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Tytuł:
Microstructure and properties of alloyed silver-gold nanoparticles
Autorzy:
Prymak, O.
Ristig, S.
Meyer-Zaika, W.
Raabe, D.
Epple, M.
Powiązania:
https://bibliotekanauki.pl/articles/285180.pdf
Data publikacji:
2014
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
nanoparticles
microstructure
alloyed nanoparticles
Opis:
Alloyed silver-gold nanoparticles recently raised an interest in biomedicine as potential antibacterial and surface-functionalized agents for imaging, drugdelivery, and tumor thermo-therapy [1,2]. The here synthesized alloyed AgAu nanoparticles with different compositions of silver and gold, as determined by atomic absorption spectroscopy (AAS), were prepared by reduction with citrate and tannic acid in aqueous media and subsequently functionalized by the addition of polyvinylpyrrolidone (PVP) [3]. UV spectroscopy confirmed that the particles consisted of alloyed Ag:Au and are not of a separate core-shell structure. The resulting nanoparticles were monodisperse and had a uniform size of ~6 nm, except pure Ag and Ag:Au-90:10, as shown by differential centrifugal sedimentation (DCS) and transmission electron microscopy (TEM). By means of X-ray powder diffraction (XRD) and use of Rietveld refinement [4], the precise lattice parameters, crystallite size and microstrain were determined. Based on the results by XRD, DCS and TEM it was shown, that the nanoparticles were not twinned, except pure Ag and Ag:Au-90:10. Additionally, a distinct deviation from Vegard’s linear rule of alloy mixtures for the lattice parameter was found for the nanoparticles. This effect was also found for AgAu bulk materials, but was much more pronounced in the nanostate. Further investigations of the crystal structure of the alloyed nanoparticles by means of synchrotron radiation might be helpful to gain more information about the interactions of silver and gold atoms.
Źródło:
Engineering of Biomaterials; 2014, 17, no. 128-129; 77
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of microstructure and chemistry of carbon nanomaterials coatings on nerve cells
Autorzy:
Frączek-Szczypta, A.
Wedel-Grzenda, A.
Jantas, D.
Powiązania:
https://bibliotekanauki.pl/articles/285693.pdf
Data publikacji:
2016
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
carbon nanomaterials
nerve cells
microstructure
Źródło:
Engineering of Biomaterials; 2016, 19, 138; 119
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Evaluation of the differentiation of structural and physicochemical properties of orthodontic wires of AISI 304 stainless steel
Autorzy:
Grygier, D.
Hoppe, V.
Zięty, A.
Rutkowska-Gorczyca, M.
Powiązania:
https://bibliotekanauki.pl/articles/284164.pdf
Data publikacji:
2018
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
stainless steel
orthodontics wire
microstructure
Opis:
Wires used for orthodontic arches play a very important role in the process of orthodontic treatment. In combination with the lock attached to the tooth, they move and align the teeth along the set trajectories. Wires of stainless steel are commonly used in orthodontics for several reasons: they are characterised by high resistance to corrosion, high strength and elasticity, formability and a possibility of obtaining defined properties through cold working and annealing during production process. The purpose of the research presented in the work is the analysis of differences of the selected structural properties in the context of corrosion resistance of the orthodontic wire material. The object of the research was edge arches of the 0.016”x0.022” size made of the stainless steel type AISI 304, provided by two different producers: G&H Orthodontics and Adenta. The research methodology involved analysis of chemical and phase composition of the tested alloy, microscopic tests with application of the light and electron microscopy methods, as well as electrochemical direct current measurements. The research presented in the work has shown significant differences in structural and physical-chemical properties of the orthodontic wires made of AISI 304 type stainless steel. Despite the fact, that the tested arches were manufactured of the theoretically the same materials, but by different producers, they significantly differ in chemical composition, metallurgical purity, phase composition and corrosion resistance. In addition, it is worth noticing that the tested materials, in terms of structure, do not meet the normative requirements obligatory for biomaterials.
