properties
    barrier properties
    hydrophobic
    Opis:
    The influence was studied of potato and wheat starch irradiation on physicochemical properties of films, prepared using either starch alone or a composition of potato starch with three surfactants: sodium laurate, sodium palmitate and cetyl-trimethyl-ammonium bromide (CTAB). The surfactants were introduced at a level of 0.038 division sign 0.075 g per 1 g of starch. This corresponds to 0.136–0.222 mmol/g, depending on the surfactant type and its amount used. Irradiations were carried out using 60Co radiation with doses of 5, 10, 20 and 30 kGy. Films were prepared with addition of glycerol (0, 20 or 30% in terms of starch mass) by means of casting from the gelatinized starch or starch-surfactant solutions. With the purpose to characterize the films, mechanical tests (using an Instron instrument) and the wetting angle measurements were performed. The effect was determined of the storage and conditioning in an atmosphere characterized by the various moisture content on the properties of films with various compositions. The results show the radiation-induced improvement of hydrophobic properties of the films prepared using potato and wheat starch, and the selected potato starch-surfactant compositions. Improvement of strength and flexibility was obtained in the case of potato starch films, while in the case of wheat starch films the increase of strength was accompanied by a decrease in flexibility. Improvement of the functional properties of potato starch films corresponds to the improvement of their structural properties, found by scanning electron microscopy (SEM). The possibilities of modification of the films properties by modification of composition and radiation treatment were discussed.
    Źródło:
    Nukleonika; 2010, 55, 2; 233-242
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The influence of ionizing radiation on the properties of starch-PVA films
    Autorzy:
    Abramowska, A.
    Cieśla, K. A.
    Buczkowski, M. J.
    Nowicki, A.
    Głuszewski, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/147450.pdf
    Data publikacji:
    2015
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    starch
    poly(vinyl alcohol)
    films
    ionizing radiation
    mechanical properties
    physicochemical properties
    Opis:
    The cornstarch: poly(vinyl alcohol) (PVA) films characterized by the alternating ratio of starch:PVA (100:0, 80:20, 60:40, 40:60, 20:80, and 0:100) and containing 30% of glycerol were prepared by solution casting. The films were irradiated with an absorbed dose of 25 kGy with gamma rays in a vacuum and with fast electrons in the air. The films characterized by a high content of starch appeared stiff, while the films characterized by a high content of PVA were highly flexible. The tensile strength and flexibility, as well as swelling and hydrophilicity, increased with the increase in the PVA content in the films. However, the tensile strength and wetting angle values achieved a minimum at an intermediate composition. It was found that irradiation enables to reduce hydrophilicity of the films accompanied by a decrease in their flexibility. No general conclusion concerning the effect of irradiation on tensile strength and swelling behavior can be derived. An increase in the homogeneity of the films and an increase in the compatibility of their components was found by scanning electron microscopy (SEM). Strong interactions of the starch and the PVA components were discovered by diffuse reflectance spectroscopy. Degradation was found to be the prevailing process occurring in the films under the infl uence of irradiation. The possible accompanying crosslinking is discussed in terms of the gel content in the samples. Creation of various oxidation products in the films characterized by the modified composition was observed under the influence of irradiation carried out in the air. Basing on the obtained results it can be supposed that the selected starch-PVA compositions might appear useful as packagings of the products predicted for radiation decontamination.
    Źródło:
    Nukleonika; 2015, 60, No. 3, part 2; 669-677
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Intercomparison of radon CR-39 detector systems conducted in CLORs calibration chamber
    Autorzy:
    Mamont-Cieśla, K.
    Stawarz, O.
    Karpińska, M.
    Kapała, J.
    Kozak, K.
    Grządziel, D.
    Chałupnik, S.
    Chmielewska, I.
    Olszewski, J.
    Przylibski, T. A.
    Żebrowski, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/148842.pdf
    Data publikacji:
    2010
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    radon-222
    CR-39 track detector
    intercomparison
    RadoSys
    Opis:
    Six radon laboratories, which perform indoor radon measurements to jointly investigate temporal variations of radon concentration in houses in a couple of regions in Poland, participated in the intercomparison exercise. There are involved three commercially available Hungarian RadoSys systems and four own laboratory methods. All of them are based on the etched-track CR-39 detectors. The intercomparison was conducted in a calibration laboratory of the Central Laboratory for Radiological Protection (CLOR), Warsaw, Poland, accredited by the Polish Center for Accreditation (previously AP 101, at present AP 057). Comparison measurements were performed during three expositions in the CLOR’s radon calibration chamber under controlled normal climatic conditions and steady radon concentration. The results were referred to the value of the radon concentration determined by AlphaGUARD monitor traceable to the primary 222Rn standard in Physikalisch-Technische Bundesanstalt (PTB), Braunchweig, Germany. The mean performance ratio defined as a ratio of the reference to participant’s result range from 0.88 to 1.31.
    Źródło:
    Nukleonika; 2010, 55, 4; 589-593
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-4 z 4

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