Źródło:
Engineering of Biomaterials; 2018, 21, 146; 8-13
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Modification of microparticles’ microstructure with carbon dioxide for application as cell carriers in modular tissue engineering
Autorzy:
Mielan, B.
Krok-Borkowicz, M.
Pamuła, E.
Powiązania:
https://bibliotekanauki.pl/articles/284508.pdf
Data publikacji:
2018
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
carbon dioxide
tissue engineering
microstructure
Źródło:
Engineering of Biomaterials; 2018, 21, 148; 102
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Laser modified functional carbon-based coatings on titanium substrate for cardiac tissue integration and blood clotting inhibition
Autorzy:
Major, Roman
Ostrowski, Roman
Surmiak, Marcin
Trembecka-Wójciga, Klaudia
Lackner, Jurgen
Powiązania:
https://bibliotekanauki.pl/articles/1844973.pdf
Data publikacji:
2020
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
thin layers
migration channels
laser ablation
microstructure
Opis:
The work focused on developing functional coatings on titanium substrates that would facilitate the integration with the cardiac tissue and with a specific form of connective tissue like blood. Surface modifications consisted in the laser evaporation of part of the biocompatible layer, thus creating a suitable environment for a particular tissue. For the myocardium integration, the metal surface was refined by biohemocompatible coatings. Such surfaces were the starting point for further modifications in the form of channels. The channeled surfaces enabled a controlled cell migration and proliferation. The interaction of endothelial cells with the material was highly dependent on the surface characteristics such as: topography, microstructure or mechanical properties. The controlled cellular response was achieved by modifying the surface to obtain a network of wells or channels of different dimensions via the laser interference lithography. This technique determined a high resolution shape, size and distribution patterns. As a result, it was possible to control cells in the scale corresponding to biological processes. The surface periodization ensured the optimal flow of oxygen and nutrients within the biomaterial, which was of a key importance for the cell adhesion and proliferation. The work attempted at producing the surface networks mimicking natural blood vessels. To stimulate the formation of new blood vessel the finishing resorbable synthetic coatings were applied on the surface to act as a drug carrier. Therefore, the initial trial to introduce factors stimulating the blood vessels growth was performed.
Źródło:
Engineering of Biomaterials; 2020, 23, 155; 22-31
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphological studies of tissues stabilized by glutaraldehyde and tannic acid
Autorzy:
Turek, B.
Marcinkowski, A.
Cwalina, B.
Nożyński, J.
Dzierżewicz, Z.
Powiązania:
https://bibliotekanauki.pl/articles/286147.pdf
Data publikacji:
2009
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
glutaraldehyde
tannic acid
porcine pericardium
microstructure
nanostructure
Opis:
Despite the disadvantages of glutaraldehyde (GA)-stabilization of tissues, it is the method most often used for xenogeneic tissues preparation. Nowadays, partial elimination of drawbacks of this method is achieved by using GA in the mixture with other crosslinking reagents, which completes the stabilization effects and acts synergistically. The aim of this work was to determine microstructure and nanostructure of porcine pericardium stabilized by GA and tannic acid (TA). The microstructure was examined by optical microscopy and the nanostructure by atomic force microscopy (AFM). Different results on the level of micro- and nanostructure were observed. No essential changes in the tissue morphology after crosslinking with GA and TA were observed under optical microscope, but significant morphological differences were revealed in AFM studies.
Źródło:
Engineering of Biomaterials; 2009, 12, no. 89-91; 32-34
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Badania mikrostruktury porowatych pokryć modelowych implantów dokostnych
Experimental investigations of porous coatings microstructure of model endoosseous implants
Autorzy:
Uklejewski, R.
Winiecki, M.
Rogala, P.
Powiązania:
https://bibliotekanauki.pl/articles/284916.pdf
Data publikacji:
2009
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
mikrostruktura
implanty
porowate pokrycia
microstructure
implants
porous coatings
Źródło:
Engineering of Biomaterials; 2009, 12, no. 89-91; 113-115
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Degradation analysis of radiosensitizer control release system based on the NMR spectroscopy
Autorzy:
Buszman, A.
Kasperczyk, J.
Jaworska, J.
Powiązania:
https://bibliotekanauki.pl/articles/284117.pdf
Data publikacji:
2012
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
biodegradable polyesters
NMR spectroscopy
hydrolytic degradation
polymeric chain microstructure
Opis:
The degradation process of multilayer radiosensitizer releasing systems was conducted and examined via the nuclear magnetic resonance spectroscopy. Copolymers of glycolide and lactide with different chain microstructure were used as biocompatible drug carriers. Metronidazole was used as radiosensitizer. The changes of copolymers chain microstructure were monitored during 16 weeks of hydrolytic degradation of material in artificial Cerebro-spinal Fluid Solution. This study shows distinct differences in the rate of copolymer degradation and changes of the degree of randomness, directly connected with the type of comonomers and the comonomeric molar ratio. During 16 weeks of hydrolytic degradation, copolymers with L-lactidyl units remain resistant to hydrolysis while materials with D,L-lactidyl units are completely degraded. Examined materials can be used as carriers of agents for different types of short-, mid- and long-term therapies based on control release systems.
Źródło:
Engineering of Biomaterials; 2012, 15, 113; 16-18
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mikrostruktura i właściwości niskotarciowej nanokompozytowej powłoki nc-TiC/a-C na utwardzonym tlenem stopie Ti-6Al-7Nb
Microstructure and properties of low friction nanocomposite nc-TiC/a-C coating on Ti-6Al-7Nb alloy
Autorzy:
Moskalewicz, M.
Wendler, B.
Zimowski, S.
Czyrska-Filemonowicz, A.
Powiązania:
https://bibliotekanauki.pl/articles/284418.pdf
Data publikacji:
2010
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
stopy tytanu
endoprotezy
mikrostruktura
titanium alloys
joint prostheses
microstructure
Opis:
W pracy przedstawiono charakterystykę mikro/nanostruktury, właściwości mikro-mechanicznych i tribologicznych powłoki nc-TiC/a-C osadzonej na utwardzonym powierzchniowo atomami tlenu stopie Ti-6Al-7Nb. Badania mikro/nanostruktury przeprowadzono za pomocą skaningowej i transmisyjnej mikroskopii elektronowej na próbkach z przekroju poprzecznego. Stwierdzono, że powłoka nc-TiC/a-C zbudowana jest z nanokrystalicznych cząstek TiC w amorficznej osnowie węgla. W warstwie wierzchniej utwardzonego tlenem stopu występował roztwór stały tlenu w tytanie α(O). Zastosowana obróbka powierzchniowa istotnie poprawiła mikrotwardość oraz właściwości tribologiczne stopu Ti-6Al-7Nb (wzrost odporności na zużycie przez tarcie, zmniejszenie współczynnika tarcia).
The microstructure as well as micro-mechanical and tribological properties of the nc-TiC/a-C coating deposited on oxygen hardened Ti-6Al-7Nb alloy were examined. Scanning- and transmission electron microscopy investigations on cross-section specimens were used for determination of microstructure and phase composition. It was found that the nc-TiC/a-C coating is composed of TiC nanocrystals embedded in an amorphous carbon matrix. The Ti α(O) solid solution enriched by interstitial oxygen atoms was mainly present in the near-surface region. A particular preliminary surface treatment of specimens significantly improved microhardness and final tribological properties: it increased wear resistance and decreased friction coefficient of the alloy against alumina bearing ball dry ball-on-disc sliding tests.
Źródło:
Engineering of Biomaterials; 2010, 13, no. 99-101; 42-44
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wpływ atmosfery wypalania na zagęszczanie, morfologię i właściwości sprężyste spieków z naturalnego hydroksyapatytu
Effect of sintering atmosphere on densification, morphology and elastic properties of natural origin hydroxyapatite
Autorzy:
Brzezińska-Miecznik, J.
Macherzyńska, B.
Haberko, K.
Mozgawa, W.
Bućko, M.
Pyda, A.
Powiązania:
https://bibliotekanauki.pl/articles/285506.pdf
Data publikacji:
2009
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
hydroksyapatyt
spiekanie
mikrostruktura
właściwości sprężyste
hydroxyapatite
sintering
microstructure
elastic properties
Opis:
Naturalny hydroksyapatyt został wyekstrahowany z korowej części długich kości wieprzowych poprzez potraktowanie ich gorącym roztworem NaOH, przemycie H2O i wyprażenie w temperaturze 450°C. Pod ciśnieniem 200 MPa wyprasowano próbki, które spiekano w atmosferze powietrza, CO2 i argonu w temperaturze 1000°C. Stwierdzono, że atmosfera spiekania wpływa na zagęszczenie, morfologię, stabilność chemiczną i w konsekwencji na właściwości sprężyste spieków. W wyniku spiekania hydroksyapatytu w powietrzu uzyskano gęste spieki o dużych, wykształconych ziarnach. Próbki spiekane w argonie i w CO2 charakteryzują się mniejszym zagęszczeniem i drobnoziarnistą mikrostrukturą. Stwierdzono także, że atmosfera CO2 nie tylko przeciwdziała rozkładowi hydroksyapatytu (nie pojawia się wolne CaO), lecz powoduje wbudowywanie się grup CO3(2-) w strukturę.
Natural hydroxyapatite was extracted from cortical part of long pig bones by treatment in hot sodium hydroxide solution. Material was washed with water, dried and calcined at 450°C. Cylindrical samples compacted under 200 MPa were sintered in air, CO2 and Ar atmospheres at 1000°C. Sintering atmosphere influences densification, microstructure, chemical stability and consequently elastic properties of the samples. Treatment in air atmosphere leads to the most dense material of the largest and faceted grains. Lower densification and smaller grains occur in CO2 and Ar atmospheres. Carbon dioxide atmosphere counteracts decomposition of the material, no free CaO appears, but additional CO3(-2) groups become built into the HAp structure.
Źródło:
Engineering of Biomaterials; 2009, 12, 86; 17-21
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Badania mechanizmu biodegradacji in vivo terpolimerów z pamięcią kształtu
The mechanisms of shape memory terpolymers’ in vivo degradation
Autorzy:
Jaros, A.
Gębarowska, K.
Stojko, J.
Kasperczyk, J.
Smola, A.
Powiązania:
https://bibliotekanauki.pl/articles/285214.pdf
Data publikacji:
2011
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
terpolimery
degradacja
mikrostruktura
implant
pamięć kształtu
terpolymers
degradation
microstructure
shape memory
Opis:
W pracy przedstawiono wyniki badań degradacji in vivo trzech różnych terpolimerów LL-laktydu, glikolidu i węglanu trimetylenu z pamięcią kształtu. Polimery charakteryzowano wykorzystując analizę DSC (właściwości termiczne), GPC (masy cząsteczkowe) i NMR (skład i mikrostruktura). Badano sterylne matryce polimerowe przed wszczepieniem oraz po określonym czasie inkubacji w organizmie królika. Oceniono przydatność badanych materiałów do zastosowania w produkcji biozgodnych polimerowych resorbowalnych chirurgicznych systemów z pamięcią kształtu.
The hereby work presents the result of the in vivo studies on the mechanism of degradation of three different lactide-co-glicolide-co-TMC shape memory terpolymers. The polymers were characterized by using DSC (thermal properties), GPC (molecular weights) and NMR (composition and microstructure) method. Sterile polymeric matrices were analyzed before implantation and after a determined period of time, after incubation in vivo in a rabbit body. The suitability of the tested materials in the production of polymeric biocompatible resorbable surgical systems with shape memory effect was determined.
Źródło:
Engineering of Biomaterials; 2011, 14, no. 106-108; 79-84
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Assessment of the microstructure and mechanical properties of porous gelatin scaffolds
Autorzy:
Morawska-Chochół, Anna
Powiązania:
https://bibliotekanauki.pl/articles/2058382.pdf
Data publikacji:
2021
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
scaffold
microstructure
tissue engineering
gelatin
freeze-drying
mikrostruktura
inżynieria tkankowa
żelatyna
Opis:
Gelatin scaffolds are in the interest of tissue engineering and drug release. The scaffold porosity and microarchitecture are of great importance in proper tissue regeneration. In this work, the freeze-drying method was used to produce the scaffolds. The effect of concentration of the initial gelatin solution and pre- -freezing temperature on the scaffold’s microstructure and microarchitecture (porosity, pores size, shape, and distribution) was evaluated. The mechanical tests of samples were performed. Moreover, the influence of the gentamicin sulphate addition on the gelatin scaffolds microstructure and mechanical properties was also studied. The linear relationship of porosity to the concentration of the initial solution was observed. Therefore, it is possible to obtain a scaffold with a planned porosity. Pores were interconnected with an aspect ratio between 1.5-1.8. For porosity 74 ± 9% the average pore size was 0.7 ± 0.6 mm, with most pores in the range 0.2-0.4 mm. For the samples with porosity 57 ± 14%, the average pore size was 0.2 ± 0.2 mm, with most pores in the range 0.05-0.2 mm. The process of pre-freezing the solution in liquid nitrogen caused the highest porosity of the sample, the smaller pores size and the lower pores size distribution in comparison to the sample pre-frozen in -20°C. The mechanical parameters for all the samples are sufficient for filling bone defects. The addition of a drug to gelatin caused only slight changes in the pore architecture. This material could be applied as a scaffold in the bone loss correlated to bacterial infection.
Źródło:
Engineering of Biomaterials; 2021, 4, 160; 22--27
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
New design of patient-specific, antimicrobial bioactive finger implants for durable functional reconstruction after amputation
Autorzy:
Dyner, Marcin
Byrski, Adam
Major, Roman
Gawlikowski, Maciej
Kasperkiewicz, Katarzyna
Lackner, Juergen M.
Dyner, Aneta
Major, Bogusław
Powiązania:
https://bibliotekanauki.pl/articles/2058387.pdf
Data publikacji:
2021
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
finger implant
thin coatings
microstructure
cytotoxicity
microbiology
implanty
palce
cytotoksyczność
mikrobiologia
Opis:
The absence of even a single finger results in a major impairment in the hand function (precise grasping, grip power), therefore significantly affecting the social and professional life of victims who are frequently young people. Finger amputation is a surgical treatment for ~69.000 patients in the EU after traumatic injury, in which replantation microsurgery fails due to the severity of tissue damage. The surgical reconstruction is currently possible only via autograft transplantation, e.g. a toe-to-hand transfer, thus leading to foot impairment. Some motion functional restoration is also possible using a bone-anchored silicone prosthesis but without the sense revalidation. Our current research focuses on alternatives for surgical reconstruction by means of novel patient- -specific, durable, biomimetic, bioactive and antibacterial implants for reconstructing lost bone and joints. The implant design – and the improved micro(neuro) surgery (beyond the project) – will consist in the fast successful rehabilitation, including the soft-tissue related mobility, the implantation of state-of-the-art nerve conduits as well as the aesthetic appearance. Key issues for the long-term functionality of the biomaterial-based reconstruction of hard tissue are based on surgical demands, such as: (1) perfect integration of a bone-substituting metal with the surrounding bone tissue (a) with no signs of loosening due to stress shielding at the interface and (b) enhanced with protective activity against bacterial inflammation (antimicrobial properties and formation of vascularized bone tissue (ossification)) even months to years after the injury; (2) biomimetic finger joints based on non-wearing materials without ossification meant to prevent the loss of the motion function.
Źródło:
Engineering of Biomaterials; 2021, 24, 161; 8--14
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Micro- and nanopatterned surfaces for guided adhesion, growth and phenotypic maturation of cells
Autorzy:
Bacakova, L.
Filova, E.
Grausova, L.
Vandrovcova, M.
Parizek, M.
Novotna, K.
Svorcik, V.
Vacik, J.
Rypacek, F.
Kromka, A.
Heitz, J.
Shard, A.
Powiązania:
https://bibliotekanauki.pl/articles/284586.pdf
Data publikacji:
2009
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
surface patterning
microstructure
nanostructure
biofunctionalization
endothelial cells
vascular smooth muscle cells
bone cells
Opis:
Micropatterned surfaces were created by UV light-irradiation of polytetrafluoroethylene through a metallic mask, by successive plasma polymerization of acrylic acid and 1,7-octadiene, or by creation of prominences and grooves by deposition of fullerenes C60 through a metallic mask. All these surface types were capable of inducing regionally-selective adhesion, proliferation and phenotypic maturation of vascular endothelial cells, vascular smooth muscle cells or human bone-derived MG 63 cells. Nanopatterned surfaces created by tethering GRGDSG oligopeptides through polyethylene oxide chains on a polymeric surface promoted spreading, formation of focal adhesion plaques and DNA synthesis in vascular smooth muscle cells. Surfaces nanopatterned with nanocrystalline diamond gave good support for the adhesion, growth and metabolic activity of osteoblast-like MG 63 cells.
Źródło:
Engineering of Biomaterials; 2009, 12, no. 89-91; 18-21
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The influence of different types of carbon nanomaterial on the properties of coatings obtained by EPD process
Autorzy:
Wedel-Grzenda, A.
Tran, K.
Frączek-Szczypta, A.
Powiązania:
https://bibliotekanauki.pl/articles/284778.pdf
Data publikacji:
2016
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
graphene oxide
multi-walled carbon nanotubes
electrophoretic deposition
hybrid coatings
surface properties
microstructure
Opis:
The first part of research is concentrated on the examination of four kinds of carbon nanomaterials: graphene oxide (GO), multi-walled carbon nanotubes (MWCNT), multi-walled carbon nanotubes functionalized by authors in acids mixture (MWCNT-F) and multi-walled carbon nanotubes with hydroxyl groups (MWCNT-OH). Their microstructure was observed in transmission electron microscopy (TEM). Based on these microphotographs, the diameters of carbon nanotubes were measured. Then, in order to determine the chemical composition of GO, MWCNT-F and MWCNT-OH, X-ray photoelectron spectroscopy was applied. The second part of study concerns the properties of the coatings deposited electrophoretically on titanium surface from previously examined nanomaterials. The coatings from individual nanomaterials, as well as hybrid layers (combination of two kinds of nanomaterial: graphene oxide with one of the nanotubes’ type) were deposited. Microstructure of the coatings was evaluated with the use of scanning electron microscopy (SEM). Furthermore, surface properties, important while considering usage of these materials in biological applications: wettability and surface free energy were evaluated. These materials are meant for application in regeneration and stimulation of nerve cells. All the research carried out so far indicate the influence of nanotubes’ functionalization degree on the properties of their suspension, as well as the characteristics of the deposited coating. It also influences the interaction between two types of nanomaterials. Functionalization in strong acids introduces functional groups which change nanotubes’ dimensions, properties and behavior in solution.
Źródło:
Engineering of Biomaterials; 2016, 19, 135; 13-20
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 21

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